Search Results (11)

The boiling point of metals is dependent on the ambient pressure. Therefore, in laser-based fusion welding and additive manufacturing processes, the resulting process regime, ranging from heat conduction welding to the keyhole mode, is also influenced by the process pressure. While laser welding deliberately uses reduced process pressures to achieve the keyhole mode with a lower laser power input as well as a more stable keyhole, there are no positive findings on the laser powder bed fusion process (PBF-LB/M) under vacuum conditions so far. Furthermore, the literature suggests that the process window is significantly reduced, particularly in the high vacuum regime. However, this work demonstrates that components made of the ferritic steel 22NiMoCr3-7 can be successfully manufactured at low process pressures of ${2 \times 10}^{-2} \mathrm{mbar}$ using a double-scanning strategy. The strategy consists of a first scan with a defocused laser beam, where the powder is preheated and partially sintered, followed by a second scan with a slightly defocused laser beam, in which the material within a single layer is completely melted. To test this manufacturing strategy, 16 test cubes were manufactured to determine the achievable relative densities and tensile specimens were produced to assess the mechanical properties. Metallographic analysis of the test cubes revealed that relative densities of up to 98.48 ± 1.43% were achieved in the test series with 16 different process parameters. The tensile strength determined ranged from 722 to 724 MPa. Additionally, a benchmark part with complex geometric features was successfully manufactured in a high vacuum atmosphere without the need for a complex parameterization of individual part zones in the scanning strategy. Full article

Hermetic glass-to-metal sealing (GMTS) technology combines metal and glass and can be used to construct vacuum tubes; electric discharge tubes; semiconductor diodes; reed switches; and pressure-tight glass-to-metal windows, optical windows, and lenses in electronics or electronic systems. The hermetic and mechanically strong seals engineered using GTMS are highly reliable, making them suitable for deployment in harsh environments and for applications requiring high performance. However, it has always been challenging to precisely and robustly join glass and metal due to the significant disparities in their properties. In this study, the laser transmission welding of borosilicate glass and aluminum alloy using a pulsed Nd:YAG laser to achieve hermetic glass–metal seals was experimentally investigated. This research focused on various processing parameters and the influence of surface conditions on bonding quality. Three different types of surfaces—a polished surface, a surface subjected to preoxidation, and a laser-modified surface—were compared. To evaluate the weld strength, shear-tensile separation forces were measured. The analysis of fracture and separation encompassed detailed examinations of the weld morphology, microstructure, and elemental composition. The results revealed that increasing the laser welding energy initially enhanced the weld strength until a saturation point was reached. Among the three different surface treatments tested, the laser surface modification of aluminum alloy yielded the highest weld strength. The maximum achieved bond force exceeded 35.38 N, demonstrating the feasibility of using cost-effective pulsed laser welding for glass-to-metal sealing. The results were significantly better than those from previous research in which aluminum alloy surfaces were pretreated using microarc oxidation. Full article

Hot-dip galvanized components offer a great potential for corrosion protection of up to 100 years, while laser beam welding in vacuum (LaVa) has the advantage of high penetration depths Combined, this process chain can be economically used in steel construction of bridges, wind turbines, or other steel constructions. Therefore, investigations of butt joint welding of galvanized 20 mm thick S355M steel plates using LaVa were carried out. The butt joints were prepared under different cutting edges such as flame-cut, sawn, and milled edges, and they were studied with and without the zinc layer in the joint gap. For this purpose, the laser parameters such as the beam power, welding speed, focus position, and working pressure all varied, as did the oscillation parameters. The welds performed using an infinity oscillation with an amplitude of 5 mm represented a pore-free weld up to a zinc layer thickness of 400 µm in the joint gap. The seam undercut increased with increasing the zinc layer thickness in the joint gap, which can be explained by the evaporating zinc and consequently the missing material, since no filler material was used. The joint welds with zinc only on the sheet surface achieved a sufficient weld quality without pores. Full article

The diffusion welded joint of oxide dispersion strengthened tungsten (ODS-W) and Mo-Ti-Zr-C alloy (TZC) was successfully fabricated with the use of spark plasma sintering (SPS) at a vacuum level of 10 Pa. This study systematically investigates the microstructure, mechanical performance, and thermal shock resistance of the ODS-W/TZC connector at four different temperatures, ranging from 1300 to 1600 °C. The diffusion distance between the W and Mo atoms at the interface of ODS-W/TZC joint raises as the sintering temperature increases, with a maximum diffusion distance of up to 2 μm at 1500 °C, but then slightly decreases at 1600 °C. The ODS-W/TZC connector bonded at 1500 °C exhibits the best tensile performance, with tensile strengths of 459 MPa and 786 MPa at room temperature and 500 °C, respectively. A maximum hardness of 446 HV is obtained at the interface when the sample is sintered at 1600 °C. Thermal shock tests are conducted on the surface and interface of the ODS-W/TZC connector sintered at various temperatures. ODS-W/TZC samples prepared below 1500 °C were severely damaged, leading to exfoliation after laser thermal shock, while samples prepared above 1500 °C produced fewer damage cracks. Confocal laser scanning microscope (CLSM) analysis demonstrated that the ODS-W/TZC joint fabricated at 1500 °C exhibited substantially reduced height perturbation of both its surface and interface compared to that of ODS-W, providing evidence for its superior thermal shock resistance. Full article

Titanium alloy is an important material for the manufacture of key components of deep-sea submersibles. High-power vacuum laser welding is an important method for welding TC4 thick plate (40–120 mm) structures. However, due to the low melting point of aluminum, its uneven distribution in the weld caused by evaporation during welding affects the quality of joints. This paper conducted experimental and simulation studies to investigate the effect of process parameters on multi-component evaporation and uneven aluminum distribution. Based on a three-dimensional model of vacuum laser welding, the mechanism of the uneven distribution of aluminum in the weld is explained. The results show that the uneven distribution of aluminum in the weld is mainly related to the metal vapor behavior and keyhole morphology. As the welding speed rises from 1 m/min to 3 m/min, the proportion of aluminum in the metal vapor and the degree of compositional unevenness increase. When the laser power increases from 6 kW to 18 kW, the proportion of aluminum in the metal vapor and degree of unevenness increase, peak at 12 kW, and then decrease. This work facilitates the selection of suitable process parameters to reduce aluminum evaporation during the high-power vacuum welding of Ti-6Al-4V alloys. Joints with a more stable performance can be obtained by avoiding the uneven distribution of aluminum. Full article

In this study, the optimal parameters of the vacuum brazing titanium alloy Ti-6Al-4V with TiCuNi filler (30 μm-thick metal foil) were investigated by the Taguchi method. The microstructures, microhardness, and fractographs of the titanium brazed joints produced by these optimal parameters were also analyzed. The results of this study demonstrate that for the best tensile strength, the optimal combination of process parameters is: 890 °C soaking temperature, 60 min soaking time, 975 °C brazing temperature, and 45 min brazing time. The tensile strength obtained by welding with the optimal parameters was found to be 1265 MPa. A small error of 0.24% between experimental and predicted values confirmed the validity of the combined optimized parameters. Finally, from the means of variance analysis (ANOVA), out of the four factors, the highest contribution to the optimal parameters was found to be the brazing time, accounting for 47.3%. The base material of vacuum brazing (VB) weldment is mainly composed of white granular α titanium, slender β titanium, and layered structures that are interlaced by α and β. The weld bead, composed of Ti-15Cu-15Ni, contains many slender needle-shaped Widmanstätten structures. This structure is associated with higher strength and lower ductility. The weld bead hardness of the vacuum brazed parts is higher than that of laser beam weldment and gas tungsten arc weldment. This study demonstrates the feasibility of the Taguchi method for obtaining the optimal process parameters of titanium vacuum brazed joints. Full article

Laser sealing for vacuum plate glass is a key step in developing the cost-effective smart vacuum-glass window for the drive towards net-zero energy buildings. In this paper, the pores, cracks, and interface with laser welding are analyzed in depth using PbO-TiO₂-SiO₂-RxOy system sealing solder to prepare vacuum flat glass. The microstructure of the sealing layer was analyzed by a BX41M-LED metallographic microscope, and the interfacial bonding characteristics were observed by thermal field emission scanning electron microscopy (SEM). The solder was analyzed by an energy spectrometer, and the influence of laser power, sealing temperature, and sealing speed on the gas holes and the crack sand interface separation of the sealing layer are reported. The results show that when the laser power reached 80 W at the welding speed of 2 mm/s, the bulk solder disappeared to most of the quantity and the sealing surface density was higher, due to which negligible pores and micro cracks were found. Thus, the sealing quality of the sealing layer is considered to be suitable when the temperature of 470 °C was maintained and the solder has 68.93% of Pb and 3.04% Si in the atom fraction to achieve the wet the glass substrate surface whilst improving the bonding quality. Full article

Vacuum laser beam welding enables deeper penetration depth and welding stability than atmospheric pressure laser welding. However, contaminated coupling glass caused by welding fumes in the vacuum space reduces laser transmittance, leading to inconsistent penetration depth. Therefore, a well-designed protective system is indispensable. Before designing the protective system, the contamination phenomenon was quantified and represented by a contamination index, based on the coupling glass transmittance. The contamination index and penetration depth behavior were determined to be inversely proportional. A cylindrical protective system with a shielding gas supply was proposed and tested. The shielding gas jet provides pressure-driven contaminant suppression and gas momentum-driven contaminant dispersion. The influence of the shielding gas flow rate and gas nozzle diameter on the performance of the protective system was evaluated. When the shielding gas flow was 2.0 L/min or higher, the pressure-driven contaminant suppression dominated for all nozzle diameters. When the shielding gas flow was 1.0 L/min or lower, gas momentum-driven contaminant dispersion was observed. A correlation between the gas nozzle diameter and the contamination index was determined. It was confirmed that contamination can be controlled by selecting the proper gas flow rate and supply nozzle diameter. Full article

The symmetrical insulated mug is composed of two layers. The two ends of the two layers form the mouth and bottom seams of the insulated mug. The weld quality of the two seams is very important to keep the vacuum degree of the air between the two layers, which is vital for the heat-insulating property of the mug. Due to the narrow seam, laser welding is used. Since laser welding has high demand on the relative position of the seam and the laser torch, a vision-based seam tracking system is designed. Before welding is started, the vision sensor scans the seam and feature sample points are collected. A reconstruction algorithm is proposed to form the image containing the seam. Then, a least square fitting (LSF) method combined with random sample consensus (RANSAC) method is proposed to detect the smooth seam from the sample points. In the welding process, a seam tracking system with fuzzy logic control method is presented to keep the torch precisely on the seam. Finally, full experiments are conducted in the welding factory of the insulated mugs to verify the effectiveness of the proposed system and method. Full article

To explore the mechanism of the pore formation in the laser-welded vacuum plate glazing sealing layer, a vacuum plate glazing laser side sealing test was carried out. The influence of the pulse current, pulse duration time, pulse frequency and welding speed on the pores of the sealing layer was studied by means of scanning electron microscopy (SEM) and metallographic microscopy, and the cause of the pores is analyzed. The results show that the porosity decreases with the increase of the pulse current. When the pulse current is 160 A, the pores are the fewest and smallest, and the porosity is only 0.1%. The porosity of the sealing layer decreases first and then increases with the increase of the pulse duration time. The porosity decreases first and then increases with the increase of the pulse frequency. When the pulse frequency is 18 Hz, the porosity is the least, at only 0.08%. The porosity of the sealing layer increases with the increase of the welding speed. When the welding speed is 80, 90, 100 and 110 mm/min, the porosity is 0.02, 0.08, 0.63 and 0.89%, respectively. These studies can provide a theoretical basis for laser sealing manufacturing of vacuum plate glazing. Full article

Laser welding has been widely used in various industry fields. In order to further alter and broaden its applicability, a novel technology of laser welding under vacuum is introduced. The combination of high power laser and low ambient pressure provides an excellent welding performance and quality. In this paper, an overview on laser welding under vacuum is presented. It begins with a short introduction about the research status of laser welding under vacuum. Next, the equipment of laser welding under vacuum is introduced. Then, the fundamental phenomena of laser welding under vacuum, including penetration depth, weld geometry, plasma plume, molten pool and keyhole behaviors, are summarized in detail. Finally, the applications and prospects of laser welding under vacuum are proposed. Full article