Search Results (15)

Joints of copper sheets with a thickness of 0.8 mm were produced by ultrasonic welding. To assess the quality of the joints, tensile lap-shear strength, area fraction of bonding, distributions of normal strains in the cross sections of welded samples, linear weld density at a magnification of ×1000, and the microstructure and microhardness of welded samples were analyzed. It was proved that the arrangement of microbonds and length of gaps in joint zones significantly depended on the local normal strains of welded samples caused by the penetration of tool ridges under the clamping pressure. Joint regions with a linear weld density of more than 70% were observed if the local compression strains of the sample exceeded 15%. The appearance of local tensile strains was accompanied by a drop in the linear weld density of the joints in some regions, down to 5%. The distribution of normal strains depends on the mutual positions of the ridges of the welding tip and anvil. It is concluded that in order to improve the quality of joints obtained by ultrasonic welding and reduce the scatter of their strength values, welding tools should provide sufficiently high normal compression strains in the weld spot area. Full article

This study improved homemade apparatus for characterizing the interfacial shear strength (IFSS) of carbon-fiber-reinforced polyphenylene sulfide (PPS/CF) composites. The upgraded generation II experimental device includes a newly developed experimental clamp for samples, as well as testing systems. Compared with the initial generation I apparatus and the commercial Toei instrument, the generation II device is easier and more efficient to operate. The average interfacial adhesion values obtained using these devices were consistently approximately 40 MPa, with relatively low data scatter, showing excellent repeatability and applicability during microbond tests. Notably, the generation II experimental device was equipped with an additional high-frequency data-capturing tool to identify the debonding peak force more precisely, which demonstrated a higher interfacial shear strength of 42.81 MPa during testing. Therefore, the new instrument was able to reflect the change in the interfacial stress state during the interface debonding process more accurately and reliably. Full article

Ultrasonic consolidation is an advanced process of sequential solid-state joining of metal foils or sheets by ultrasonic welding. This process was used for joining six sheets of nickel with a thickness of 0.2 mm. Ultrasonic consolidation was accompanied by the formation of wear particles between the sheets. The appearance of microbonds between the sheet surface and the wear particles led to the formation of parallel rows of voids and swirl-like patterns near the interfaces. It was shown that ultrasonic consolidation of nickel sheets led to the formation of fine recrystallized grains near contact surfaces and a subgrain structure in the bulk of the consolidated layers. The microstructural changes were accompanied by an increase in the microhardness of nickel from 1567 MPa in the initial sheet to 2065 and 2400 MPa, respectively, in the bulk and joint zones of the consolidated sample. However, significant differences in the microstructure and microhardness of the layers were not revealed, despite the fact that the accumulated plastic deformation and thermal effects were different from layer to layer. This unexpected result was explained by an inhomogeneity of the microstructure of the nickel samples obtained by ultrasonic consolidation and by a possible interplay between ultrasonic residual hardening and softening. Full article

Processing structural or semi-structural thermoplastic-based composites is a promising solution to solve the environmental issues of the aeronautic industry. However, these composites must withstand high standard specification to ensure safety during transportation. For this reason, there is a real need to develop strong interactions between thermoplastic polymers and reinforcement fibers. This paper investigates relationships between the surface chemistry, microstructure and micromechanical properties between polyphenylene sulfide and ex-PAN carbon fibers. The incorporation of ionic salt such as 1,3-Bis(4-carboxyphenyl)imidazolium chloride into neat polyphenylene sulfide was able to significantly increase the interfacial shear strength measured by microbond micromechanical test combined with different carbon fiber surfaces treatment. Full article

Currently, the vast majority of composite waste is either landfilled or incinerated, causing a massive burden on the environment and resulting in the loss of potentially valuable raw material. Here, conventional pyrolysis and reactive pyrolysis were used to reclaim carbon fibers from aeronautical scrap material, and to evaluate the feasibility of using reclaimed carbon fibers in structural components for the automotive sector. The need for fiber sizing was investigated as well as the behavior of the fiber material in macroscopic impact testing. The fibers were characterized with the single fiber tensile test, scanning electron microscopy, and the microbond test. Critical fiber length was estimated in both polypropylene and polyamide matrices. Tensile strength of the fiber material was better preserved with the reactive pyrolysis compared to the conventional pyrolysis, but in both cases the interfacial shear strength was retained or even improved. The impact testing revealed that the components made of these fibers fulfilled all required deformation limits set for the components with virgin fibers. These results indicate that recycled carbon fibers can be a viable option even in structural components, resulting in lower production costs and greener composites. Full article

The microbond test of natural fibers tends to produce scattered interfacial shear stress (IFSS) values. The sources of this scattering are known, but the roles they play in producing high IFSS scattering remain to be investigated. In this study, a numerical method was used to simulate microbond testing and to examine the experimental parameters in a microbond test of Typha angustifolia fiber/epoxy. Three parameters were considered: fiber diameter, fiber length embedded in the epoxy, and the distance between the vise and the specimen. The geometries were modeled and analyzed by ABAQUS software using its cohesive zone model features. There were two types of contact used in this analysis: tie constraint and surface-to-surface. The results showcased the roles of the following experimental parameters: a larger fiber diameter from a sample increased the IFSS value, a longer embedded length reduced the IFSS value, and a shorter vise–specimen distance increased the IFSS value. The IFSS scattering in the microbond test could have originated from the interaction between these parameters. Of the three parameters, only the vise–specimen distance was found to be able to be reasonably controlled. When the IFSS value was atypically large, fiber diameter and/or embedded length potentially drove the scattering. This study advises further compilation and classification of the role of each experimental parameter in modulating the IFSS value. Full article

Aramid fibers are high-strength and high-modulus technical fibers used in protective clothing, such as bulletproof vests and helmets, as well as in industrial applications, such as tires and brake pads. However, their full potential is not currently utilized due to adhesion problems to matrix materials. In this paper, we study how the introduction of mechanical adhesion between aramid fibers and matrix material the affects adhesion properties of the fiber in both thermoplastic and thermoset matrix. A microwave-induced surface modification method is used to create nanostructures to the fiber surface and a high throughput microbond method is used to determine changes in interfacial shear strength with an epoxy (EP) and a polypropylene (PP) matrix. Additionally, Fourier transform infrared spectroscopy, atomic force microscopy, and scanning electron microscopy were used to evaluate the surface morphology of the fibers and differences in failure mechanism at the fiber-matrix interface. We were able to increase interfacial shear strength (IFSS) by 82 and 358%, in EP and PP matrix, respectively, due to increased surface roughness and mechanical adhesion. Also, aging studies were conducted to confirm that no changes in the adhesion properties would occur over time. Full article

Growing environmental concerns and stringent waste-flow regulations make the development of sustainable composites a current industrial necessity. Natural fibre reinforcements are derived from renewable resources and are both cheap and biodegradable. When they are produced using eco-friendly, low hazard processes, then they can be considered as a sustainable source of fibrous reinforcement. Furthermore, their specific mechanical properties are comparable to commonly used, non-environmentally friendly glass-fibres. In this study, four types of abundant natural fibres (jute, kenaf, curaua, and flax) are investigated as naturally-derived constituents for high performance composites. Physical, thermal, and mechanical properties of the natural fibres are examined to evaluate their suitability as discontinuous reinforcements whilst also generating a database for material selection. Single fibre tensile and microbond tests were performed to obtain stiffness, strength, elongation, and interfacial shear strength of the fibres with an epoxy resin. Moreover, the critical fibre lengths of the natural fibres, which are important for defining the mechanical performances of discontinuous and short fibre composites, were calculated for the purpose of possible processing of highly aligned discontinuous fibres. This study is informative regarding the selection of the type and length of natural fibres for the subsequent production of discontinuous fibre composites. Full article

The focus of this paper is the realization and verification of a modified fiber bundle pull-out test setup to estimate the adhesion properties between threads and elastic matrix materials with a more realistic failure mode than single fiber debond techniques. This testing device including a modified specimen holder provides the basis for an adequate estimation of the interlaminar adhesion of fiber bundles including the opportunity of a faster, easier, and more economic handling compared to single fiber tests. The verification was done with the single-fiber and microbond test. Overall, the modified test setup showed the typical pull-out behavior, and the relative comparability between different test scales is given. Full article

The microbond test for natural fibers is difficult to conduct experimentally due to several challenges including controlling the gap distance of the blade, the meniscus shape, and the large data spread. In this study, a finite element simulation was performed to investigate the effects of the bonding characteristics in the interface between the fiber and matrix on the Typha fiber/epoxy microbond test. Our aim was to obtain the accurate mesh and cohesive properties via simulation of the Typha fiber/epoxy microbond test using the cohesive zone model technique. The axisymmetric model was generated to model the microbond test specimen with a cohesive layer between the fiber and matrix. The cohesive parameter and mesh type were varied to determine the appropriate cohesive properties and mesh type. The fine mesh with 61,016 elements and cohesive properties including stiffness coefficients K_nn = 2700 N/mm³, K_tt = 2700 N/mm³, and K_ss = 2700 N/mm³; fracture energy of 15.15 N/mm; and damage initiation t_nn = 270 N/mm², t_tt = 270 N/mm², and t_ss = 270 N/mm² were the most suitable. The cohesive zone model can describe the debonding process in the simulation of the Typha fiber/epoxy microbond test. Therefore, the results of the Typha fiber/epoxy microbond simulation can be used in the simulation of Typha fiber reinforced composites at the macro-scale. Full article

The dispensing resolution of high-viscosity liquid is essential for adhesive micro-bonding. In comparison with the injection technique, the transfer printing method appears to be promising. Herein, an analytical model was developed to describe the dynamic mechanism of squeezing-and-deforming a viscous droplet between plates in a transfer printing process: as the distance between plates decreases, the main constituents of contact force between the droplet and substrate can be divided into three stages: surface tension force, surface tension force and viscous force, and viscous force. According to the above analysis, the transfer printing method was built up to dispense high-viscosity adhesives, which replaced the geometric parameters, utilized the critical contact force to monitor the adhesive droplet status, and served as the criterion to trigger the liquid-bridge stretching stage. With a home-made device and a simple needle-stamp, the minimum dispensed amount of 0.05 nL (93.93 Pa·s) was achieved. Moreover, both the volume and the contact area of adhesive droplet on the substrate were approximately linear to the critical contact force. The revealed mechanism and proposed method have great potential in micro-assembly and other applications of viscous microfluidics. Full article

In this work, bamboo fibers are chemically modified with NaOH solution of 1, 4, and 7 wt% concentrations at room temperature, respectively, and subsequently the untreated and treated fibers are prepared with epoxy resin for unidirectional composites by hot pressing molding technique. Tensile and micro-bond tests are conducted on the composite specimens to obtain mechanical properties, such as tensile strength and modulus, elongation at break, and interfacial strength. Besides, scanning electron microscopy (SEM) is employed to perform morphological observations for constituent damages. In addition, the influence of alkali concentration on the thermal performance of epoxy-based composites is examined by using differential scanning calorimetry (DSC) and thermogravimetric (TG) analysis. It is found that composite tensile strength reaches the maximum when the alkali concentration is 4%, increased by 45.24% compared with untreated composites. The composite elongation at break increases on increasing the concentration. Inversely, the composite modulus decreases as the concentration increases. Besides, the results demonstrate that the chemical treatment on the fiber surface could improve interface adhesion, as observed from its topography by SEM. Micro-bond test reveals that there is maximum interfacial shear strength when the alkali concentration is 4%, which increases by 100.30% in comparison with the untreated samples. In case of thermal properties, the DSC analysis indicates that the glass transition temperature is maximized at 4% alkali concentration, which is increased by 12.95%, compared to those from unmodified fibers. In addition, TG results show that the 4% concentration also facilitates thermal stability improvement, indicative of superior interfacial bonding. Full article

The outstanding diffusivity and permeability of supercritical carbon dioxide (scCO₂) are extremely beneficial for grafting reaction. In this work, aramid fibers (AF) are modified in scCO₂ by glycidyl-polyhedral oliomeric silsesquioxane (POSS) with 2-ethyl-4-methylimidazole (2E4MZ) on the basis of cleaning with acetone. The surface morphology and chemical structure of the modified AF were measured and characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Scanning electron microscope (SEM), Thermogravimetric (TG), and Atomic force microscope (AFM). The interfacial shear strength (IFSS) was measured by a micro-bond pull-out test, then the modified AF/EP composites were prepared and the interlaminar shear strength (ILSS) was characterized. Research has shown that some of the glycidyl-POSS molecular chains permeated into the surface of the fiber and grafted onto the surface of the AF after modification, and the other glycidyl-POSS self-assembled on the surface of the fiber. XPS indicated the introduction of C–O and –COO–, which confirmed the existence of chemical reactions between AF and glycidyl-POSS. AFM and SEM images revealed that 2E4MZ, not only promoted the grafting reaction of glycidyl-POSS, but also intensified the self-assembly of glycidyl-POSS, both of which increased the roughness of the fiber. A monofilament tensile test and micro-bond pull-out test showed that there was a negative effect on the tensile strength after scCO₂ processing. The tensile strength of modified AF, with glycidyl-POSS, increased the highest strength of 25.7 cN dtex⁻¹, which was 8% higher than that of pristine AF. The improvement of ILS roughness and the polar chemical groups produced in grafting reaction. These results indicated that AF, treated in scCO₂, with glycidyl-POSS, which is a suitable way of fiber modification, can significantly improve the surface adhesion of AF reinforced composites. Full article

This study reports the application of an optoacoustic method for evaluating the bonding strength of ultrasonically bonded joints in a non-destructive and non-contact fashion. It is proposed that the bonding strength is correlated with the resonant frequency of bonded joints. The bonding strength measured with a destructive tensile test roughly increased with the vibration time, however, it varied, causing the transitional and dispersed formation of micro-bonds at the bonding interface. Scanning Electron Microscopic observation of the fractured surface suggested that the bonding strength depends on the total bonded area of micro-bonds. Frequency response of the bonded joint was examined with a non-destructive method using a piezo-electric vibrator. The experiment revealed that the resonant frequency exponentially increased with the bonding strength. In addition, this vibration behavior was dynamically visualized with electronic speckle pattern interferometry (ESPI). The correlation between the bonded area and the resonant frequency is discussed based on finite element analysis. The results indicate the possibility for in-situ evaluation of the ultrasonic bonding strength. Full article

Two high-performance bacterial cellulose (BC) nanofiber-based hybrid structures were produced using an in situ self-assembly approach, one with microfibrillated cellulose (MFC) and another with sisal fiber, by incorporating them in the fermentation media. The fabricated BC-MFC hybrid and BC-sisal hybrid fibers showed enhanced mechanical properties compared to pure BC and sisal fibers, respectively. Tensile tests indicated BC-MFC hybrid and their nanocomposites fabricated with soy protein isolate (SPI) resin had better tensile properties than corresponding BC and BC-SPI nanocomposites. This was because of the uniform distribution of MFC within the BC nanofiber network structure which reduced the defects such as pores and voids or intersections of the BC nanofibers. BC-sisal hybrid fibrous structures were obtained after BC nanofibers self-assembled on the surface of the sisal fibers during the fermentation. The results of the microbond tests indicated that the BC-sisal hybrid fiber/SPI resin bond strength was higher than the control sisal fiber/SPI resin bond with p value of 0.02 at the significance level of 0.05. Higher bond strength is preferred since it can potentially lead to better tensile properties of the composites. The presented work suggests a novel route to fabricate hybrid nanocomposites with higher functional properties. Full article