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Article

Machine Learning-Enhanced Nanoindentation for Characterizing Micromechanical Properties and Mineral Control Mechanisms of Conglomerate

1
Xinjiang Petroleum Administration Bureau, Research Institute of Oil Production Technology, Karamay 83400, China
2
National Key Laboratory of Petroleum Resources and Engineering, China University of Petroleum (Beijing), Beijing 102249, China
3
Xinjiang Key Laboratory of Intelligent Petroleum Exploration and Engineering, Karamay 83400, China
*
Author to whom correspondence should be addressed.
Appl. Sci. 2025, 15(17), 9541; https://doi.org/10.3390/app15179541 (registering DOI)
Submission received: 4 August 2025 / Revised: 25 August 2025 / Accepted: 26 August 2025 / Published: 29 August 2025
(This article belongs to the Section Energy Science and Technology)

Abstract

Conglomerate reservoirs present significant technical challenges during drilling operations due to their complex mineral composition and heterogeneous characteristics, yet the quantitative relationships between mineral composition and microscopic mechanical behavior remain poorly understood. To elucidate the variation patterns of conglomerate micromechanical properties and their mineralogical control mechanisms, this study develops a novel multi-scale characterization methodology. This approach uniquely couples nanoindentation technology, micro-zone X-ray diffraction analysis, and machine learning algorithms to systematically investigate micromechanical properties of conglomerate samples from different regions. Hierarchical clustering algorithms successfully classified conglomerate micro-regions into three lithofacies categories with distinct mechanical differences: hard (elastic modulus: 81.90 GPa, hardness: 7.83 GPa), medium-hard (elastic modulus: 54.97 GPa, hardness: 3.87 GPa), and soft lithofacies (elastic modulus: 25.21 GPa, hardness: 1.15 GPa). Correlation analysis reveals that quartz (SiO2) content shows significant positive correlation with elastic modulus (r = 0.52) and hardness (r = 0.51), while clay minerals (r = −0.37) and plagioclase content (r = −0.48) exhibit negative correlations with elastic modulus. Mineral phase spatial distribution patterns control the heterogeneous characteristics of conglomerate micromechanical properties. Additionally, a random forest regression model successfully predicts mineral content based on hardness and elastic modulus measurements with high accuracy. These findings bridge the gap between microscopic mineral properties and macroscopic drilling performance, enabling real-time formation strength assessment and providing scientific foundation for optimizing drilling strategies in heterogeneous conglomerate formations.
Keywords: conglomerate reservoir; nanoindentation technology; micromechanical properties; mineral composition; clustering analysis; random forest conglomerate reservoir; nanoindentation technology; micromechanical properties; mineral composition; clustering analysis; random forest

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MDPI and ACS Style

Guo, Y.; Zhang, W.; Li, P.; Zhao, Y.; Mu, Z.; Yang, Z. Machine Learning-Enhanced Nanoindentation for Characterizing Micromechanical Properties and Mineral Control Mechanisms of Conglomerate. Appl. Sci. 2025, 15, 9541. https://doi.org/10.3390/app15179541

AMA Style

Guo Y, Zhang W, Li P, Zhao Y, Mu Z, Yang Z. Machine Learning-Enhanced Nanoindentation for Characterizing Micromechanical Properties and Mineral Control Mechanisms of Conglomerate. Applied Sciences. 2025; 15(17):9541. https://doi.org/10.3390/app15179541

Chicago/Turabian Style

Guo, Yong, Wenbo Zhang, Pengfei Li, Yuxuan Zhao, Zongjie Mu, and Zhehua Yang. 2025. "Machine Learning-Enhanced Nanoindentation for Characterizing Micromechanical Properties and Mineral Control Mechanisms of Conglomerate" Applied Sciences 15, no. 17: 9541. https://doi.org/10.3390/app15179541

APA Style

Guo, Y., Zhang, W., Li, P., Zhao, Y., Mu, Z., & Yang, Z. (2025). Machine Learning-Enhanced Nanoindentation for Characterizing Micromechanical Properties and Mineral Control Mechanisms of Conglomerate. Applied Sciences, 15(17), 9541. https://doi.org/10.3390/app15179541

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