The Effect of Laser Irradiation to Surfaces of Computer-Aided Design/Computer-Aided Fabrication Resin Blocks Coated with a Silane Coupling Agent on Bond Strength between the Resin Blocks and Composite Resin
Abstract
:1. Introduction
2. Materials and Methods
2.1. Experimental Materials
2.2. Plate Preparation
2.3. Specimen Preparation
2.4. Shear Bond Strength (SBS) Test
2.5. SBS Test after the Thermal Cycling Load Test
2.6. Failure Mode Analysis
2.7. Scanning Electron Microscopy (SEM) Observation
2.8. Measurement of Plate Surface Temperatures after Laser Irradiation
3. Results
3.1. SBS
3.2. Results of the Analysis of Failure Modes
3.3. SEM Images of Specimens Representing Each Failure Mode
3.4. Surface Temperature of the Plates Estimated Immediately after Laser Irradiation
4. Discussion
5. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Material | Code | Lot#No. | Composition | Manufacturer |
---|---|---|---|---|
Cerasmart 300 | CS | 2302206 | Bis-MEPP, UDMA, DMA (29 wt%), SiO2 and B2O3 glass nanofillers (71 wt%) | GC |
Vita Enamic | EN | 97110 | Bis-GMA, UDMA, Bis-EMA, TEGDMA, polymer network (14 wt%), SiO2, Al2O3, Na2O, K2O, B2O3, ZrO2, CaO ceramic network (86 wt%) | Vita |
Clearfil Majesty ES Flow | – | A30347 | Surface-treated barium glass, surface-treated silica fillers, monomer (TEGDMA and methacrylic acid monomer), photopolymerization catalyst, stabilizing agent, coloring agent | Kuraray Noritake Dental |
Clearfil Ceramic Primer Plus | – | B10087 | Silane coupling agents, monomer (MDP), and ethanol | Kuraray Noritake Dental |
Clearfil Universal Bond Quick ER | – | 4J0349 | Monomer (Bis-GMA, phosphate ester monomer: MDP, HEMA, hydrophilic amide monomer), filler (silica-based micro filler), ethanol, photopolymerization catalyst, scientific polymerization accelerators, purified water, and NaF | Kuraray Noritake Dental |
Group Code | Laser Irradiation Power | n | Thermal Cycling Load Test |
---|---|---|---|
CSC | without irradiation | 10 | Without loading |
CS3 | 3 W | ||
CS5 | 5 W | ||
CS7 | 7 W | ||
ENC | without irradiation | ||
EN3 | 3 W | ||
EN5 | 5 W | ||
EN7 | 7 W | ||
sCSC | without irradiation | 10 | With loading of 10,000 cycles |
sCS7 | 7 W | ||
sENC | without irradiation | ||
sEN7 | 7 W |
Factor | Type III Sum of Squares | Degrees of Freedom | Mean Square | F Value | p Value |
---|---|---|---|---|---|
Material Type | 1.044 | 1 | 1.04 | 0.12 | 0.72 |
Laser Power | 128.44 | 3 | 42.81 | 5.19 | 0.003 |
Material Type * Laser Power | 19.04 | 3 | 6.34 | 0.77 | 0.51 |
Error | 592.91 | 72 | 8.23 | ||
Overall | 741.44 | 79 |
Factor | Type III Sum of Squares | Degrees of Freedom | Mean Square | F Value | p Value |
---|---|---|---|---|---|
Material Type | 440.10 | 1 | 440.10 | 1279.44 | <0.001 |
Laser Power | 1069.43 | 2 | 534.71 | 1554.49 | <0.001 |
Material Type * Laser Power | 57.63 | 2 | 28.81 | 83.77 | <0.001 |
Error | 18.57 | 54 | 0.34 | ||
Overall | 1585.74 | 59 |
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Ohno, H.; Suzuki, M.; Shinkai, K. The Effect of Laser Irradiation to Surfaces of Computer-Aided Design/Computer-Aided Fabrication Resin Blocks Coated with a Silane Coupling Agent on Bond Strength between the Resin Blocks and Composite Resin. Dent. J. 2023, 11, 290. https://doi.org/10.3390/dj11120290
Ohno H, Suzuki M, Shinkai K. The Effect of Laser Irradiation to Surfaces of Computer-Aided Design/Computer-Aided Fabrication Resin Blocks Coated with a Silane Coupling Agent on Bond Strength between the Resin Blocks and Composite Resin. Dentistry Journal. 2023; 11(12):290. https://doi.org/10.3390/dj11120290
Chicago/Turabian StyleOhno, Hiroshi, Masaya Suzuki, and Koichi Shinkai. 2023. "The Effect of Laser Irradiation to Surfaces of Computer-Aided Design/Computer-Aided Fabrication Resin Blocks Coated with a Silane Coupling Agent on Bond Strength between the Resin Blocks and Composite Resin" Dentistry Journal 11, no. 12: 290. https://doi.org/10.3390/dj11120290