Comparative Analysis on the Structure and Properties of Iron-Based Amorphous Coating Sprayed with the Thermal Spraying Techniques
Abstract
:1. Introduction
2. Materials and Methods
3. Results and Discussion
3.1. Morphological Analysis
3.2. Phase Analysis of the Coating
3.3. Corrosion Studies
3.3.1. Potentiodynamic Polarization Scan
3.3.2. Electrochemical Impedance Spectroscopy
3.4. Wear Studies
Tribometric Test
4. Conclusions
Author Contributions
Funding
Conflicts of Interest
References
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Voltage | Current | Feeding Rate | Spray Distance | Power |
---|---|---|---|---|
55–60 V | 200–850 A | 30 g min−1 | 200 mm | 35 KW |
Propane Flow | Oxygen Flow | Feeding Rate | Spray Distance | Compressed Air |
---|---|---|---|---|
25 L min−1 | 15 L min−1 | 30 g min−1 | 300 mm | 0.5 MPa |
Bare and Coated Samples | Ecorr (mV) | icorr (nA/cm2) | Corrosion Rate (mpy) |
---|---|---|---|
APS | −364.563 mV (±0.50%) | 954.144 nA (±0.50%) | 1.0233 (±0.50%) |
HVOF | −282.065 mV (±0.25%) | 118.793 nA (±0.25%) | 0.1274 (±0.25%) |
Mild Steel Substrate | −0.957 V (±0.25%) | 46.7 µA (±0.25%) | 40.13 (±0.25%) |
EIS Sample | Rs (ohm) | CPE, Yο Q1 (S-secn) | n | R1 (ohm) | CPE, Yο Q1 (S-secn) | n | R2 (ohm) |
---|---|---|---|---|---|---|---|
APS | 2.542 | 5.067 × 10−5 | 0.7787 | 6153 | 8.648 × 10−5 | 0.4121 | 6257 |
HVOF | 6.389 | 0.001492 | 0.6447 | 4.335 | 8.139 × 10−7 | 0.689 | 1790 |
Bare and Coated Samples | Coating Thickness (µm) | Hardness (Hv) | Accumulated Wear Volume (mm3) | Distance (m) | Wear Rate mm3N−1m−1 |
---|---|---|---|---|---|
HVOF | 302.96 | 1152 ± 22.14 | 0.001120428 | 50 | 0.005602138 (±0.000112) |
APS | 315.98 | 1107 ± 23.04 | 0.009491135 | 50 | 0.047455677 (±0.000949) |
MS | - | 227 ± 4.5 | 0.005092087 | 50 | 1.01842 × 10−5 (±0.00204) |
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Iqbal, A.; Siddique, S.; Maqsood, M.; Atiq Ur Rehman, M.; Yasir, M. Comparative Analysis on the Structure and Properties of Iron-Based Amorphous Coating Sprayed with the Thermal Spraying Techniques. Coatings 2020, 10, 1006. https://doi.org/10.3390/coatings10101006
Iqbal A, Siddique S, Maqsood M, Atiq Ur Rehman M, Yasir M. Comparative Analysis on the Structure and Properties of Iron-Based Amorphous Coating Sprayed with the Thermal Spraying Techniques. Coatings. 2020; 10(10):1006. https://doi.org/10.3390/coatings10101006
Chicago/Turabian StyleIqbal, Amjad, Sumera Siddique, Moazam Maqsood, Muhammad Atiq Ur Rehman, and Muhammad Yasir. 2020. "Comparative Analysis on the Structure and Properties of Iron-Based Amorphous Coating Sprayed with the Thermal Spraying Techniques" Coatings 10, no. 10: 1006. https://doi.org/10.3390/coatings10101006