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(E)-3-(2,5-Dimethoxyphenyl)-1-{[4-(2,5-dimethoxy-phenyl)-6-((E)-2,5-dimethoxystyryl)-2-thioxo-1,2,3,4-tetrahydropyrimidin-5-yl]}prop-2-en-1-one and (E)-3-(2,5-Dimethoxyphenyl)-1-{[4-(2,5-dimethoxyphenyl)-6-methyl-2-thioxo-1,2,3,4-tetrahydropyrimidin-5-yl]}prop-2-en-1-one
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Department of Life Sciences, School of Sciences, European University Cyprus, 6 Diogenis Str., Engomi, P.O. Box 22006, 1516 Nicosia, Cyprus
Department of Chemistry, University of Cyprus, P.O. Box 20537, 1678 Nicosia, Cyprus
Author to whom correspondence should be addressed.
Molbank 2019, 2019(2), M1064;
Received: 23 May 2019 / Revised: 6 June 2019 / Accepted: 8 June 2019 / Published: 9 June 2019
(This article belongs to the Special Issue Heteroatom Rich Organic Heterocycles)
The reaction of 3-chloro-5-methoxy-4H-1,2,6-thiadiazin-4-one (9) with Na2S·9H2O (0.5 equiv) in tetrahydrofuran (THF) at ca. 20 °C for 20 h gives 5,5′-thiobis(3-methoxy-4H-1,2,6-thiadiazin-4-one) (10) in a 44% yield as yellow needles. The compound was fully characterized. View Full-Text
Keywords: heterocycle; 1,2,6-thiadiazine; sulfide; nucleophilic displacement heterocycle; 1,2,6-thiadiazine; sulfide; nucleophilic displacement
MDPI and ACS Style

Kalogirou, A.S.; Koutentis, P.A. 5,5′-Thiobis(3-methoxy-4H-1,2,6-thiadiazin-4-one). Molbank 2019, 2019, M1064.

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