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59 pages, 62632 KB  
Review
Laser Shock Peening of Gear Steels and Related Metallic Materials: Near-Surface States, Surface Integrity, and Component-Level Applications
by Yuxuan Sheng, Xin Hou, Yi Hou, Wenjie Chen, Qianjin Liu, Xiaoqiang Li and Shengguan Qu
Materials 2026, 19(15), 3257; https://doi.org/10.3390/ma19153257 - 1 Aug 2026
Viewed by 203
Abstract
Contact fatigue, bending fatigue, and wear failures in gears are governed by the stress state, hardening gradient, microstructural stability, and surface topography within the near-surface and subsurface regions. For tooth flanks, rolling–sliding contact, asperity interaction, lubricant-film disturbance, and subsurface shear stress control micropitting, [...] Read more.
Contact fatigue, bending fatigue, and wear failures in gears are governed by the stress state, hardening gradient, microstructural stability, and surface topography within the near-surface and subsurface regions. For tooth flanks, rolling–sliding contact, asperity interaction, lubricant-film disturbance, and subsurface shear stress control micropitting, pitting, and spalling. For tooth-root fillets, local stress concentration and surface or near-surface defects dominate bending-fatigue crack initiation. Laser shock peening (LSP) introduces deep compressive residual stress, gradient hardening, and microstructural refinement, and is therefore relevant to gears when these effects are matched to the critical damage zones. This review examines LSP of gear steels and related load-bearing steels from the viewpoint of tooth-flank and tooth-root damage control. It links laser parameters, shock-induced plastic deformation, residual-stress depth, hardening response, surface roughness, and profile accuracy to bending fatigue, rolling contact fatigue, and wear behavior. LSP is most effective when the compressive residual-stress layer and hardened layer reach the contact- or bending-damage depth while lubrication compatibility, flank form accuracy, and subsequent finishing are preserved. Excessive pulse energy, overlap, or unstable absorbing/confining conditions may increase roughness, produce ablation or micropitting-sensitive defects, and compromise tooth profile accuracy. Thus, LSP for gears should be evaluated together with carburizing, nitriding, shot peening, surface rolling, polishing, coatings, and laser texturing rather than as an isolated treatment. The central task is to define gear-specific process windows that balance residual-stress depth, surface integrity, dimensional accuracy, and manufacturing repeatability. Full article
(This article belongs to the Special Issue Laser Technology for Materials Processing—Second Edition)
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24 pages, 8730 KB  
Article
Research on the Mechanism of Fabricating Hierarchical Microstructured Hydrophobic Surfaces via Laser Ablation Imprinting
by Genyi Li, Pin Li, Rui Zhang, Haoran Sun, Zheng Shi and Zongbao Shen
Metals 2026, 16(3), 349; https://doi.org/10.3390/met16030349 - 20 Mar 2026
Viewed by 441
Abstract
This study aims to reveal the mechanism of a novel method for fabricating hierarchical microstructured hydrophobic surfaces. Specifically, plasma shock waves induced by laser ablation are applied to the workpiece to replicate the microstructures on the mold surface, thus obtaining primary microstructures. Meanwhile, [...] Read more.
This study aims to reveal the mechanism of a novel method for fabricating hierarchical microstructured hydrophobic surfaces. Specifically, plasma shock waves induced by laser ablation are applied to the workpiece to replicate the microstructures on the mold surface, thus obtaining primary microstructures. Meanwhile, the material splashing effect induced by laser ablation is utilized to form secondary microstructures on the basis of the primary microstructures. Subsequently, fluorination treatment and aging treatment are adopted to alter the chemical composition of the hierarchical microstructures on the workpiece surface, thereby reducing the surface energy and enhancing hydrophobicity. In addition, this study investigates the effects of a different number of laser shocks, laser fluence and mold periods on the forming results. Under a laser fluence of 28.97 J/cm2, within the range of one to five laser shocks, the forming effect of the aluminum foil workpiece improves with the increase in the number of laser shocks. When the number of laser shocks is set to 3, within the laser fluence range of 19.1–76.39 J/cm2, the forming result of the aluminum foil workpiece is enhanced as the laser fluence increases. The larger the mold period, the better the forming effect of the workpiece. An analysis of aging treatment and fluorination treatment reveals their impacts on the workpiece through assessments of wettability, surface chemical composition, and surface morphology. The findings reveal that both aging and fluorination treatments significantly enhance the contact angle of the aluminum foil workpiece, all while preserving its original surface structure. The main changes occur in terms of element content and chemical composition, and a large number of non-polar groups are generated on the workpiece surface after the modification treatments. Full article
(This article belongs to the Special Issue Surface Treatments and Coating of Metallic Materials (2nd Edition))
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18 pages, 7585 KB  
Article
Design and Characterization of a Bench-Top Ludwieg Tube for Aerodynamic Measurements via Simultaneous Quantification of Mach Number and Velocity
by Boris S. Leonov, Richard Q. Binzley, Nathan G. Phillips, Roman Rosser, Farhan Siddiqui, Arthur Dogariu and Richard B. Miles
Fluids 2026, 11(3), 80; https://doi.org/10.3390/fluids11030080 - 15 Mar 2026
Viewed by 1081
Abstract
This article presents the design and detailed characterization of a new supersonic wind tunnel at the Aerospace Laboratory for Lasers, ElectroMagnetics, and Optics of Texas A&M University, tailored for optical diagnostic development and sub-scale fundamental compressible fluid dynamics research. A Ludwieg tube tunnel [...] Read more.
This article presents the design and detailed characterization of a new supersonic wind tunnel at the Aerospace Laboratory for Lasers, ElectroMagnetics, and Optics of Texas A&M University, tailored for optical diagnostic development and sub-scale fundamental compressible fluid dynamics research. A Ludwieg tube tunnel architecture was selected due to its robustness, versatility, and low operational costs. The tunnel consists of a 50-foot-long driver tube constructed from modular Tri-Clamp spools, a Mach 4 nozzle with 3 in. exit diameter configured as a free jet, and a fast-acting valve with 14 ms opening time for high-duty-cycle operation. Such construction proved to be a robust, compact, and affordable solution for academic applications. Characterization methods consisted of simultaneous high-speed dot-schlieren, total and static pressure measurements, and femtosecond laser electronic excitation tagging. Average flow velocity for the first steady-state test time was measured via FLEET at (668.0 ± 5.7) m/s. The Mach number was calculated based on the angles of the attached oblique shocks formed near the 30° cone model. Calculated Mach number was repeatable from run to run and had small oscillations near the average value of 3.96 ± 0.03. Based on the simultaneously measured velocity and Mach number, the static temperature was calculated to be between (68.6 ± 0.3) K and (66.3 ± 0.3) K throughout the 400 ms test time, completely defining the thermodynamic state of the generated freestream flow. Full article
(This article belongs to the Special Issue High-Speed Processes in Continuous Media)
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19 pages, 6995 KB  
Article
Amorphous Carbon-Mediated Microstructural Optimization for Enhanced Thermal Shock Resistance in TaC/Amorphous-Carbon Coatings
by Yi Hu, Jian Peng, Huanjun Jiang, Qiang Shen and Chuanbin Wang
Coatings 2026, 16(3), 345; https://doi.org/10.3390/coatings16030345 - 10 Mar 2026
Viewed by 737
Abstract
TaC/amorphous-carbon (TaC/a-C) composite coatings with varied a-C contents were deposited on graphite by dual-target magnetron sputtering to mitigate the thermal-expansion mismatch that commonly triggers cracking and spallation in TaC coatings on carbon substrates during rapid thermal cycling. However, existing TaC–C (often termed “free [...] Read more.
TaC/amorphous-carbon (TaC/a-C) composite coatings with varied a-C contents were deposited on graphite by dual-target magnetron sputtering to mitigate the thermal-expansion mismatch that commonly triggers cracking and spallation in TaC coatings on carbon substrates during rapid thermal cycling. However, existing TaC–C (often termed “free carbon”) approaches rarely identify the carbon’s structural state and spatial distribution explicitly, and a clear correlation between carbon fraction, thermal-shock-driven microstructural evolution, and cyclic damage remains insufficiently established. Increasing the a-C fraction progressively refines the TaC grain structure and introduces an a-C phase along grain boundaries, thereby lowering the effective coefficient of thermal expansion (CTE) and improving compatibility with the graphite substrate. Under laser thermal cycling, coatings with higher a-C contents exhibit markedly enhanced resistance to cracking and spallation. After 15 cycles, the high-a-C (~28.99 at.%) coating remains free of through-thickness cracks, maintains its thickness, and retains a single-phase TaC structure without detectable Ta2C, whereas the low-a-C coating shows severe thinning, through-cracks, and partial TaC → Ta2C transformation. Microstructural observations indicate that the a-C phase forms a compliant, stress-relaxing boundary network and promotes a porous, mechanically interlocked TaC architecture, synergistically redistributing thermal stresses and deflecting crack propagation. Full article
(This article belongs to the Special Issue Ceramic-Based Coatings for High-Performance Applications)
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15 pages, 5710 KB  
Article
Effect of Gradient Layer Induced by Laser Shock Peening on Adhesion and Wear Resistance of AlCrN Coatings on TC4 Titanium Alloy
by Ying Xu, Wenqian Yu, Xinlong Liao, Yuxuan Zhu and Boyong Su
Materials 2026, 19(3), 608; https://doi.org/10.3390/ma19030608 - 4 Feb 2026
Cited by 2 | Viewed by 636
Abstract
To address the inherent defects in the fabrication of AlCrN titanium alloy coatings and enhance interfacial bonding strength as well as tribological performance, an AlCrN coating was employed as an absorption layer and subjected to laser shock processing to form an AlCrN/TC4 transition [...] Read more.
To address the inherent defects in the fabrication of AlCrN titanium alloy coatings and enhance interfacial bonding strength as well as tribological performance, an AlCrN coating was employed as an absorption layer and subjected to laser shock processing to form an AlCrN/TC4 transition layer. Subsequently, a secondary AlCrN coating was deposited to construct a gradient coating architecture. The surface and cross-sectional morphologies and elemental distributions under varying laser energies were systematically investigated, and the influence of laser energy on the adhesion and wear resistance of the gradient coatings was analyzed. The results demonstrate that with increasing laser impact energy, the thickness of the AlCrN/TC4 transition layer gradually decreases from 3.75 μm to 1.32 μm, accompanied by significant changes in elemental distribution across the surface and cross-section. The interfacial bonding strength of the gradient coating increases substantially from 13.6 N to 43.3 N, while the average friction coefficient rises from 0.436 to 0.507. Concurrently, the wear track depth is reduced, and the wear rate decreases from 86.46 × 10−5 mm3/(N·m) to 7.67 × 10−5 mm3/(N·m). Laser shock peening promotes elemental diffusion, enabling the formation of a diffusion-aided interlayer. The incorporation of this diffused zone facilitates the successful construction of a high-quality TC4 titanium alloy gradient coating, effectively broadening the film–substrate interface, enhancing surface hardness, and significantly improving both interfacial adhesion and wear resistance. Full article
(This article belongs to the Special Issue Surface Modifications and Coatings for Metallic Materials)
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14 pages, 4168 KB  
Article
Effect of Laser Shock Peening Times on Low-Cycle Fatigue Properties and Fracture Mechanism of Additive TA15 Titanium Alloy
by Xu Pei, Sailan Wang, Zhaomei Xu, Zhouzhi Gu, Yuchun Peng and Pengfei Li
Materials 2025, 18(24), 5670; https://doi.org/10.3390/ma18245670 - 17 Dec 2025
Cited by 1 | Viewed by 831
Abstract
This study investigates the effects of multiple laser shock peening (LSP) treatments on the low-cycle fatigue performance and fracture mechanisms of laser-melted, additive-manufactured Ti-6.5Al-1Mo-1V-2Zr (TA15) titanium alloy. The primary objective is to systematically evaluate how different LSP impact numbers (0, 1, and 2 [...] Read more.
This study investigates the effects of multiple laser shock peening (LSP) treatments on the low-cycle fatigue performance and fracture mechanisms of laser-melted, additive-manufactured Ti-6.5Al-1Mo-1V-2Zr (TA15) titanium alloy. The primary objective is to systematically evaluate how different LSP impact numbers (0, 1, and 2 impacts) enhance fatigue life and alter fracture behavior. Low-cycle fatigue life was determined via tensile-compression fatigue testing. Microfracture morphology was examined using scanning electron microscopy (SEM), surface residual stresses were measured by X-ray diffraction (XRD), and microhardness tests were conducted concurrently. Results indicate that LSP significantly enhances fatigue life: fatigue life increased by 2.34 times and 2.56 times after one and two LSP impacts, respectively, compared to the untreated state. As impact cycles increased, the microhardness of the material surface rose by 8.51% and 14.53%, respectively, with residual compressive stresses reaching −145 MPa and −183 MPa. Concurrently, LSP-2 treatment formed a refined microstructure featuring coexisting lamellar α and acicular martensite in the surface layer. This strengthening effect is attributed to LSP-induced surface residual compressive stress, grain refinement, and the resulting migration of fatigue crack initiation from the surface to subsurface regions. These findings provide critical insights for optimizing fatigue-resistant designs of additively manufactured titanium alloy components. Full article
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13 pages, 7244 KB  
Article
Surface Integrity and Corrosion Resistance of Additively Manufactured AZ91 Mg Alloys Post-Processed by Laser Shock Peening
by Shan Gao, Wenquan Wang, Xintian Zhao, Wenhui Yu, Hongyu Zheng, Xingchen Yan, Cheng Chang, Harry M. Ngwangwa, Xiaoli Cui and Zongshen Wang
Metals 2025, 15(12), 1374; https://doi.org/10.3390/met15121374 - 15 Dec 2025
Cited by 2 | Viewed by 709
Abstract
Mg alloys show great potential in biomedical fields due to superior biocompatibility and biodegradability. Additive manufacturing (AM) provides opportunities in fabricating metallic implants with complex geometries while inherent defects during AM limit its further applications. In this work, laser shock peening (LSP) was [...] Read more.
Mg alloys show great potential in biomedical fields due to superior biocompatibility and biodegradability. Additive manufacturing (AM) provides opportunities in fabricating metallic implants with complex geometries while inherent defects during AM limit its further applications. In this work, laser shock peening (LSP) was employed as a post-processing technique to tailor the surface integrity and corrosion resistance of additively manufactured AZ91 Mg alloy by selective laser melting (SLM). The surface morphology, microstructure and porosity, surface hardness and residual stress, and corrosion resistance of the SLMed alloy before and after LSP were examined. The results show that a gradient structure is formed along the depth direction after LSP and high-density dislocations and high-fraction low-angle grain boundaries are induced. The porosity is gradually reduced in number and size and the highest density of 1.794 g/cm3 is obtained after two impacts of LSP. The surface hardness and residual compressive stress both increase with LSP number and the highest values of 135.26 HV and 40.13 MPa after four impacts, respectively. All of the SLMed alloy samples show improved corrosion resistance after LSP. This work provides a promising route for enhancing the performance of additively manufactured Mg alloys through laser materials surface modification. Full article
(This article belongs to the Special Issue Laser Shock Peening: From Fundamentals to Applications)
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12 pages, 3425 KB  
Article
Fatigue Performance Improvement of Titanium Alloy with Microstructure Gradient and Residual Stress Gradient Produced by Laser Shock Peening
by Libing Ren and Jutao Li
Coatings 2025, 15(12), 1443; https://doi.org/10.3390/coatings15121443 - 8 Dec 2025
Cited by 1 | Viewed by 1202
Abstract
In the present paper, the fatigue performance of a TC6 titanium alloy with a microstructure gradient and residual stress gradient produced by laser shock peening (LSP) is investigated. After LSP, a 1 mm thickness gradient compressive residual stress layer with a maximum surface [...] Read more.
In the present paper, the fatigue performance of a TC6 titanium alloy with a microstructure gradient and residual stress gradient produced by laser shock peening (LSP) is investigated. After LSP, a 1 mm thickness gradient compressive residual stress layer with a maximum surface compressive residual stress of −708 MPa is introduced into the materials. Electron back-scattering diffraction (EBSD) and transmission electron microscopy (TEM) techniques are used to characterize the microstructural evolution of the TC6 titanium alloy subjected to LSP. The results show that a nanostructured layer forms on the surface of the TC6 titanium alloy. At a depth of 20 μm, high dense dislocation and nanocrystalline are observed on the top surface. Based on the results of the microstructural characterization, it is found that dislocation movement is the main reason for the formation of nanocrystalline on the top surface. A high-cycle fatigue test showed that the fatigue limit of the TC6 titanium alloy treated by LSP improves from 431 ± 10 MPa to 486 ± 14 MPa, increasing by 12.8%. Full article
(This article belongs to the Section Corrosion, Wear and Erosion)
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35 pages, 5860 KB  
Review
Preparation Technology, Reactivity and Applications of Nano-Aluminum in Explosives and Propellants: A Review
by Huili Guo, Weipeng Zhang and Weiqiang Pang
Nanomaterials 2025, 15(20), 1564; https://doi.org/10.3390/nano15201564 - 14 Oct 2025
Cited by 5 | Viewed by 2264
Abstract
Aluminum powder is the most commonly used metal fuel in the industry of explosives and propellants. The research progress in preparation technology, reactivity and application of nano-aluminum in explosives and propellants is systematically reviewed in this paper. The preparation technology of nano-aluminum powder [...] Read more.
Aluminum powder is the most commonly used metal fuel in the industry of explosives and propellants. The research progress in preparation technology, reactivity and application of nano-aluminum in explosives and propellants is systematically reviewed in this paper. The preparation technology of nano-aluminum powder includes mechanical pulverization technology (such as the ball milling method and ultrasonic ablation method, etc.), evaporation condensation technology (such as the laser induction composite heating method, high-frequency induction method, arc method, pulsed laser ablation method, resistance heating condensation method, gas-phase pyrolysis method, wire explosion pulverization method, etc.), chemical reduction technology (such as the solid-phase reduction method, solution reduction method, etc.) and the ionic liquid electrodeposition method, each of which has its own advantages. Some new preparation methods have emerged, providing important reference value for the large-scale production of high-purity, high-quality nano-aluminum powder. The reactivity differences between nano-aluminum powder and micro-aluminum powder are compared in the thesis. It is clear that the reactivity of nano-aluminum powder is much higher than that of micro-aluminum powder in terms of ignition performance, combustion performance and reaction completeness, and it has a stronger influence on the detonation performance of mixed explosives and the combustion performance of propellants. Nano-aluminum powder is highly prone to oxidation, which seriously affects its application efficiency. In addition, when aluminum powder oxidizes or burns, a surface oxide layer will be formed, which hinders the continued reaction of internal aluminum powder. In addition, nano-aluminum powder may deteriorate the preparation process of explosives or propellants. To improve these shortcomings, appropriate coating or modification treatment is required. The application of nano-aluminum powder in mixed explosives can improve many properties of mixed explosives, such as detonation velocity, detonation heat, peak value of shock wave overpressure, etc. Applying nano-aluminum powder to propellants can significantly increase the burning rate and improve the properties of combustion products. It is pointed out that the high reactivity of nano-aluminum powder makes the preparation and storage of high-purity nano-aluminum powder extremely difficult. It is recommended to increase research on the preparation and storage technology of high-purity nano-aluminum powder. Full article
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20 pages, 9438 KB  
Article
Influence of Laser Shock Forming Parameters on Deformation Behavior and Dimensional Precision of Q355ME Carbon Steel Skin Components
by Mingming Ma, Xianrong Cao, Jun Chen, Weimin Huang, Ran Zhu and Boyu Sun
Coatings 2025, 15(9), 1044; https://doi.org/10.3390/coatings15091044 - 5 Sep 2025
Viewed by 1088
Abstract
A systematic investigation was conducted on the laser shock forming (LSF) process of carbon steel Q355ME sheets and practical skin components, focusing on the influence of absorption layer types, laser energy, and impact cycles on forming capacity and surface properties. Three kinds of [...] Read more.
A systematic investigation was conducted on the laser shock forming (LSF) process of carbon steel Q355ME sheets and practical skin components, focusing on the influence of absorption layer types, laser energy, and impact cycles on forming capacity and surface properties. Three kinds of absorbing layers were compared in the experiment: no absorbing layer, 0.1 mm aluminum foil and 0.12 mm black tape. The results show that when the black tape is used as the absorbing layer, the forming effect is the best, the arc height value reaches 2.63 mm, and the radius of curvature is 1066 mm. Using 0.1 mm thick black tape as the absorption layer and laser parameters of 10% overlap rate, 15 ns pulse width, 4 mm spot, and 1064 nm wavelength, the single impact of 13 J, 15 J, and 17 J, and one, two, and three impacts of 15 J energy were carried out on the plate. It was found that the increase in laser energy and impact times resulted in increases in deformation, surface roughness, microhardness, and residual stress of the plate. The surface work hardening phenomenon of Q355ME plate after laser shock slowed down the increase in these performance parameters. The experimental results show that the laser energy is linearly positively correlated with the residual stress in a certain energy range. Under the optimized laser process parameters, the forming error of the actual skin parts is controlled within ± 0.4 mm, the surface residual stress increases by 368.9%, and the surface microhardness increases by 10.4%. The ultra-high strain plastic deformation and grain refinement on the surface of the sheet were caused by multiple laser shock peenings, which confirmed that LSF technology can improve the formability of carbon steel skin parts and improve its surface properties. Full article
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14 pages, 6123 KB  
Article
Effects of Near-Infrared Diode Laser Irradiation on Pain Relief and Neuropeptide Markers During Experimental Tooth Movement in the Periodontal Ligament Tissues of Rats: A Pilot Study
by Kanako Okazaki, Ayaka Nakatani, Ryo Kunimatsu, Isamu Kado, Shuzo Sakata, Hirotaka Kiridoshi and Kotaro Tanimoto
Int. J. Mol. Sci. 2025, 26(15), 7404; https://doi.org/10.3390/ijms26157404 - 31 Jul 2025
Cited by 4 | Viewed by 1551
Abstract
Pain following orthodontic treatment is the chief complaint of patients undergoing this form of treatment. Although the use of diode lasers has been suggested for pain reduction, the mechanism of laser-induced analgesic effects remains unclear. Neuropeptides, such as substance P (SP) and calcitonin [...] Read more.
Pain following orthodontic treatment is the chief complaint of patients undergoing this form of treatment. Although the use of diode lasers has been suggested for pain reduction, the mechanism of laser-induced analgesic effects remains unclear. Neuropeptides, such as substance P (SP) and calcitonin gene-related peptide (CGRP), contribute to the transmission and maintenance of inflammatory pain. Heat shock protein (HSP) 70 plays a protective role against various stresses, including orthodontic forces. This study aimed to examine the effects of diode laser irradiation on neuropeptides and HSP 70 expression in periodontal tissues induced by experimental tooth movement (ETM). For inducing ETM for 24 h, 50 g of orthodontic force was applied using a nickel–titanium closed-coil spring to the upper left first molar and the incisors of 20 male Sprague Dawley rats (7 weeks old). The right side without ETM treatment was considered the untreated control group. In 10 rats, diode laser irradiation was performed on the buccal and palatal sides of the first molar for 90 s with a total energy of 100.8 J/cm2. A near-infrared (NIR) laser with a 808 nm wavelength, 7 W peak power, 560 W average power, and 20 ms pulse width was used for the experiment. We measured the number of facial groomings and vacuous chewing movements (VCMs) in the ETM and ETM + laser groups. Immunohistochemical staining of the periodontal tissue with SP, CGRP, and HSP 70 was performed. The number of facial grooming and VCM periods significantly decreased in the ETM + laser group compared to the ETM group. Moreover, the ETM + laser group demonstrated significant suppression of SP, CGRP, and HSP 70 expression. These results suggest that the diode laser demonstrated analgesic effects on ETM-induced pain by inhibiting SP and CGRP expression, and decreased HSP 70 expression shows alleviation of cell damage. Thus, although further validation is warranted for human applications, an NIR diode laser can be used for reducing pain and neuropeptide markers during orthodontic tooth movement. Full article
(This article belongs to the Special Issue Advances in Photobiomodulation Therapy)
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13 pages, 2262 KB  
Article
Application of Bioinspired Structural Ceramics with High-Temperature Electrical Insulation and High Adhesion in K-Type Coaxial Thermocouples
by Zhenyin Hai, Yue Chen, Zhixuan Su, Yemin Wang, Shigui Gong, Yihang Zhang, Shanmin Gao, Chengfei Zhang, Zhangquan Wang, Hongwei Ji, Chenyang Xue and Zhichun Liu
Materials 2025, 18(12), 2901; https://doi.org/10.3390/ma18122901 - 19 Jun 2025
Cited by 1 | Viewed by 1256
Abstract
Surface erosion of the coaxial thermocouple probe initiates continuous bridging of thermoelectric materials on the insulation layer surface, forming new temperature measurement junctions. This inherent ability to measure continuous self-erosion ensures the operational reliability of the coaxial thermocouples in high-temperature ablative environments. However, [...] Read more.
Surface erosion of the coaxial thermocouple probe initiates continuous bridging of thermoelectric materials on the insulation layer surface, forming new temperature measurement junctions. This inherent ability to measure continuous self-erosion ensures the operational reliability of the coaxial thermocouples in high-temperature ablative environments. However, the fabrication of a high-temperature electrical insulation layer and a high-adhesion insulating layer in the coaxial thermocouples remains a challenge. Inspired by calcium carbonate/oxalate crystals in jujube leaves that strengthen the leaves, a bioinspired structural ceramic (BSC) mimicking these needle-like crystals is designed. This BSC demonstrates excellent high-temperature insulation (with insulation impedance of 2.55 kΩ at 1210 °C) and adhesion strength (35.3 Newtons). The BSC is successfully used as the insulating layer in a K-type coaxial thermocouple. The generation rules for surface junctions are systematically studied, revealing that stable and reliable measurement junctions can be created when the sandpaper grit does not exceed 600#. Static test results show that the K-type coaxial thermocouple ranges from 200 °C to 1200 °C with an accuracy of 1.1%, a drift rate better than 0.0137%/h, and hysteresis better than 0.81%. Dynamic test results show that the response time is 1.08 ms. The K-type coaxial thermocouple can withstand a high-temperature flame impact for 300 s at 1200 °C, as well as over forty cycles of high-power laser thermal shock, while maintaining good response characteristics. Therefore, the K-type coaxial thermocouple designed in this study provides an ideal solution for long-term temperature monitoring of the thermal components of aerospace engines under extremely high-temperature, high-speed, and strong thermal shock conditions. Full article
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20 pages, 5550 KB  
Article
The Key Process Factors in Prestressed Laser Peen Forming and the Design of Parameters Through an Artificial Neural Network
by Jiayang Lyu, Yongjun Wang, Zhiwei Wang and Junbiao Wang
Metals 2025, 15(4), 445; https://doi.org/10.3390/met15040445 - 16 Apr 2025
Viewed by 1006
Abstract
This research investigated the influences of some key factors in the prestressed laser peen forming (PLPF) process, namely, the plate thickness, the coverage ratio, and the prestress, on the deformation of 2024-T351 rectangular plates through experiments and numerical simulations. In the experiments, laser [...] Read more.
This research investigated the influences of some key factors in the prestressed laser peen forming (PLPF) process, namely, the plate thickness, the coverage ratio, and the prestress, on the deformation of 2024-T351 rectangular plates through experiments and numerical simulations. In the experiments, laser parameters, such as the laser energy and spot size, were kept unchanged, and prestress was applied through a piece of self-developed, four-point-bending equipment. The curvature radius of the samples was measured through a digital radius gauge. A corresponding finite element analysis (FEA) model of PLPF was also established to simulate the full procedure of the PLPF, including prebending, laser shock peening, and spring back. Based on the PLPF experimental results, an artificial neural network (ANN) was trained to help to design the process parameters, including the coverage ratio and the amount of prebending, according to the plate thickness and the target curvature radius. By adding a penalty term to the loss function, the amount of prebending (AOP) can be reduced as much as possible. The validation of the ANN was confirmed by three other PLPF experiments. Full article
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16 pages, 1975 KB  
Article
SWEEPS-Assisted Antibacterial Photodynamic Therapy Against Dual-Species Biofilms in Mandibular Molars: An In Vitro Study
by Pargol Guity, Shima Afrasiabi, Ali Shahi Ardakani, Stefano Benedicenti, Antonio Signore, Nasim Chiniforush and Kiumars Nazari Moghaddam
Pharmaceuticals 2025, 18(4), 558; https://doi.org/10.3390/ph18040558 - 10 Apr 2025
Cited by 3 | Viewed by 1692
Abstract
Objectives: The synergistic effect of shock wave-enhanced emission photoacoustic streaming (SWEEPS) and antimicrobial photodynamic therapy (aPDT) in mandibular molar root canal disinfection remains underexplored, particularly against dual-species biofilms that better simulate clinical conditions. This study evaluates their combined antimicrobial efficacy against Enterococcus faecalis [...] Read more.
Objectives: The synergistic effect of shock wave-enhanced emission photoacoustic streaming (SWEEPS) and antimicrobial photodynamic therapy (aPDT) in mandibular molar root canal disinfection remains underexplored, particularly against dual-species biofilms that better simulate clinical conditions. This study evaluates their combined antimicrobial efficacy against Enterococcus faecalis and Candida albicans biofilms and assesses potential tooth discoloration caused by riboflavin and nano-curcumin. Materials and Methods: The mesiobuccal canals of 57 extracted mandibular molars were inoculated with E. faecalis and C. albicans biofilms. The antimicrobial effects were assessed using riboflavin or nano-curcumin with a 450 nm diode laser (BDL), SWEEPS, or their combinations, compared to 5.25% NaOCl (positive control) and saline (negative control). Biofilm reduction was quantified by colony-forming units (CFUs/mL), and discoloration was evaluated using the ΔE metric in the CIE L*a*b* color space. Results: Both microorganisms showed a significant decrease in colony numbers in all experimental groups compared to the negative control (p < 0.001), except for E. faecalis, where no significant difference was observed between the riboflavin/nano-curcumin groups and the negative control. Combining riboflavin or nano-curcumin with SWEEPS or BDL significantly enhanced antimicrobial efficacy compared to individual treatments (p < 0.001). The combined photodynamic therapy and SWEEPS groups showed the lowest colony counts. The ΔE values were, on average, 1.81 for riboflavin and 1.09 for nano-curcumin. Conclusions: The combination of SWEEPS and aPDT effectively reduces E. faecalis and C. albicans biofilms in molars, supporting its potential as an adjunct in endodontic disinfection. Minimal discoloration further highlights its clinical applicability. Full article
(This article belongs to the Section Natural Products)
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20 pages, 5723 KB  
Article
Influence of Overloading on Residual Stress Distribution in Surface-Treated Wire Arc Additive-Manufactured Steel Specimens
by Fraser O’Neill, Emmet McLaughlin, Anna Ermakova and Ali Mehmanparast
Materials 2025, 18(7), 1551; https://doi.org/10.3390/ma18071551 - 29 Mar 2025
Cited by 7 | Viewed by 1772
Abstract
Many countries around the world are in a race against time to decarbonise their energy systems. One of the avenues being explored in detail is Offshore Renewable Energy (ORE), with technologies such as wind, wave, and tidal. All of these technologies are in [...] Read more.
Many countries around the world are in a race against time to decarbonise their energy systems. One of the avenues being explored in detail is Offshore Renewable Energy (ORE), with technologies such as wind, wave, and tidal. All of these technologies are in their infancy within the marine environment and required heavy Research and Development (R&D) to make them commercially viable. With so much demand for these industries, the supply chain is heavily constrained. A solution that has shown great potential to alleviate the pressure on the supply chain is the use of Wire Arc Additive Manufacturing (WAAM) for the use of onsite repair or manufacture for components. This is due to its ability to produce large-scale parts, with low emissions and at a lower cost than other Additive Manufacturing (AM) processes. The opportunity to use this technology could result in shorter downtimes and lead to a reduction in the Levelised Cost of Energy (LCOE). However, knowing that offshore structures are subject to cyclic loading conditions during their operational lifespan, fatigue properties of new materials and manufacturing processes must be well documented and studied to avoid any catastrophic failures. An issue often seen with WAAM is the presence of residual stresses. This study looks at fatigue cracking on Compact Tension C(T) specimens that have undergone laser shock peening and rolling, surface treatment processes that form compressive residual stresses at the surface of the material. In this study, the influence of fatigue overloading on the residual stress distribution in surface-treated WAAM specimens is evaluated and the effectiveness of the post-processing techniques on the subsequent fatigue behaviour is explored. Full article
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