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Open AccessArticle

First Synthesis of (−)-Altenuene-D3 Suitable as Internal Standard for Isotope Dilution Mass Spectrometry

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HPC Standards GmbH, Am Wieseneck 7, D-04451 Borsdorf, Germany
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AnalytiCon Discovery GmbH, Hermannswerder Haus 17, D-14473 Potsdam, Germany
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Bundesanstalt für Materialforschung und –prüfung, Abteilung Analytische Chemie, Referenzmaterialien, Richard-Willstätter-Strasse 11, D-12489 Berlin-Adlershof, Germany
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Author to whom correspondence should be addressed.
Academic Editor: Ari Koskinen
Molecules 2019, 24(24), 4563; https://doi.org/10.3390/molecules24244563
Received: 11 November 2019 / Revised: 5 December 2019 / Accepted: 10 December 2019 / Published: 12 December 2019
Metabolites from Alternaria fungi exhibit a variety of biological properties such as phytotoxic, cytotoxic, or antimicrobial activity. Optimization of a literature procedure culminated in an efficient total synthesis of (−)-altenuene as well as a stable isotope-labeled derivative suitable for implementation in a LC-MS/MS method for mycotoxin analysis. View Full-Text
Keywords: altenuene; Alternaria mycotoxins; food safety; isotope-labeled; SIDA-LC-MS/MS; Suzuki coupling altenuene; Alternaria mycotoxins; food safety; isotope-labeled; SIDA-LC-MS/MS; Suzuki coupling
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MDPI and ACS Style

Sebald, M.A.; Gebauer, J.; Sommerfeld, T.; Koch, M. First Synthesis of (−)-Altenuene-D3 Suitable as Internal Standard for Isotope Dilution Mass Spectrometry. Molecules 2019, 24, 4563.

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