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Short Note

(±)-((2S,5R)-5-(Acetoxymethyl)tetrahydrofuran-2-yl)methyl Benzoate

Department of Chemical Sciences, University of Naples Federico II, Via Cintia 4, 80126 Naples, Italy
Academic Editor: Nicola Della Ca
Molbank 2022, 2022(1), M1349; https://doi.org/10.3390/M1349
Received: 9 February 2022 / Revised: 23 February 2022 / Accepted: 1 March 2022 / Published: 4 March 2022
(This article belongs to the Collection Molecules from Catalytic Processes)
In this note we report the synthesis of a doubly acylated cis-THF-diol product synthesised in three steps by the stereoselective RuO4-catalysed oxidative cyclisation of 1,5-hexadiene, followed by benzoylation and acetylation. This substance is one of the substrates chosen to probe a new developed oxidative procedure to transform bis-acylated THF-diols into bis-acylated 1,4-diketones. This new derivative was fully characterised by spectroscopic methods. View Full-Text
Keywords: bis-acylated α-bis-hydroxymethyl-tetrahydrofuran; oxidative cyclization; 1H-NMR; 13C-NMR; FTIR; HRESIMS bis-acylated α-bis-hydroxymethyl-tetrahydrofuran; oxidative cyclization; 1H-NMR; 13C-NMR; FTIR; HRESIMS
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MDPI and ACS Style

Piccialli, V. (±)-((2S,5R)-5-(Acetoxymethyl)tetrahydrofuran-2-yl)methyl Benzoate. Molbank 2022, 2022, M1349. https://doi.org/10.3390/M1349

AMA Style

Piccialli V. (±)-((2S,5R)-5-(Acetoxymethyl)tetrahydrofuran-2-yl)methyl Benzoate. Molbank. 2022; 2022(1):M1349. https://doi.org/10.3390/M1349

Chicago/Turabian Style

Piccialli, Vincenzo. 2022. "(±)-((2S,5R)-5-(Acetoxymethyl)tetrahydrofuran-2-yl)methyl Benzoate" Molbank 2022, no. 1: M1349. https://doi.org/10.3390/M1349

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