Encapsulation of Cinnamon Essential Oil for Active Food Packaging Film with Synergistic Antimicrobial Activity
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Preparation of the Ion-Exchanged Permutite and Ag+/Zn2+-Permutite/CEO
2.3. Characterization and Measurement
2.4. Anti-Discoloration Property Assays and Nitrogen Physisorption
2.5. FT-IR Spectra and DSC Curve of Permutite Samples
2.6. The Loading Capacity and Release Behavior
2.7. Antimicrobial Assays
2.8. Extension of the Shelf Life of Chinese Bayberry Fruit and Migration Security Tests
2.9. Statistical Analysis
3. Results
3.1. Permutite Sample Characterization
3.2. Characterization of Ag+/Zn2+-Permutite/CEO
3.3. Release Behavior of Ag+/Zn2+-Permutite/CEO
3.4. Antimicrobial Activity of Pads
3.5. Application of the Antimicrobial Pads in Chinese Bayberry Fruit
4. Conclusions
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
References
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Samples | Content of Metal Ion (wt%) | |||||
---|---|---|---|---|---|---|
Na+ | Mg2+ | K+ | Ca2+ | Ag+ | Zn2+ | |
a | 11.73 ± 0.5 | 1.35 ± 0.09 | 0.40 ± 0.03 | 0.77 ± 0.05 | ND | ND |
b | 6.16 ± 0.3 | 0.52 ± 0.06 | ND | 0.49 ± 0.02 | 18.47 ± 1.32 | ND |
c | ND | 0.87 ± 0.04 | ND | 0.69 ± 0.04 | ND | 9.55 ± 0.74 |
d | 1.10 ± 0.3 | 0.65 ± 0.03 | ND | 0.47 ± 0.06 | 9.68 ± 0.94 | 7.80 ± 0.61 |
Specimens | L* | a* | b* | W (L, a, b) | ∆E | ||||
---|---|---|---|---|---|---|---|---|---|
Original | UV | Original | UV | Original | UV | Original | UV | ||
a | 91.26 ± 2.42 | 88.20 ± 3.62 | 0.00 | −0.09 ± 0.02 | −0.38 ± 0.06 | −0.48 ± 0.09 | 91.3 ± 3.98 | 88.2 ± 2.13 | 3.1 ± 0.41 |
b | 72.04 ± 1.42 | 82.08 ± 2.41 | 1.00 ± 0.12 | −0.42 ± 0.04 | 5.08 ± 0.24 | 4.45 ± 0.29 | 71.6 ± 2.12 | 81.5 ± 2.94 | 10.2 ± 0.67 |
c | 76.65 ± 2.38 | 74.95 ± 1.46 | −0.17 ± 0.06 | −0.40 ± 0.04 | 0.23 ± 0.06 | 0.73 ± 0.14 | 76.6 ± 2.65 | 74.9 ± 2.45 | 1.8 ± 0.27 |
d | 71.99 ± 2.23 | 77.72 ± 1.77 | 0.45 ± 0.09 | −0.10 ± 0.01 | 2.53 ± 0.14 | 2.22 ± 0.19 | 71.9 ± 2.71 | 77.6 ± 2.38 | 5.8 ± 0.38 |
Time (d) | Control | Silver Permutite | Zinc Permutite | Silver/Zinc Permutite | Silver/Zinc p-CEO | |||||
---|---|---|---|---|---|---|---|---|---|---|
A | P | A | P | A | P | A | P | A | P | |
1 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 |
2 | 2 | 2 | 1 | 2 | 1 | 2 | 1 | 2 | 0 | 0 |
3 | 3 | 3 | 2 | 2 | 2 | 3 | 1 | 2 | 0 | 0 |
4 | 4 | 4 | 2 | 3 | 3 | 3 | 2 | 3 | 0 | 0 |
5 | 4 | 4 | 3 | 4 | 3 | 4 | 2 | 3 | 0 | 0 |
Simulants | Ions Migrate from Ag+/Zn2+-Permutite/CEO Antibacterial Pads (mg/L) | ||
---|---|---|---|
Ag+ | Zn2+ | Al3+ | |
Water | 0.04330 ± 0.002 | 0.9420 ± 0.005 | ND |
Limit value | 0.5 | 25 | 0.2 |
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Niu, B.; Yan, Z.; Shao, P.; Kang, J.; Chen, H. Encapsulation of Cinnamon Essential Oil for Active Food Packaging Film with Synergistic Antimicrobial Activity. Nanomaterials 2018, 8, 598. https://doi.org/10.3390/nano8080598
Niu B, Yan Z, Shao P, Kang J, Chen H. Encapsulation of Cinnamon Essential Oil for Active Food Packaging Film with Synergistic Antimicrobial Activity. Nanomaterials. 2018; 8(8):598. https://doi.org/10.3390/nano8080598
Chicago/Turabian StyleNiu, Ben, Zhipeng Yan, Ping Shao, Ji Kang, and Hangjun Chen. 2018. "Encapsulation of Cinnamon Essential Oil for Active Food Packaging Film with Synergistic Antimicrobial Activity" Nanomaterials 8, no. 8: 598. https://doi.org/10.3390/nano8080598