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Open AccessArticle

Synthesis of γ-Nitro Aliphatic Methyl Esters Via Michael Additions Promoted by Microwave Irradiation

Centro de Investigaciones Químicas, Universidad Autónoma del Estado de Morelos. Av. Universidad No. 1001, Col. Chamilpa, C.P. 62210 Cuernavaca, Mor., Mexico
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Molecules 2009, 14(4), 1595-1604; https://doi.org/10.3390/molecules14041595
Received: 5 February 2009 / Revised: 21 March 2009 / Accepted: 8 April 2009 / Published: 21 April 2009
(This article belongs to the Special Issue Microwave Assisted Synthesis)
A simple and efficient protocol has been developed for the direct synthesis of γ-nitrobutyric acid methyl esters under microwave irradiation. This methodology reduces reaction times from days to minutes, compared to conventional conditions. Additionally, these conditions increased yields and provided cleaner reactions. View Full-Text
Keywords: Microwave irradiation; α; β-Unsaturated; Michael additions; γ-Nitro aliphatic methyl esters; Catalysis Microwave irradiation; α; β-Unsaturated; Michael additions; γ-Nitro aliphatic methyl esters; Catalysis
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Escalante, J.; Díaz-Coutiño, F.D. Synthesis of γ-Nitro Aliphatic Methyl Esters Via Michael Additions Promoted by Microwave Irradiation. Molecules 2009, 14, 1595-1604.

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