Search Results (85)

Al-Mg-Si (6XXX) series aluminum alloys are widely applied in aerospace and transportation industries. However, exploring how varying compositions affect alloy properties and deformation mechanisms is often time-consuming and labor-intensive due to the complexity of the multicomponent composition space and the diversity of processing and heat treatments. This study, inspired by the Materials Genome Initiative, employs high-throughput experimentation—specifically the kinetic diffusion multiple (KDM) method—to systematically investigate how the pop-in effect, indentation size effect (ISE), and creep behavior vary with the composition of Al-Mg-Si alloys at room temperature. To this end, a 6016/Al-3Si/Al-1.2Mg/Al KDM material was designed and fabricated. After diffusion annealing at 530 °C for 72 h, two junction areas were formed with compositional and microstructural gradients extending over more than one thousand micrometers. Subsequent solution treatment (530 °C for 30 min) and artificial aging (185 °C for 20 min) were applied to simulate industrial processing conditions. Comprehensive characterization using electron probe microanalysis (EPMA), nanoindentation with continuous stiffness measurement (CSM), and nanoindentation creep tests across these gradient regions revealed key insights. The results show that increasing Mg and Si content progressively suppresses the pop-in effect. When the alloy composition exceeds 1.0 wt.%, the pop-in events are nearly eliminated due to strong interactions between solute atoms and mobile dislocations. In addition, adjustments in the ISE enabled rapid evaluation of the strengthening contributions from Mg and Si in the microscale compositional array, demonstrating that the optimum strengthening occurs when the Mg-to-Si atomic ratio is approximately 1 under a fixed total alloy content. Furthermore, analysis of the creep stress exponent and activation volume indicated that dislocation motion is the dominant creep mechanism. Overall, this enhanced KDM method proves to be an effective conceptual tool for accelerating the study of composition–deformation relationships in Al-Mg-Si alloys. Full article

This work aims to reveal the full-field strain evolution characteristics and failure mechanisms of anisotropic coal samples under creep loading. A series of compression tests combined with digital image correlation (DIC) monitoring were employed to characterize the strain evolution process of coal specimens with bedding angles of 0°, 30°, 60°, and 90°. Testing results show that the peak strength, peak strain, and the creep loading stage of coal are significantly influenced by the bedding angle. The peak strength initially decreases and then increases as the bedding angle increases. In addition, the creep failure of coal manifests as a process of instantaneous deformation, decelerating creep, steady-state creep, accelerating creep, and failure. Under graded creep loading conditions, coal specimens exhibit distinct creep characteristics at high stress levels. Moreover, the bedding angle significantly influences the strain field evolution of the coal samples. Finally, for coal specimens with bedding angles of 0° and 90°, the final macroscopic fracture pattern upon failure is characterized by longitudinal tensile splitting. In contrast, coal samples with bedding angles of 30° and 60° tend to exhibit failure along the bedding interfaces, forming tensile-shear fractures. The results of this study will provide theoretical guidance for the prevention, early warning, and safety management of coal mine disasters. Full article

This study conducted uniaxial creep tests on coal samples under both natural and water-saturated conditions for durations of about 180 days per sample to study the stability of coal pillar dams of the Daliuta Coal Mine underground reservoir. Combined with synchronized acoustic emission (AE) monitoring, the research systematically revealed the time-dependent deformation mechanisms and damage evolution laws of coal under prolonged water immersion and natural conditions. The results indicate that water-immersed coal exhibits a unique negative creep phenomenon at the initial stage, with the strain rate down to −0.00086%/d, attributed to non-uniform pore compaction and elastic rebound effects. During the steady-state creep phase, the creep rates under water-immersed and natural conditions were comparable. However, water immersion led to an 11.4% attenuation in elastic modulus, decreasing from 2300 MPa to 2037 MPa. Water immersion would also suppress AE activity, leading to the average daily AE events of 128, which is only 25% of that under natural conditions. In the accelerating creep stage, the AE event rate surged abruptly, validating its potential as an early warning indicator for coal pillar instability. Based on the identified long-term strength of the coal sample, it is recommended to maintain operational loads below the threshold of 9 MPa. This research provides crucial theoretical foundations and experimental data for optimizing the design and safety monitoring of coal pillar dams in CMURs. Full article

Aluminum alloys based on the eutectic Al–Ni system are a promising class of lightweight materials for applications at elevated temperatures owing to the thermal stability of the eutectic Al₃Ni phase. In this study, the eutectic Al–Ni alloy was modified by the addition of 0.6 wt.% Zr to enhance the α_Al matrix by precipitation strengthening. The alloys were cast and subjected to T5 heat treatment followed by long-term isothermal aging at 350 °C. A comprehensive study was carried out to evaluate the evolution of microstructure, microhardness and mechanical performance over time. The formation of fine, coherent L1₂-Al₃Zr precipitates contributed to significant strengthening, as reflected by a ~60% increase in microhardness and an approximately twofold improvement in room temperature (RT) yield strength. A TEM analysis of the L1₂-Al₃Zr precipitates showed relatively good thermal stability after 30 days. Despite the improved mechanical properties at room temperature, the alloy did not retain this improvement when tested at 300 °C. Nevertheless, these results provide a comprehensive insight into the aging and thermal stability of Al–Ni–Zr alloys. Full article

Electroless nickel deposition (ELD) on polymer substrates enables the fabrication of flexible, conductive fibres for wearable and functional textiles. However, achieving uniform, low-defect coatings on synthetic fibres such as nylon-6,6 remains challenging due to their chemical inertness, hydrophobicity, and poor interfacial compatibility with metal coatings. This study presents a solvent-assisted approach using dimethyl sulfoxide (DMSO) in a conventional aqueous ELD bath to control both polymer–metal interfacial chemistry and nickel coating microstructure. The modified surface supports dense catalytic sites, triggering spatially uniform Ni nucleation. The combination of scanning electron microscopy and transmission electron microscopy confirms the difference in coarse grains with fully aqueous baths to a nanocrystalline shell with DMSO-modified baths. This refined microstructure relieves residual stress and anchors firmly to the swollen polymer, delivering +7 °C higher onset decomposition temperature and 45% lower creep strain at 50 °C compared with aqueous controls. The fabric strain sensor fabricated by 1 wt.% DMSO-modified ELD shows a remarkable sensitivity against strain, demonstrating a 1400% resistance change under 200% stain. Electrochemical impedance and polarisation tests confirm a two-fold rise in charge transfer resistance and negligible corrosion current drift after accelerated ageing. By clarifying how a polar aprotic co-solvent couples polymer swelling with metal growth kinetics, the study introduces a scalable strategy for tuning polymer–metal interfaces and advances solvent-assisted ELD as a route to mechanically robust, thermally stable, and corrosion-resistant conductive textiles. Full article

With the further implementation and development of the Western Development Strategy, studying the mechanical behavior and deformation characteristics of deep-buried tunnels in layered hard rock under high ground stress conditions holds considerable engineering significance. To study the mechanical properties and long-term deformation and failure characteristics of different bedding stratified rocks, this research employed an MTS815 electro-hydraulic servo rock testing system and a French TOP rheometer. Triaxial compression tests, rheological property tests, and long-term cyclic and unloading tests were conducted on shale samples under varying confining pressures and bedding angles. The results indicate that (1) under triaxial compression, shale demonstrates pronounced anisotropic behavior. When the confining pressure is constant, the peak strength of the rock sample exhibits a “U”-shaped variation with the bedding angle (its minimum value at 60°). For a fixed bedding angle, the peak strength of the rock sample progressively increases as the confining pressure rises. (2) The mode of shale failure varies with the angle: at 0°, shale exhibits conjugate shear failure; at 30°, shear slip failure along the bedding is controlled by the bedding weak plane; at 60° and 90°, failure occurs through the bedding. (3) During the creep process of layered shale, brittle failure characteristics are evident, with microcracks within the sample gradually failing at stress concentration points. The decelerated and stable creep stages are prominent; while the accelerated creep stage is less noticeable, the creep rate increases with increasing stress level. (4) Under low confining pressure, the peak strength during cyclic loading and unloading creep processes is lower than that of conventional triaxial tests when the bedding plane dip angles are 0° and 30°, which is the opposite at 60° and 90°. (5) In the cyclic loading and unloading process, Poisson’s ratio gradually increases, whereas the elastic modulus, shear modulus, and bulk modulus gradually decrease. Full article

This study investigates the elevated-temperature mechanical and viscoelastic properties of a PDMS–silica-based superhydrophobic nanocomposite coating using nanoindentation and a nano-dynamic mechanical analysis over a temperature range of 24 °C to 160 °C. The nanoindentation load–displacement curves exhibited consistent hysteresis, indicating a stable energy dissipation across the temperature range. Creep tests revealed an increased displacement and accelerated deformation at elevated temperatures, displaying a two-stage creep profile characterized by rapid primary and steady-state secondary creep. The hardness decreased with the creep time, while the strain rate sensitivity remained relatively stable, suggesting consistent deformation mechanisms. A time-dependent creep model incorporating linear and logarithmic terms accurately captured the experimental data. The nano-dynamic mechanical analysis results showed a decrease in the storage modulus with depth, while the loss modulus and tan δ peaked at shallow depths. These findings are crucial for the evaluation and design of superhydrophobic nanocomposite coatings. Full article

Different temperatures and continuous loads have significant effects on the long-term performance of asphalt concrete facings. The effects of temperature and stress on creep strain and creep rate were analyzed by designing a bending creep test of impermeable asphalt concrete under different temperatures and stresses. Based on the test data, a time–temperature–stress-dependent creep constitutive model was constructed to predict the long-term creep behavior of asphalt concrete at low temperature. The results showed that the creep behavior of asphalt concrete showed significant temperature and stress dependence. The creep behavior accelerated as the temperature or stress increased, especially under high-stress conditions, indicating obvious nonlinear characteristics. Under the condition of 0.2376 MPa, when the temperature increased from 0 °C to 20 °C, the strain at the creep time of 9330 s nearly increased by 24 times. Under 0 °C, the loading stress increased from 0.2376 MPa to 1.3176 MPa, and the strain nearly increased by six times at a creep time of 880 s. The creep strain is expected to increase to 8% after 8 years at −15 °C and 0.2376 MPa. The results can provide a scientific basis for engineering practice and significant implications for designing and maintaining asphalt concrete facings. Full article

Underground engineering rock masses are significantly affected by stress redistribution induced by mining or adjacent engineering disturbances, leading to initial damage accumulation in coal-rock masses. Under sustained geostress, these masses exhibit pronounced time-dependent creep behavior, posing serious threats to long-term engineering stability. Dynamic loading effects triggered by adjacent mining activities (manifested as medium strain-rate loading) further exacerbate damage evolution and significantly influence creep characteristics. In this study, coal samples with identical initial damage were prepared, and graded loading creep tests were conducted at rates of 0.005 mm·s⁻¹ (50 microstrains·s⁻¹), 0.01 mm·s⁻¹ (100 microstrains·s⁻¹), 0.05 mm·s⁻¹ (500 microstrains·s⁻¹), and 0.1 mm·s⁻¹ (1000 microstrains·s⁻¹) to systematically analyze the coupled effects of loading rate on creep behavior. Experimental results demonstrate that increased loading rates markedly shorten creep duration, with damage rates during the acceleration phase showing nonlinear surges (e.g., abrupt instability at 0.1 mm·s⁻¹ (1000 microstrains·s⁻¹)). Based on experimental data, an integer-order viscoelastic-plastic creep model incorporating stress-dependent viscosity coefficients and damage correlation functions was developed, fully characterizing four behaviors stages: instantaneous deformation, deceleration, steady-state, and accelerated creep. Optimized via the Levenberg–Marquardt algorithm, the model achieved correlation coefficients exceeding 0.96, validating its accuracy. This model clarifies the impact mechanisms of loading rates on the long-term mechanical behavior of initially damaged coal samples, providing theoretical support for stability assessment and hazard prevention in underground engineering. Full article

The moisture content is closely related to the shear creep deformation behavior of soft rock, and the linear creep deformation behavior of soft rock can be described by the classical Nishihara model. However, its accuracy in describing accelerated nonlinear creep characteristics and the effects of moisture content still needs to be improved. The innovation of this paper is to propose an improved Nishihara model that can describe the whole creep process of shale with different moisture content. The model uses a strain-triggered nonlinear sticky pot to describe the process of accelerated creep of rock, and proposes a damage factor to reflect the effect of moisture content on the creep characteristics of rock. The relationship between the moisture content and damage factor is an exponential function, and the damage factor and related model parameters are determined by the shear creep test results under moisture conditions (0%, 0.46%, 0.87%, 1.24%). The shear creep tests were carried out by a self-developed rock shear apparatus. The experimental results show that the shear creep rate decreases first and then increases. The higher the moisture content of shale, the greater the initial shear displacement and stable creep displacement, and the longer it takes to enter the stable creep stage. The improved Nishihara model proposed in this paper can accurately fit the shear creep curves of four groups of shale samples with different moisture contents, and the correlation coefficients all reach 0.99. The fitting effect is better than that of the traditional model, which has good accuracy and practicability. Full article

Nanoindentation has been used to characterize the mechanical and creep properties of various materials. However, research on the viscoelastic and creep properties of superhydrophobic surfaces remains limited. In this study, a superhydrophobic coating was developed and its corrosion resistance was evaluated initially. Electrochemical impedance spectroscopy (EIS) results quantitatively confirm the enhanced anti-corrosion performance of the superhydrophobic coating. Subsequently, this study investigates the creep, hardness, strain rate sensitivity, and viscoelastic behavior of the superhydrophobic surface at the nanoscale before and after accelerated corrosion exposure. Our findings reveal that during the creep tests, the logarithmic values of creep strain rate and stress exhibited a good linear relationship. Additionally, the surface retains its key viscoelastic properties (hardness, storage modulus, loss modulus, and tan δ) even after exposure to corrosion. These results highlight the surface’s robustness under corrosive conditions, a crucial factor for applications requiring both mechanical integrity and environmental resilience. Full article

In tunnel construction in western China, a vast amount of carbonaceous slate is encountered. High in situ stress and foliation structures cause the rock mass to exhibit pronounced anisotropic creep, readily inducing a series of engineering disasters like collapses and lining cracks. Investigating the anisotropic time-dependent characteristics of carbonaceous slate is beneficial to the long-term stability of tunnel construction and operation. In view of this, carbonaceous slate specimens with different angles, β, between the foliation plane and loading direction were studied using a graded loading method through uniaxial compression creep tests. The results show that the instantaneous axial strain, ε_i, the axial creep strain, ε_c, the duration time of decelerating creep stage, t_d, and the steady creep strain rate, ${\dot{\epsilon }}_s$, increased with the rise in the loading ratio, k. Their variations followed a power law relationship, with the R² (Coefficient of Determination) values all exceeding 0.95. The value of ${\dot{\epsilon }}_s$ was observed to be less than 1.5 × 10⁻⁴/h when β < 45°, while it was found to exceed 1.5 × 10⁻⁴/h in the cases of $\beta \ge 45°$. The long-term strength, σ_L, of carbonaceous slate showed a U-shaped pattern with the variation in β. The maximum σ_L occurred at β = 90° and the minimum was observed at β = 15°. A fractional nonlinear creep model (FNC model) was developed. The sensitivity analysis reveals that the larger the fractional order n is, the t_d and ${\dot{\epsilon }}_s$ increase. η₂ and E₂ primarily affect the decelerated creep stage, while the ${\dot{\epsilon }}_s$ exhibits a rapid increase with the rise of η₁. To further validate the FNC model, a comparison is made with the traditional Nishihara model. The R² of the FNC model is larger than 0.965, which is higher than that of the Nishihara model (R² ≤ 0.911). The FNC model can effectively cope with the impact of the sudden increase in strain and well describe the characteristics of the decelerating, steady-state, and accelerating creep stages at any stress level and any angle. The results provide a reference for the study of the creep mechanism of layered rocks. Full article

Calcareous sand has been widely used as a construction material for offshore projects; however, the problem of foundation settlement caused by particle crushing cannot be ignored. Although many methods for reinforcing calcareous sands have been proposed, they are difficult to apply on-site. In this study, a permeable polyurethane polymer adhesive (PPA) was used to reinforce calcareous sands, and its mechanical properties after reinforcement were investigated through compression creep, direct shear, and triaxial shear tests. The reinforcement mechanism was analyzed using optical microscopy, CT tomography, and mercury intrusion porosimetry. The experimental results indicate that there is a critical time during the compression creep process. Once the critical time is surpassed, creep accelerates again, causing failure of the traditional Burgers and Murayama models. The direct shear strength of the fiber- and geogrid-reinforced calcareous sand reinforced by PPA was approximately nine times greater than that without PPA. The influence of normal stress was not significant when the moisture content was less than 10%, but when the moisture content was more than 10%, the shear strength increased with an increase in vertical normal stress. Strain-softening features can be observed in triaxial shear tests under conditions of low confining pressure, and the relationship between the deviatoric stress and strain can be described using the Duncan–Chang model before softening occurs. The moisture content also has a significant influence on the peak strength and cohesive force but has little influence on the internal friction angle and Poisson’s ratio. This influence is caused by the different PPA structures among the particles. The higher the moisture content, the greater the number of pores left after grouting PPA. Full article

In the longstanding development of hydrate-bearing sediment (HBS) reservoirs, slow and permanent deformation of the formation will occur under the influence of stress, which endangers the safety of hydrate development projects. This paper takes hydrate-bearing sandy sediment (HBSS) as the research object and conducts triaxial compression creep tests at different saturation degrees (20%, 30%, and 40%). The results show that the hydrate-containing sandy sediments have strong creep characteristics, and accelerated creep phenomenon will occur under the long-term action of high stress. The longstanding destructive power of the specimen progressively raises with the increase in hydrate saturation, but the difference in the triaxial strength of the specimen progressively increases. This indicates that the damage to the hydrate structure during long-term loading is the main factor causing the strength decrease. Further, a new nonlinear creep constitutive model was developed by using the nonlinear Burgers model in series with the fractional-order viscoplastic body model, which can well describe the creep properties of HBSS at different saturation levels. Full article

The water environment greatly affects the creep deformation of recycled aggregate concrete (RAC). Hence, a humidity–stress–damage coupling numerical model was used for investigating the time-dependent deformation of RAC in the water environment in this study. Firstly, uniaxial compression and water absorption tests were performed to determine the calculation parameters of the creep numerical simulation of RAC in a water environment. Experimental results indicate that the elastic modulus and compressive strength drop as the water content increases. Then, the time-dependent deformation of RAC in a water environment was studied using a numerical simulation test of compressive creep when multiple stress levels were applied, and the critical stress for accelerated creep and the long-term strength of RAC were obtained. Finally, the influence of confining pressures on the long-term deformation of RAC in a water environment was discussed. When there is no confining pressure, the long-term strength of RAC is 23.53 MPa. However, when a confining pressure of 3.921 MPa is loaded onto RAC, the long-term strength of RAC is 47.052 MPa, which increases by 100%. Increasing confining pressures has an obvious effect on ensuring the long-term stable application of RAC in a water environment. Compared with the creep test, the method adopted in this study saves time and money and provides the theoretical basis for evaluating the time-dependent deformation of RAC in a water environment. Full article