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Article

Additive Manufacturing of Variable Density Lenses for Radio Frequency Communications in X-Band

1
Instituto de Telecomunicaciones y Aplicaciones Multimedia, Universitat Politecnica de Valencia, Avda. de los Naranjos s/n, E-46022 Valencia, Spain
2
Innovative Materials and Manufacturing Area, Aiju Instituto Tecnológico de Producto Infantil y Ocio, Avda. de la Industria, 23, E-03440 Alicante, Spain
3
Institute of Information and Communication Technologies (ITACA), Universitat Politecnica de Valencia, Avda. de los Naranjos s/n, E-46022 Valencia, Spain
4
Institute of Computer and Communication Technology, University of Applied Sciences-TH Köln, Betzdorfer Straße 2, 50679 Köln, Germany
*
Author to whom correspondence should be addressed.
J. Manuf. Mater. Process. 2025, 9(7), 238; https://doi.org/10.3390/jmmp9070238
Submission received: 9 May 2025 / Revised: 30 June 2025 / Accepted: 8 July 2025 / Published: 11 July 2025
(This article belongs to the Special Issue Recent Advances in Optimization of Additive Manufacturing Processes)

Abstract

This paper presents three realizations of a complete set with a horn antenna and a focusing Gradient Index (GRIN) lens in X-band. The set was specifically designed for advancing additive manufacturing (AM) of polymers with different materials and techniques. The set has three constituent parts: a horn antenna, a support, and a lens. The horn antenna is the active element and must be electrically conductive; it was manufactured with Rigid10K acrylic resin and subsequently metallized using an electroless process. The support needed to be light, robust, and electrically transparent, so that Polyamide 11 (PA11) was used. The lens realization was intended for a dielectric material whose permittivity varies with its density. Therefore, the dielectric permittivity and loss tangent of different polymeric materials used in AM at 2.45, 6.25, and 24.5 GHz were measured. In addition, stochastic and gyroid mesh structures have been studied. These structures allow for printing a volume that presents porosity, enabling control over material density. Measuring the dielectric characteristics of each material with each density enables the establishment of graphs that relate them. The sets were then manufactured, and their frequency response and radiation diagram were measured, showing excellent results when compared with the literature.

Graphical Abstract

1. Introduction

In recent years, additive manufacturing (AM) has emerged as a transformative technology with profound implications across various industries, including aerospace, healthcare, automotive, and beyond [1]. The unique capabilities of AM—particularly in terms of material diversity, precision, and design freedom—have opened the way for novel applications in the field of communication systems. The communications industry increasingly demands higher frequency devices capable of handling the complex requirements of modern wireless systems [2]. Additive manufacturing offers several advantages in meeting these demands. First, it enables rapid prototyping and iterative testing, allowing engineers to optimize designs in shorter time frames [3]. This rapid design-to-manufacture process is essential for the fast-paced communications sector, where technologies are continuously evolving to support new standards like 5G and 6G [4]. Secondly, AM facilitates the production of highly intricate structures that are difficult to machine or mold. For example, horn antennas and GRIN lenses with complex internal geometries can be manufactured as single components, reducing the need for assembly and the potential for alignment errors, which are critical factors in RF applications [5].
Antenna design has evolved significantly in response to the ever-growing demand for high-performance communication systems. Traditionally, antennas are fabricated from metals such as copper or aluminum, chosen for their high electrical conductivity and robustness in high-frequency applications. The horn antenna, a staple in RF communications, is particularly valued for its simplicity, directivity, and broadband capabilities [6]. With the advent of AM, researchers have explored new methods to manufacture these antennas, often focusing on materials and processes that allow for high precision and reduced weight. Metallic coatings can be applied to 3D-printed polymer structures to achieve the necessary conductivity [7]. Shen et al. [8] offers a more versatile manufacturing process for complex designs. This approach not only reduces the weight of the component but also lowers material costs by limiting the use of expensive metals to surface coatings, customizing antenna properties without the constraints of conventional subtractive manufacturing. By enabling the use of composite polymer-based materials, AM also enhances the thermal management of devices, which is especially important for high-power applications in the communications field [9].
Gradient Index (GRIN) lenses are widely used in communications to manipulate the propagation of electromagnetic waves. By gradually varying the refractive index of the lens material, GRIN lenses focus or direct RF energy in a controlled manner, enhancing the performance of antennas in terms of gain and beam shaping [10]. Traditionally, these lenses are made from homogenous dielectric materials, with their refractive index modified by altering their geometry [11]. This often requires a labor-intensive shaping of dielectric materials to achieve the desired index gradient, which limits design flexibility and increases production time. However, AM provides the ability to adjust the refractive index more flexibly by changing the density or porosity of the polymeric material within a single component during fabrication. This method also allows for the integration of stochastic and gyroid mesh structures, which offers an additional degree of control over material properties. By adjusting the porosity of the material, designers can achieve specific permittivity values across the lens profile, as in [12,13]. This capability opens up new possibilities in lens design, enabling devices that are both lightweight and capable of complex wavefront shaping.
There are several AM techniques that are particularly suited to the polymer-based fabrication of RF components, for instance, Vat Photopolymerization (VPP) and Powder Bed Fusion (PBF). VPP, which uses ultraviolet light to selectively cure photopolymer resins, is valued for its high resolution and is often used to fabricate intricate components such as waveguides and lenses. In contrast, PBF enables the use of materials like polyamide polymer, which is lightweight and offers good mechanical stability and electrical transparency. As detailed by [14], using PBF to create support structures in RF devices enables engineers to maintain both structural integrity and desired electromagnetic transparency. The integration of these AM techniques has driven substantial advancements in the manufacture of complex antenna and lens structures, especially when complemented with material innovations like electroless metallization [15,16,17].
This article outlines the research gap that existed between integration of different additive manufacturing techniques (VPP, PBF), electroless metallization, and used materials (resin or nylon polymer) in developing radio frequency (RF) communication devices (previous measurements of EM properties of the material samples are accomplished in Section 2.2.4. Specifically, it focuses on the development of a horn antenna and a Gradient Index (GRIN) lens set, designed for operation in the X-band frequency range, making use of the capabilities of AM of polymeric materials. The work begins with measuring the dielectric permittivity and loss tangent of different polymeric materials at frequencies of 2.45 (WiFi at 2.4 GHz, 3G/4G mobile bands), 6.25 (WiFi at 5 GHz, 5G mobile bands, satellite communications), and 24.5 GHz (6G mobile bands, satellite communications). Furthermore, samples of stochastic and gyroid mesh structures of the different materials were measured, and the empirical relationships between material density and electromagnetic properties were established.
Then, the lens set was designed. The design of the horn antenna, lens, and support structure was tailored to their specific functional requirements, both electromagnetic and mechanical. Three realizations of the GRIN lens were produced, using the results of the characterization of polymers whose dielectric properties vary with density, allowing for a radial permittivity gradient that enhances its focusing capabilities.
The sets were then manufactured. The horn antenna, designed to be conductive, was fabricated using VPP with an acrylic resin with silica load and subsequently metallized using an electroless plating process. This combination ensures that the antenna meets the necessary conductivity specifications while benefiting from the lightweight and cost-effective nature of the polymer base. The support structure was fabricated using PBF with polyamide polymer, chosen for its mechanical stability and electrical transparency. This allows the support to maintain the structural integrity of the device without interfering with the antenna’s radiation pattern. Finally, the three GRIN lenses were manufactured using different acrylic resins and meshes with different densities radially distributed.
The final assembled devices were then evaluated for frequency response and radiation pattern, yielding results that aligned well with theoretical predictions and those of comparable studies in the existing literature.

2. Dielectric Permittivity Measurements

A material that can store energy when an external electric field is applied is known as a dielectric. Since the advent of modern communications, dielectric materials have been included in antennas and RF components; thus, the accurate measurement of their properties is crucial. The main parameter of dielectric properties is permittivity ϵ and is expressed as in Equation (1) where ϵ 0 is called the permittivity of vacuum and ϵ r is the relative permittivity of the material.
ϵ = ϵ 0 ϵ r = ϵ 0 ( ϵ r j ϵ r )
where the permittivity of vacuum is ϵ 0 = 8.854 × 10 12 F/m. The relative permittivity ϵ r is a complex number including the real part ϵ r , which shows how much energy from an external electric field is stored. Usually, the term dielectric constant relates only to this real part, while the imaginary part ϵ r represents how dissipative or lossy this material is to an external electric field. The ratio of the energy lost to the energy stored is called the loss tangent or tan δ , see Equation (2).
tan δ = ϵ r ϵ r
The characterization of these two parameters in new materials is essential for the proper design of devices that make use of them.

2.1. Microwave Characterization Methods

Methods for characterizing the samples can be divided into non-resonant and resonant categories. In non-resonant methods, material properties are determined using reflection or reflection/transmission data in a transmission line. This data is collected via a vector network analyzer (VNA) in a wide frequency range. Transmission/reflection methods require both reflection and transmission data (scattering parameters S 11 and S 21 , respectively) to determine material properties, whereas reflection methods only need reflection data ( S 11 ). Various transmission lines, including coaxial lines, hollow metallic waveguides, dielectric waveguides, and free space, can be utilized in these methods.
Resonant methods offer greater accuracy and sensitivity compared to non-resonant methods [18], but they are restricted to one or a few discrete frequencies. These methods are divided into the methods of material under test (MUT) as a resonator and the resonant perturbation methods. The main difference between them is that in the resonant perturbation method, the properties of the MUT are determined by observing changes in the properties of a resonant device with and without the MUT, whereas the MUT as a resonator method relies directly on how an MUT behaves as a resonator with its resonant properties. In resonant methods, the dimensions of the MUT are crucial since they impact the measurement, so accurate dimensional control is required.
Three measurement methods were used in this work to characterize the AM polymeric material samples at a narrow band; all of them are considered resonant perturbation methods: Resonant Coaxial Bireentrant Microwave Cavity at 2.45 GHz, Split-Cylinder Resonant Cavity at 6.25 GHz, and Rectangular Waveguide at 24.5 GHz.

2.1.1. Resonant Coaxial Bireentrant Microwave Cavity

In the method described in [19], the measurements are based on how the resonant frequency and the quality factor of a resonant cavity change when a cylindrical sample of MUT is introduced into the cavity. The Single-post coaxial reentrant cavity is constructed using a coaxial transmission line, where a rod sample is introduced in a gap created in the inner conductor, Figure 1a. This cavity features a partially dielectric-filled gap and an endplate. To ensure alignment, a cylindrical tube housing the cylindrical sample of MUT is inserted through a hole in the endplate, see Figure 1b. It is then further inserted into the coaxial center conductor, which also serves to maintain concentricity. In order to perform the measurements a stand-alone microwave equipment, Dielectric Kit for Vials (DKV) from the Institute of Information and Communication Technologies (ITACA) settled in Valencia, Spain, which consisted of a Single-Post Reentrant Cavity for measuring cylindrical samples at resonance frequency of 2.45 GHz (mode T E 111 is excited in the cavity without sample), as shown in Figure 2a, and a VNA are used. Measuring the reflection coefficient ( S 11 ) of the cavity with and without the sample enables the extraction of the dielectric constant and the loss tangent. The procedure is described in detail at [20], where the circuital analysis of dielectric-loaded cylindrical waveguides and cavities is performed. The measurement equipment is detailed in [21].

2.1.2. Split-Cylinder Resonant Cavity

The split-cylinder resonator is a nondestructive technique used to measure the permittivity and loss tangent of low-loss dielectric substrates. Initially proposed by Kent [22], this method utilizes a circular-cylindrical cavity divided into two halves. A planar dielectric sample is positioned in the gap between the two shorted cylindrical waveguide sections. To excite the family of resonant modes, coupling loops in the cylindrical waveguide sections are connected to the input ports of a network analyzer. By measuring the resonant frequency ( f 0 ) and quality factor (Q) of the T E 0 n p resonant modes, the relative permittivity and loss tangent of the sample can be determined. This procedure is based on an analytical model first developed by Michael D. Janezic and James Baker-Jarvis [23,24].
The equipment used is a Split-Cylinder Cavity, from the Institute of Information and Communication Technologies (ITACA) settled in Valencia, Spain, for measuring rectangular flat samples with a resonance frequency of 6.25 GHz (mode T E 101 is excited in the cavity at vacuum) and a VNA, as shown in Figure 2b. Then, MATLAB R2025a software was used to calculate the permittivity of the materials following the circuit analysis described in [20], with an extension of the circuital model for the circular modes in the split cavity, which can be found in [25].

2.1.3. Rectangular Waveguide

Rectangular waveguide is one of the most commonly used instruments for the measurement of dielectric properties [26,27]. A rectangular sample of MUT, with a specified length, is placed in an empty waveguide, provoking a perturbation of an electric field, which is frequency-dependent. By measuring the resulting S 21 and S 11 parameters, the dielectric properties of the MUT at a given frequency can be extracted. For the measurements of the work, the WR42 (18–26.5 GHz) rectangular waveguide is used jointly with a VNA, as shown in Figure 3. The MUT size must fit the X-band rectangular waveguide aperture, which is 10.668 × 4.318 mm (corresponding to WR42 rectangular waveguide size standard). This measurement setup was used for the MUT characterization at 24.5 GHz.

2.2. Materials

2.2.1. Polymers for Additive Manufacturing

Traditional materials for AM, as PLA or ABS polymers used with FDM technologies, have been characterized at microwave frequencies, and their dielectric constant and tangent loss are well known [28,29]. Nevertheless, the advent of new technologies and materials raises the need for analysing their dielectric properties. In this work, six different polymers were characterized: Thought 200 and Rigid 10K resins from Formlabs, MLSA Modelling Dental resin from ApplyLabWork, Composite X (CX) resin from Liqcreate, Ultrasint PP (UPP) powder from BASF, and Polyamide 11 (PA11) Bio powder from Stratasys. Dental and Thought 200 are acrylic resins used by VPP, similar to Rigid 10K and Composite X. However, these last two resins have a load of silica, making them more resistant to temperature, harder, and less prone to deformations. UPP is a polypropylene powder used for Multijet PBF technology, while PA11 is a polyamide powder used in PBF technology.
Three different types of samples were printed in order to obtain the measurements at the three frequencies: a cylinder of 6.50 mm of radius and 40 mm of height for the Resonant Coaxial Bireentrant Microwave Cavity at 2.45 GHz, a flat square size 95 × 95 × 2 mm for the Split-Cylinder Resonant Cavity at 6.25 GHz and a cuboid size 10.668 × 4.318 mm and 3 mm of length for the WR42 Rectangular Waveguide at 24.5 GHz, as can be seen in Figure 4. It should be emphasized that it is not required for the cuboid sample to have precise micron-level dimensions to be measured using the WR42 Rectangular Measurement Kit; it only needs to fit within the waveguide. The small deviations can be corrected with the measurement method used. To design the three geometries, Solidworks software was used.

2.2.2. Permittivity Measurements of Solid Polymers

Table 1 shows the dielectric properties of the different polymers for the three frequencies. The materials show very slight differences in frequency, indicating that within the microwave bandwidth, the dielectric properties are stable. As expected, materials containing silica in the resin (Rigid 10K and Composite X) present a higher dielectric constant, and materials made from polymer powder (UPP and PA11) present a lower one. The same behavior is observed in the material density, which, in the end, will be translated to the weight of the final printed item.

2.2.3. Stochastic and Regular Meshing

Once the solid polymers were characterized, the complex permittivity of the same materials but with different densities was measured. The objective was to have graphs for different materials and frequencies relating density to dielectric properties. Since these properties seem to be quite constant in the frequency range, only the measurements for 2.45 and 24.5 GHz were performed. Furthermore, not all the materials were measured at this stage; since Dental and Though 200 seem to have similar properties, only Dental was used. Composite X and Rigid 10K presented different dielectric constants, so both were measured. Similarly, the measurements were also performed for PA11 and UPP.
The samples (cylinder and cuboid) were manufactured using porous lattices. These structures are widely used in various fields, including materials science and engineering. They can be broadly categorized into two types, both used in this work: regular lattices (gyroid mesh) and stochastic lattices (Voronoi mesh). The printing densities were 25, 50 and 75% (100% is the solid sample), as it is shown in Figure 5. To design the gyroid mesh, the Flattpack v.2025 software was used, which is a freely distributed library implemented in Matlab, developed within the framework of the University of Nottingham, and allows for the processing of geometrical objects by directly uploading the models to the program and processing them to obtain porous structures. To design the Voronoi mesh, the Grasshopper 3D tool from Rhinoceros 3D version 8 commercial CAD software was used.

2.2.4. Permittivity Measurements of Porous Polymers

Regarding the porous samples, Table 2 shows the results for the materials at the two extreme frequencies. The samples were manufactured with gyroid or Voronoi meshes. From these data, the graphs in Figure 6 and Figure 7 were extracted, enabling a wide range of permittivities within the same material (at 2.45 and 24.5 GHz, respectively).
Measuring the dielectric properties at 24.5 GHz presents a technological challenge, as methods such as the bi-reentrant cavity and split cylinder do not provide reliable results due to the small size of the samples and cavities and the manufacturing tolerances, so the rectangular waveguide method is used instead. Although this method is reliable for characterizing the dielectric constant, its uncertainty in calculating the loss tangent presents challenges, as stated in [30,31], so that the results of the loss tangent at that frequency are missing in this study. However, this uncertainty does not affect the phase, only the attenuation, so the impact of losses is limited to a reduction in gain and radiation efficiency of the antenna set.

3. Horn Antenna and Gradient Index Lens Design

The objective of the design was to obtain a complete set with a horn antenna and GRIN lens, which meet certain EM and mechanical specifications. The main idea behind the GRIN lens is that it focuses the radiation pattern of a radiating element, enhancing the directivity of the set. In this general approach, two main elements were designed, on the one hand, the radiating element, and on the other hand, the lens. The electromagnetic design is frequency-dependant, but scalable, allowing a design developed for one frequency to be easily adjusted for another. The selected working frequency for the set was 10 GHz, covering services in X-band satellite communications. On the other hand, mechanical issues were considered, such as the weight of the set and how the radiation element and the lens are built up together, in order to obtain a compact element ready to be used.

3.1. Electromagnetic Design

3.1.1. Horn Antenna

The radiating element is located in the focal point of the set. For the type of communication services the set was intended for (satellite), the whole system would have to handle high power and require low loss; the optimal technology in that case would be waveguide, either rectangular or circular. Traditionally, horn antennas have been used together with waveguides due to ease of integration and high efficiency. In this case, a conic horn was designed to achieve a good balance between illumination efficiency and spillover efficiency. The criterion adopted was that the electromagnetic field level radiated by the horn at the edges of the lens should be 10 dB below the maximum, ensuring an optimal balance between illumination efficiency and spillover efficiency, thereby maximizing the total efficiency of the system. The sketch with the dimensions of the horn is presented in Figure 8a,b, and the values are provided in Table 3.

3.1.2. Gradient Index Lenses

The design of the lens covered several stages. First of all, some parameters were chosen in order to meet the sensible size and weight of the whole set. Then, an adjoint method, see [32], was used to obtain the permittivity values depending on the radius.
The focal point r 0 was chosen such that f / D = 1 , indicating that the focal length is equal to the diameter of the lens. For practical purposes, the diameter of the lens was D = 15 cm, and its width H = 2.5 cm. That would provide a realizable lens with a low cost AM printer. However, the achievable range of permittivity values was constrained by the available materials and the limitations of the additive manufacturing process. Specifically, printing densities below 20% were avoided to maintain the structural integrity of the lens. Consequently, the feasible permittivity values ranged from ε max to 0.2 ( ε max 1 ) + 1 , where ε max represents the relative dielectric constant of the material at 100% density.
On the other hand, not all possible ranges of permittivity could be considered, as the design was constrained by the available materials and the limitations of the printers. A printing density lower than 20% would compromise the structural integrity of the lens. So the possible values ranged from ϵ m a x to 0.2( ϵ m a x 1) + 1, where ϵ m a x is the relative dielectric constant of the material printed at 100 % density.
The optimization process determined the optimal distribution of ϵ r ( x , y ) within a rectangular domain of height D and width H. This domain was divided into 11 regions, resulting in 11 levels of freedom where ϵ r was constant within each region. Thus, the lens was modeled via the Lippmann–Schwinger integral equation in 2D, as in Equation (3).
E ( r ) = E inc ( r ) + k 0 2 V G ( r , r ) χ ( r ) E ( r ) d V ,
with contrast χ ( r ) = ε r ( r ) 1 and free-space Green’s function G. The design objective was the field intensity at the focal point r f , Equation (4).
J = E ( r f ) 2 ,
By using the adjoint field E and satisfying Equation (5),
E ( r ) = G ( r , r f ) + k 0 2 V G ( r , r ) χ ( r ) E ( r ) d V ,
the gradient with respect to each annular permittivity ε r ( i ) was given by Equation (6).
J ε r ( i ) = 2 k 0 2 V i E ( r ) E ( r ) d V ,
A quasi-Newton optimizer then updated the 11 discrete ε r ( i ) until convergence ( Δ J / J < 10 5 or 100 iterations).
The sketch representing the lens with sectors and corresponding values of permittivity is presented in Figure 8d. It is worth mentioning that the optimized and manufactured lenses presented a central cylindrical sector with a radius of 12.5 mm (which corresponds to the permittivity ϵ r 6 ) and then the five successive concentric rings with a thickness of 12.5 mm.
The optimizer achieved three different results: a flat heterogeneous lens design, referred to as lens A (Figure 9a); an airy disk pattern, lens B (Figure 9b); and a ring pattern, lens C (Figure 9c). The values of the relative dielectric constant for the different sectors of the three realizations are shown in Table 4. Both lens B and C present patterns associated with Fraunhoffer diffraction through circular apertures.

3.2. Mechanical Design

The feeding horn antenna and the lens were assembled using a mechanical support. The support was required to provide structural resistance without affecting electromagnetic performance of the antenna, promote the modularity of the system, as well as allow for the exchange of the three types of lenses. The dimensions of the support are outlined in Figure 8c and their values are given in Table 3. A four-piece design was chosen, with the pieces connected by pegs, allowing for easy assembly and disassembly. Additionally, to reduce the weight of the support while maintaining its structural resistance, it was designed as a series of rods connected by St. Andrew’s crosses, as shown in Figure 10. The mechanical support was designed using Solidworks v.2025 software.

3.3. Electromagnetic Impact of Support Structure

To assess the scattering and diffraction effects of St. Andrew’s cross lattice support, we conducted two complementary studies:
  • Full-wave simulation: The CST model was executed twice—once with the support structures included, and once with them omitted. A comparison of the resulting far-field patterns at 10 GHz showed a maximum change in main-lobe gain of 0.3 dB and an increase in sidelobe levels of no more than 0.5 dB. No additional lobes or ripples were observed.
  • Experimental measurement: Using an anechoic chamber, we measured the radiation pattern of the lens–horn assembly both with and without the printed support. The resulting patterns aligned within ±0.4 dB across the entire angular range, confirming the simulation findings.
These results demonstrate that the selected lattice geometry and materials (PA11 and UPP) introduce minimal electromagnetic interference. Consequently, the support structure has a negligible impact on the overall antenna performance.

4. Prototype Manufacturing

4.1. Additive Manufacturing

The assembly of the horn antenna, the lens, and the support was additively manufactured. Different materials and technologies were used for each piece, depending on their characteristics.
The designed RF feeding element, the X-band conical horn antenna, was manufactured using Vat Photopolymerization technology with curing by exposure to an ultraviolet laser beam with acrylic resin (VPP) with the printer Form 3BL of Formlabs; resin Rigid10K was used, suitable for precise and rigid prints. The piece then underwent the process of sandblasting and metallization; the manufactured part is presented in Figure 10a, before metallization, and (b), after the metallization process.
The three realizations of the lenses were manufactured with different materials, depending on their required dielectric constants provided by adjoint method optimization. Lens A was fabricated using Composite X resin due to its higher dielectric permittivity variation. Lens B was manufactured using Dental resin, selected for its dielectric constant, which is compatible with the design requirements, as well as its lower density compared to other acrylic-based resins. For the same reasons, Lens C was manufactured using Rigid 10K resin. All of them were printed using Vat Photopolymerization technology, with curing by exposure to an ultraviolet laser beam with acrylic resin (VPP). All of the prototypes are presented in Figure 9.
Regarding the support, it was manufactured using two different powder materials: PA11, printed with Stratasys SAF 350 equipment, and UPP, printed with HP Multi Jet Fusion 5200 3D. These materials were chosen for their lightness, low permittivity, and good mechanical performance. In both cases, their mechanical and electromagnetic performances were similar. The assemblies using both PA11 and UPP mechanical support are presented in Figure 10c.

4.2. Metallization Process

The feeding horn antenna must be a conductive element, so it must be coated with a homogeneous layer of electrically conductive material. This was performed using two successive electroless coating processes of nickel and copper [33]. This method uses a chemical reaction to bond particles of the desired metal to the surface of the polymer pieces [34] without the use of an electric current.
Initially, the surface of the piece must be prepared to allow strong bonding with the metal deposition. The most common method for this involves chemical etching with strong oxidizing compounds such as chromium salts, which are highly corrosive and polluting. In this work, the chromium salt etching was replaced by a combination of a first shot blasting and a subsequent chemical etching with sodium hydroxide solution. Then, a catalytic layer of palladium is deposited on the surfaces of the pieces by immersion in an activating bath consisting of a P d C l 2 and S n C l 2 acidic solution, as described in [35]. Before the final metallization bath, an acceleration step is performed by treating the sample in an acidic solution to remove the non-reacted salts and the S n ( I V ) and expose the P d ( 0 ) to the autocatalytic reaction. This layer is responsible for initiating the chemical reduction reaction in which the metal adheres to the surface.
The initial nickel coating process results in a relatively uniform and stable metallic deposition, although it may leave some small uncovered areas, particularly in the corners. Despite the uniformity of the layer, the nickel coating presents very low conductivity, so an additional copper bath is applied to fix minor defects and increase the conductivity.

5. Results

The electromagnetic response of the assembled prototypes was evaluated in an anechoic chamber, with the experimental setup depicted in Figure 11. The simulated directivity of the horn antenna and the set with the three different lenses, using the CST Dassault Systems Suite, is presented in Figure 12a. Therefore, the horn directivity at the maximum of the radiation ( ϕ = 0 ) is 13.4 dB. By adding lenses to the radiation set, a substantial increase in directivity is achievable (up to total directivity of 21 dB for lens A and 20 dB for lenses B and C). The directivities of the different lens antennas were measured and their results are given in Figure 12b. Regarding lens A, the achieved directivity is 19.5 dB, less than the 21 dB predicted by the simulation. This is most probably due to the fact that the lens was manufactured in four separate pieces. Therefore, airy gaps may appear due to an imperfect mechanical assembly, see Figure 9a, so the degradation in the farfield measured directivity response is observed. Regarding lenses B and C, the simulation results match very well, even with better results, showing a slightly more directive radiation pattern in the maximum (22 dB for lens B and 22.1 dB for lens C at ϕ = 0 ).
Additionally, the lenses, as well as the horn antenna and the support, were weighed, with the results presented in the Table 5. As shown, both the horn antenna and the support are very light, with the lens providing the main contribution to the overall weight. The total weight of the sets ranges from approximately 500 g for lens A to 280 g for lens C.
Table 6 displays the results of our three lenses, which are compared to the recent literature. The main conclusion is that the lenses present similar measured directivity. Lenses B and C present similar or better aperture efficiency compared to the lenses with similar sizes but with an important reduction in thickness, which substantially decreases the volume of the whole set. This is achieved by using variable densities of the printing material in different sectors with consistent thickness, instead of varying the lens thickness—a traditional approach for these lenses. This approach also enhances lens aperture efficiency, as evidenced by our measured results.

6. Conclusions

In this work, we have designed, fabricated, and experimentally validated three GRIN-lens realizations for a compact X-band horn-lens assembly. Experimental measurements showed that lens B achieved the highest performance—measured directivity of 22.1 dBi and aperture efficiency of 55.8%—with a total lens weight of 207 g, see Table 5. Consequently, lens B is identified as the optimal solution for the envisaged compact X-band satellite-communication application. This result demonstrates the effectiveness of full-wave adjoint optimization, coupled with additive manufacturing, in producing application-specific high-performance RF components.
Furthermore, the GRIN-lens antenna presented in this work was designed for terrestrial satellite–ground communications, where environmental conditions (temperature, humidity, and mechanical loads) remained within the operational limits of polymer-based 3D-printed dielectrics. Nevertheless, the study of 3D-printed materials for RF Applications in space flights is a current trend [43]. It was demonstrated that the metallized polymeric materials (Rigid 10K and Composite-X), as used here, can be space-qualified [44]. As for other polymers used in this work, they may exhibit significant outgassing in vacuum and cannot withstand the extreme thermal cycling encountered in space, so further research is required. Consequently, the GRIN-lens antenna design proposed in this work may be suitable for deployment on the payload of a satellite, with substantial modifications. Future adaptation for spaceflight would require substituting the polymer GRIN lens with space-rated dielectrics (e.g., ceramics or radiation-hardened glasses), along with full vacuum, thermal-vacuum, and radiation qualification [45].
In conclusion, the exploration of AM for fabricating complex RF components—such as horn antennas and GRIN lenses—is not only feasible but also advantageous for the communications industry. By enabling the integration of lightweight, customizable, and precisely engineered polymer structures with metalized conductive elements, AM provides a versatile platform for advanced RF device design. The ability to control material properties and topology on a fine scale, particularly for gradient-index lenses, represents a key advancement in wave manipulation and antenna performance. As the field of AM continues to evolve, its application in communications is likely to expand, supporting the development of more sophisticated, compact, and efficient systems across a range of frequencies and applications.

Author Contributions

Conceptualization, F.V. and C.B.; methodology, C.B.; software, A.V., F.V., and L.S.; validation, F.V., F.P., and R.K.; formal analysis, F.V.; investigation, A.V. and Á.F.; resources, C.B.; data curation, A.V.; writing—original draft preparation, A.V.; writing—review and editing, C.B.; visualization, A.V.; supervision, C.B. and F.V.; project administration, F.V.; funding acquisition, C.B. All authors have read and agreed to the published version of the manuscript.

Funding

This work has been funded by Agencia Valenciana de la Innovación through the research project INNEST/2022/124; FEDER, EU: PID2022-136590OB-C41/AEI/10.13039/501100011033; European Union NextGenerationEU project PRTR-C17.I1 as part of the Advanced Materials program supported by Ministerio de Ciencia e Innovación, Generalitat Valenciana project: MAOCOM-6G, Code: MFA/2022/056 and Ministerio de Ciencia e Innovación project PID2022-136869NB-C33.

Data Availability Statement

The original contributions presented in this study are included in the article. Further inquiries can be directed to the corresponding author.

Conflicts of Interest

The authors declare no conflict of interest.

Abbreviations

The following abbreviations are used in this manuscript:
AMAdditive Manufacturing
CXComposite X
EMElectromagnetic
FFFFused Filament Fabrication
GRINGradient Index
MUTMaterial Under Test
OEWGOpen End Waveguide
PA11Polyamide 11
PBFPowder Bed Fusion
RFRadio Frequency
SLAStereolithography
UPPUltrasint PP
VNAVector Network Analyzer
VPPVat Photopolymerization

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Figure 1. Resonant Coaxial Bireentrant Microwave Cavity: (a) schematic of the resonant cavity; (b) detail of the actual cavity before being inserted into the measurement equipment.
Figure 1. Resonant Coaxial Bireentrant Microwave Cavity: (a) schematic of the resonant cavity; (b) detail of the actual cavity before being inserted into the measurement equipment.
Jmmp 09 00238 g001
Figure 2. Measurement Equipment: (a) Single-Post Reentrant Cavity Measurement Kit at 2.45 GHz; (b) Split-Cylinder Resonant Cavity Measurement Kit at 6.25 GHz.
Figure 2. Measurement Equipment: (a) Single-Post Reentrant Cavity Measurement Kit at 2.45 GHz; (b) Split-Cylinder Resonant Cavity Measurement Kit at 6.25 GHz.
Jmmp 09 00238 g002
Figure 3. WR42 Rectangular Waveguide Measurement Kit at 24.5 GHz.
Figure 3. WR42 Rectangular Waveguide Measurement Kit at 24.5 GHz.
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Figure 4. Solid samples of: (a) PA11; (b) Dental; (c) Rigid 10K.
Figure 4. Solid samples of: (a) PA11; (b) Dental; (c) Rigid 10K.
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Figure 5. Cylindrical Rigid 10K samples: (a) gyroid mesh; (b) Voronoi mesh.
Figure 5. Cylindrical Rigid 10K samples: (a) gyroid mesh; (b) Voronoi mesh.
Jmmp 09 00238 g005
Figure 6. Variable density sample measurements at 2.45 GHz.
Figure 6. Variable density sample measurements at 2.45 GHz.
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Figure 7. Variable density sample measurements at 24.5 GHz.
Figure 7. Variable density sample measurements at 24.5 GHz.
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Figure 8. Mechanical design dimensions of the X-Bend Antenna Assembly: (a) horn elevation view; (b) horn plan view; (c) support profile view; (d) plan view of the X-Bend Lens.
Figure 8. Mechanical design dimensions of the X-Bend Antenna Assembly: (a) horn elevation view; (b) horn plan view; (c) support profile view; (d) plan view of the X-Bend Lens.
Jmmp 09 00238 g008
Figure 9. X-Band GRIN Lenses: (a) Lens A, material Composite X resin, technology VPP; (b) Lens B, material Dental resin, technology VPP; (c) Lens C, material Rigid 10K resin, technology VPP.
Figure 9. X-Band GRIN Lenses: (a) Lens A, material Composite X resin, technology VPP; (b) Lens B, material Dental resin, technology VPP; (c) Lens C, material Rigid 10K resin, technology VPP.
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Figure 10. Manufactured Prototypes: (a) feeding horn antenna, material Rigid 10K resin, technology VPP, sandblasted; (b) horn antenna after Ni+Cu autocatalytic coating; (c) X-Band lens assembly: feeding horn, support, and lens.
Figure 10. Manufactured Prototypes: (a) feeding horn antenna, material Rigid 10K resin, technology VPP, sandblasted; (b) horn antenna after Ni+Cu autocatalytic coating; (c) X-Band lens assembly: feeding horn, support, and lens.
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Figure 11. X-Band Antenna Assembly Measurements in laboratory anechoic chamber.
Figure 11. X-Band Antenna Assembly Measurements in laboratory anechoic chamber.
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Figure 12. Directivity of the lenses at 10 GHz, ϕ = 0 º : (a) simulated; (b) measured.
Figure 12. Directivity of the lenses at 10 GHz, ϕ = 0 º : (a) simulated; (b) measured.
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Table 1. Solid sample measurements.
Table 1. Solid sample measurements.
f = 2.45 GHzf = 6.25 GHzf = 24.5 GHz
ResinDens. ( g / cm 3 ) ϵ r tan ( δ ) ϵ r tan ( δ ) ϵ r tan ( δ )
CX1.523.540.151313.670.194203.470.02900
Dental1.302.840.055492.830.050062.940.06000
Tough1.112.890.033412.950.03745--
Ultrasint PP0.892.190.033202.190.035842.110.02570
Rigid 10K1.633.230.034793.320.034893.170.02000
PA111.012.720.05020--2.63-
Table 2. Variable density sample measurements.
Table 2. Variable density sample measurements.
f = 2.45 GHzf = 24.5 GHz
ResinPorosity (%)Dens. ( g / cm 3 ) ϵ r tan ( δ ) ϵ r tan ( δ )
CX0.251.143.250.132322.87-
CX0.500.762.290.078842.08-
CX0.750.381.620.029781.61-
Dental0.250.982.550.041622.36-
Dental0.500.651.830.030211.80-
Dental0.750.331.400.014671.37-
PA110.250.762.290.037702.29-
PA110.500.511.860.027671.71-
PA110.750.251.440.017631.26-
Ultrasint PP0.250.671.980.026091.91-
Ultrasint PP0.500.451.730.023061.67-
Ultrasint PP0.750.221.380.011011.24-
Rigid 10K0.251.222.670.026092.63-
Rigid 10K0.500.822.120.017402.08-
Rigid 10K0.750.411.560.008701.54-
Table 3. Parameters of mechanical design of the X-Bend Antenna Assembly.
Table 3. Parameters of mechanical design of the X-Bend Antenna Assembly.
ParameterDimmension (mm)ParameterDimmension (mm)
C129.74C27.07
D156D223.40
D348D456
D52.8D160
L133L225
L380H25
T2f131.6
R12.5g25
Table 4. Values of ϵ r of the GRIN lens models.
Table 4. Values of ϵ r of the GRIN lens models.
ϵ r 1 ϵ r 2 ϵ r 3 ϵ r 4 ϵ r 5 ϵ r 6 ϵ r 7 ϵ r 8 ϵ r 9 ϵ r 10 ϵ r 11
A1.702.252.963.543.543.543.543.542.962.251.71
B2.84111.371.491.591.491.37112.84
C2.751111111112.75
Table 5. Weight of the X-Bend Antenna Assembly.
Table 5. Weight of the X-Bend Antenna Assembly.
Device:Conical HornSupportLens ALens BLens C
Weight (g):2296376207163
Table 6. Comparison of different realizations of 3D printed perforated dielectric GRIN lens antennas.
Table 6. Comparison of different realizations of 3D printed perforated dielectric GRIN lens antennas.
Ref.Freq. [GHz]Lens TypeTech.Mat.Feed TypeDiameter/Thickness (F+T) mm.Dir. (Sim./Meas.)Ap. eff. (Sim./Meas.)
lens A10Flat heterogenousSLAComposite X ResinCircular Waveguide160/2521/19.549.1%/32.17%
lens B10Airy diskSLADental ResinCircular Waveguide160/2520/22.141.22%/55.80%
lens C10RingSLARigid 10K ResinCircular Waveguide160/2520/2242.37%/49.21%
[10]12, 15, 18Flat finite Focal GRIN lensFFFPLACircular Waveguide120/18.518 at 12 GHz/21.4 at 15 GHz/24 at 18 GHz 218% at 12 GHz/33% at 15 GHz/41% at 18 GHz 2
[36]12–22Zero Focal length GRIN LensFFFPREPERMCircular Waveguide150/9022.6/22.938%/40%
[11,37]34Flat Finite Focal Length GRIN LensFFFPREPERMCorrugated Circular OEWGs88/40.526.5/25.745%/37%
[38]12–40Flat Finite Focal GRIN lensFFFPREPERMRectangular OEWGs120/18.515.1 at 12 GHz/23.6 at 40 GHz 282% 2
[39]13.43D ShapedFFFPLAMicrostrip Patch180/22326.3/25.166.7% 1
[40]15RectangularMat. JettingVerowhiteRectangular OEWGs-/5921.3/19.130% 1
[41]27Flat finite Focal GRIN lensSLAResinMicrostrip Patch Antenna77/7721.3 130% 1
[42]33Fresnel Zone LensFFFPREPERMRectangular OEWGs97.6/39.325.2/25.2-/31.1%
1 Simulated data. 2 Measured data.
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MDPI and ACS Style

Voronov, A.; Bachiller, C.; Ferrer, Á.; Vico, F.; Sempere, L.; Peñaranda, F.; Kronberger, R. Additive Manufacturing of Variable Density Lenses for Radio Frequency Communications in X-Band. J. Manuf. Mater. Process. 2025, 9, 238. https://doi.org/10.3390/jmmp9070238

AMA Style

Voronov A, Bachiller C, Ferrer Á, Vico F, Sempere L, Peñaranda F, Kronberger R. Additive Manufacturing of Variable Density Lenses for Radio Frequency Communications in X-Band. Journal of Manufacturing and Materials Processing. 2025; 9(7):238. https://doi.org/10.3390/jmmp9070238

Chicago/Turabian Style

Voronov, Aleksandr, Carmen Bachiller, Álvaro Ferrer, Felipe Vico, Lluc Sempere, Felipe Peñaranda, and Rainer Kronberger. 2025. "Additive Manufacturing of Variable Density Lenses for Radio Frequency Communications in X-Band" Journal of Manufacturing and Materials Processing 9, no. 7: 238. https://doi.org/10.3390/jmmp9070238

APA Style

Voronov, A., Bachiller, C., Ferrer, Á., Vico, F., Sempere, L., Peñaranda, F., & Kronberger, R. (2025). Additive Manufacturing of Variable Density Lenses for Radio Frequency Communications in X-Band. Journal of Manufacturing and Materials Processing, 9(7), 238. https://doi.org/10.3390/jmmp9070238

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