1. Introduction
Although selective laser melting (SLM) has many significant advantages, such as capability of producing complex designs, effective material usage, short total manufacturing time, etc., it cannot be ignored that the surface quality of SLMed parts is generally poor and difficult to control, which is also one of main factors that restricts the development and application of SLM [
1,
2]. Poor surface roughness not only affects the dimensional accuracy of parts [
3], but also causes cracks in parts, thus seriously affecting the service life of parts [
4]. At present, the surface quality of parts fabricated by SLM is mostly improved by post-processing, but the structure of SLM parts is generally complex, especially for the parts with curved surfaces and inner holes, which are difficult to be polished by traditional means. Recently, some researchers used abrasive flow machining (AFM) and magnetic abrasive finishing (MAF) to polish the complex surface of SLMed parts and obtained satisfactory results. Mohammadian et al. [
5] developed a combined-chemical abrasive flow polishing method for Inconel 625 parts prepared by SLM, and the surface roughness (
Ra) with an inclination of 15° was improved by 43% after polishing for 1 h. Zhang et al. [
6] used magnetic abrasives to polish SLMed 316L stainless steel, with the surface roughness (
Ra) decreased by 75.7% at most. Although it has been proved that these subsequent polishing methods have positive effects on improving the surface quality, these subsequent processing steps further extend the manufacturing cycle and significantly increase production costs. Therefore, improving the surface quality of parts by optimizing SLM process parameters is of great significance to reduce post-treatment steps and production costs.
According to the technical characteristics of SLM layer-by-layer manufacturing, the surface of SLMed parts can be divided into several categories, as shown in
Figure 1. The surface parallel to the substrate and facing up is referred to as the top surface [
7], and the plane perpendicular to the substrate is called the vertical surface [
8]. In addition, according to the inclination angle between the targeted surface and substrate, the inclined surface can be divided into the upskin (>90°) and the downskin (<90°) [
9]. Finally, the suspended surface that is parallel to the substrate and directly in contact with powders is referred to as the lower surface [
10]. The processing of top surface and lower surface belongs to core scanning, which is related to the laser power, laser scanning speed, and hatch spacing. The vertical surface is superposed by the edge of each layer, and its quality is only related to the process parameters of the contour. However, for the upskin and downskin, both core and contour process parameter make a difference to the surface quality, among which the contour process parameter is more influential. Furthermore, owing to the stair step-effect [
11], the inclination angle also can impact the surface quality of the upskin and downskin.
In recent years, many investigations related with the surface of SLMed parts were reported. The relatively flat top surface is manufactured mainly by selecting a continuous, straight single track with appropriate hatch spacing. In addition, the laser remelting process is generally used to greatly improve the quality of the top surface [
3,
12,
13,
14,
15]. With regard to the vertical surface, Mumtaz et al. [
8] achieved the desired surface roughness by increasing the scanning speed of the contour to limit the thermal variation in the molten pool and control the stability of the scanning. Tao Yang et al. [
4] studied the effect of linear energy density of the contour on the vertical roughness of AlSi10Mg parts fabricated by SLM. The results showed that the low linear energy density tends to cause spheroidization, and the high linear energy density would give rise to the instability of the molten pool, resulting in a “fluctuating” structure. The roughness of vertical surface was reduced from 15 μm to 4 μm by process optimization. With respect to of the upskin and downskin surface, Tian et al. [
16] investigated the impact of process parameters of the contour on the roughness of Hastelloy X alloy parts built by SLM. Their conclusions indicated that the laser power and scanning speed have little effect on the upskin roughness, whereas the downskin roughness will dramatically increase with increasing laser power or decreasing scanning speed due to the fact that a larger melt pool will protrude outward and entrain surrounded powders. Xiang et al. [
17] found that the quality of the downskin is significantly worse than that of the upskin in SLMed parts of 316L stainless steel, and its roughness noticeably increased with the decrease of the inclination angle. Wang et al. [
18] reported that increasing the scanning speed can suppress the slag hanging on the downskin of SLMed 316L parts, thus enhancing the formability of overhanging structures.
The downskin with an inclination angle of 0° is the lower surface. Because it is formed on a complete powder bed, the thermophysical process is more complicated, and the process parameter optimization is more difficult. Thus, the research on the lower surface is very limited at present. Mertens et al. [
10] investigated the influence of laser power on the quality of AlSi10Mg overhanging structures manufactured by SLM. Their results revealed that the lower laser power could avoid the formation of large agglomerations and improve the quality of the lower surface but would lead to more pores in the lower surface area and a density reduction of parts. Saunders [
19] concluded that the parts manufactured by SLM include bulk regions and different types of surfaces. High density, high efficiency, and good material properties should be pursued when manufacturing the bulk regions, but surface manufacturing is different, in that it is necessary to consider avoiding distortion and dross. Therefore, it is necessary to further study how to not only maintain the density of parts, but also improve the quality of the lower surface. In addition, the influence of the scanning strategies (e.g., the effective remelting strategy to improve the quality of the top surface) on the quality of the lower surface is also noteworthy.
This work mainly focuses on the quality of the lower surface of TA15 titanium alloy fabricated by SLM. As a common titanium alloy used in aerospace, TA15 has excellent mechanical properties at room and high temperatures. Furthermore, the aerospace field has relatively stringent requirements on the surface quality of parts; therefore it is necessary to optimize the lower surface quality of TA15 fabricated by SLM. In this paper, the influence of process parameters and scanning strategies on the quality of the lower surface in SLMed TA15 parts is investigated by measuring the roughness of the lower surface, recording the cooling time of the molten pool during the lower surface manufacturing process, and observing the lower surface morphology. The results obtained in this study can increase the understanding of the manufacturing mechanism of the lower surface and have certain guiding significance for optimizing the quality of the lower surface of SLM manufacturing parts.
3. Results
The macroscopic morphology of all overhanging structure samples is shown in
Figure 4. From
Figure 4 it can be seen that the formation qualities of the overhanging structure varied greatly with different process parameters of the lower surface. When the core processing parameters and scanning strategy I were used to manufacture the lower surface of the overhanging parts, the slag hanging on the lower surface of 1-I sample was very serious, and the overhanging feature was almost invisible. This serious slag hanging also appeared on the 2-I sample. Compared with 1-I and 2-I, the slag hanging condition of 1-II and 2-II samples with strategy II were reduced, and the overhanging feature of these two samples could be seen. With the decrease of the laser energy density, the amount of slag hanging on the lower surface of the samples manufactured by the two scanning strategies gradually decreased, and the overhanging structure feature became more and more obvious. In addition, it could be seen that the lower surface of the sample gradually became flatter from the inclined and irregular surface. Among all the samples, the overhanging surface of the 8-I sample was the smoothest without obvious slag hanging. However, it is worth noting that, contrary to the phenomenon that the slag hanging on the lower surface of sample No. 1 would decrease when the scanning strategy II was adopted, the slag hanging on the lower surface of sample No. 8 appeared clearly when the scanning strategy II was adopted. With the continuous decreasing of laser energy density, the slag hanging on the lower surface of No. 9 and No. 10 samples with the two scanning strategies became more pronounced.
Figure 5 shows the variation trend of the overhanging section thickness and the lower surface roughness of all samples with the laser surface energy density, respectively. The thickness of the overhanging section reflected the slag hanging on the lower surface of the samples. The greater the thickness, the more serious the slag hanging was. The lower surface roughness
Sa and
Sz directly reflected the quality of the lower surface of the sample. In
Figure 5, it can be seen that the overhanging section thickness and the lower surface roughness
Sa and
Sz showed the same trend, which decreased first and then increased with reduction of the
EF. In the case of scanning strategy I, the sample with the maximum thickness and roughness was the sample 1-I with almost invisible overhanging features. However, in the case of scanning strategy II, the sample with the largest thickness was sample 1-II, while the sample with the largest roughness was sample 10-II. This indicated that in the case of scanning strategy II, the
EF of lower surface reduction was likely to obtain a worse surface than when the core process was directly used to form the lower surface. The minimum thickness and roughness of the strategy I and strategy II appeared near the
EF of 0.6 J/mm
2 and 1.1 J/mm
2, respectively. The corresponding samples were 8-I and 6-II respectively. These two samples were also samples with less slag hanging on the lower surface and relatively flat lower surface. It is worth noting that the thickness and roughness of strategy II was lower than that of strategy I at high
EF, but when
EF went down to about 1.0 J/mm
2, the variation trend of the thickness and roughness was converse. This shows that the influence of scanning strategy on the quality of the lower surface was dynamic. When the
EF was different, the scanning strategy played a different role. The thickness of the overhanging section and the roughness of the lower surface showed a similar trend with the change of
EF, indicating that there was a certain positive correlation between them. However, it can be seen from the
Figure 5 that the roughness varied more widely than the thickness.
In order to further analyze the influence of process parameters and scanning strategies on the quality of the lower surface, the lower surface morphology of samples with highest and lowest
EF was observed.
Figure 6 shows the morphology of the lower surface of sample 1 and 10 with two different scanning strategies. The white arrow in the figure represents the building direction, and the groove area between the red edges is the lower surface of the overhanging structures. In
Figure 6a, the “valley-like” characteristics can be seen around the entire surface, and the lower surface of sample 1-I is very rough with the roughness
Sa and
Sz reaching to 97.33 μm and 887.38 μm, respectively. In comparison, the lower surface quality of sample 1-II without cross-melting was significantly improved with the “valley-like” features disappearing, but the surface fluctuations were still obvious with an
Sa of 71.56 μm and
Sz of 658.5 μm. As seen in
Figure 6c,d, it is clear that sample 10 with the smallest
EF had a more distinct and clear overhanging structure outline compared to the sample 1-I. The lower surface of sample10-I was flatter, with an
Sa of 48.72 μm, and only included some slight fluctuations. However, the lower surface of sample 10-II was more rough and had a huge pit, as shown in the red square line in
Figure 6d. Therefore, the roughness
Sa and
Sz of sample 10-II reached 76.41 μm and 801.2 μm, respectively, which were the maximum values of all the samples adopted in strategy II. In conclusion, strategy II can indeed improve the quality of the lower surface to some extend at high
EF; however, with low
EF applied, this strategy conversely deteriorates the lower surface quality.
Figure 7 shows the lower surface morphology of sample 8-I (a,c) and 6-II (b,d). The two samples were the samples with best lower surface quality when the scanning strategy I and II were adopted, respectively. It was found that the lower surfaces of both samples were relatively flat without obvious fluctuations (
Figure 7a,b), and the corresponding roughness
Sa was 27.17 μm and 31.71 μm, respectively. By observing the SEM images (
Figure 7c,d), the difference between the two surfaces can be seen more clearly. There are a large number of powder particles adhering to the lower surface of both samples. In comparison, the surface of the 6-II sample had some protruding molten pool tracks and pits, while the surface of the 8-I sample was smoother. This is also the reason why the
Sz value (370.68 μm) of sample 6-II was significantly higher than that of sample 8-I (251.82 μm).
4. Discussion
The processing of the lower surface is carried out on a powder bed made up entirely of loose powder. On the one hand, the change of processing parameters will inevitably affect the melting of the powder, which will lead to the different quality of the lower surface. On the other hand, the difference of the thermal conduction mechanism between the powder bed and the solidified part will also have additional influence on the lower surface. As is well-known, the thermal conductivity of metal powder is much lower than that of metal solid [
29,
30], so the heat generated by laser dissipates slowly on the powder bed, which will easily lead to the heat accumulation, thus causing the cooling rate of the molten pool to slow down. The cooling process of the molten pool can be clearly displayed by the video recording during the processing of the lower surface.
As seen in
Figure 8a–d, the cooling process of the molten pool was recorded at 30 fps by an Mi8-phone (Beijing Xiaomi Technology Co. LTD, Beijing, China) when the first layers of the lower surfaces of samples 1-I, 1-II, 10-I, and 10-II were processed, respectively. Each figure consists of several frames. Each frame represents a time of 1/30 s, which means that the cooling time of the molten pool can be estimated by the number of frames. It can be seen from
Figure 8 that the heat dissipation on the powder bed is a slow and continuous process. The cooling process of the molten pool of the 1-I sample with the highest
EF takes about 0.43 s. The cooling time of the molten pool will be significantly shortened by reducing the laser energy input density. The cooling time of the molten pool of sample 10-I is only 0.17 s. Different scanning strategies will also cause changes in the cooling time of the molten pool. Compared with the cross-remelting strategy, the cooling times of sample 1-II and 10-II without remelting are reduced to 0.3 s and 0.1 s, respectively, due to the reduction of additional heat accumulation caused by remelting.
The cooling time of the molten pool during the processing of the first layer of the lower surface and the first layer of the core of all the samples is shown in
Table 3. As can be seen from
Table 3, when the first layer of the lower surface is processed, the cooling time of the molten pool is gradually shortened with the reduction of the
EF. However, when the first layer of core is processed after the processing of the lower surface, the cooling time of the molten pool of the core gradually increases with the decrease of the
EF of the lower surface. This is due to the decrease of
EF, which leads to the increase of unmelted powders and pores in the lower surface area, resulting in the decrease of density and the gradual decrease of heat dissipation performance from metal solid to metal powders.
The forming process of the lower surface can be described more clearly by the cooling time of the molten pool. When the
EF for lower surface processing is relatively high, such as in the 1-I sample, the laser can fully melt the metal powder and the volume of the molten pool gets large. In addition, the heat accumulation caused by slow heat dissipation in the powder layer further increases the volume of the molten pool. Under the action of gravity and capillary forces [
9], the molten pool continuously sinks on the powder bed, forming the “valley-like” features as displayed in
Figure 6a. This phenomenon can be seen more obviously from the cross-sectional pictures of the overhanging structures.
Figure 9a–f shows the cross-sectional pictures of some representative overhanging structural parts. The large-sized agglomerate can be observed distinctly on the lower surface in sample 1-I (
Figure 9a), which leads to poor surface quality. The schematic diagram of the molten pool sinking is described in
Figure 10a.
The reduction of the
EF will decrease the maximum temperature of the molten pool [
30] and its cooling time, so that the volume of the molten pool is effectively diminished and the molten pool subsidence is retrained to some extent, which ultimately improves the dimensional deviation and poor lower surface quality. However, when the
EF is too low, it will lead to the lack of powder fusion or incomplete powder melting [
31]. A large amount of unmelted powder cannot provide a good support and heat dissipation platform for the subsequent core forming. Taking sample 10-II as an example, it can be seen from
Table 3 that the cooling time of the molten pool reached 0.2 s when the first layer of the core was processed. Due to the accumulation of heat, a similar phenomenon of molten pool sinking occurs compared to the case of the lower surface forming of sample 1-I, resulting in the large-scale slag hanging as shown in
Figure 9f. At the same time, due to the lack of powder fusion in the lower surface area and the molten pool generated by the core not being enough to fill the entire lower surface area, the result is the occurrence of irregular pores and the large-sized pits after the powder spalling. This forming process can be described as shown in
Figure 10c. The forming quality of the lower surface can be effectively judged by the cooling time of the molten pool when the first layer of the core is processed. The shorter the cooling time of the molten pool is, the higher the density of the lower surface region is.
The moderate
EF is beneficial to the forming of the lower surface. For the sample 8-I with moderate
EF on the lower surface, the volume of molten pool is small, which will not cause serious sinking. At the same time, sufficient
EF ensures the necessary metallurgical bonding, which results in a relatively dense metal solid in the lower surface region and provides a good heat dissipation platform for core forming. This can be proven by the fact that the cooling time of the molten pool is only 0.07 s when the first layer of the core is processed. By this way, the negative impact of the core forming on the quality of the lower surface can be avoided, which ultimately results in a smooth lower surface with optimal roughness and relatively best forming accuracy, as shown in
Figure 9b. Inevitably, due to the thermal influence of the molten pool, a large number of powder particles will adhere to the lower surface, which is displayed in
Figure 10b.
In addition, the different scanning strategies will also have a direct impact on the forming of the lower surface. Rashid et al. [
22] found that the strategy of scanning the same layer twice resulted in a very high amount of heat energy accumulation. Therefore, when a high
EF is applied, the strategy II with non-remelting can effectively reduce the density of laser energy input, decrease the cooling time of molten pool, and suppress the agglomeration phenomenon, thus improving the quality of the lower surface of parts. As revealed in
Figure 9a,d, the agglomeration size on the lower surface of sample 1-II is significantly smaller than that of sample 1-I, which is the reason why the lower surface roughness of sample 1-II is better than that of sample 1-I. However, when the
EF is low, the strategy I with cross-remelting can help reduce the metallurgical defects and improve the quality of the lower surface of the parts. As shown in
Figure 9b,c,e,f, compared with sample 8-II, the agglomeration size of the lower surface of sample 8-I is greatly reduced with metallurgical defects almost disappeared, and the surface quality is improved. The same is true of sample 10-I as compared with sample 10-II.