Evaluation of Mango Kernel Seed (Mangifera indica) Oil as Cutting Fluid in Turning of AISI 1525 Steel Using the Taguchi-Grey Relation Analysis Approach
Abstract
:1. Introduction
2. Methodology
2.1. Seed Samples Description
2.2. Oil Extraction Process
2.3. Characterization of Crude Oil Extracts
2.4. Formulation of Cutting Fluids Emulsion
2.5. Evaluation of pH of Emulsion Cutting Fluids
2.6. Machining Operations
2.7. Determination of Surface Roughness
2.7.1. Determination of Cutting Temperature
2.7.2. Determination of Machine Vibration
2.7.3. Determination of Machine Sound Level
3. Results and Discussion
3.1. Phytochemical Characterization of MKSO Extracts
3.2. Physiochemical and Thermal Properties Characterization of MKSO Extracts
3.3. Experimental Results for AISI 1525 Steel Machining with Emulsion Cutting Fluids
3.4. Grey Relational Analysis
3.5. Application of Grey Relation Analysis to Obtain Multiple Responses Parametric Optimizations
3.6. Mathematical Model
4. Conclusions
- MKSO extracts were found to be enriched in four compounds: cis-vaccenic acid, hexadecanoic acid, 3-pentadactyl phenol, and squalene.
- MOCF outperformed MKSO by a significant margin in most conditions considered.
- The spindle speed of 0.683 rev/min, feed of 0.617 mm/rev, and depth of cut of 0.620 mm are the optimal characteristics for mango kernel seed oil, while 0.7898 rev/min spindle speed, 0.6483 mm/rev feed, and 0.6373 mm depth of cut are the best specifications for MOCF cutting fluid.
- Spindle speed had the greatest influence on multi-responses in turning operations with both cutting fluids.
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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S/N | Parameter | Methodology |
---|---|---|
1 | Fourier transform infrared analysis | This was determined by using a PerkinElmer FT-IR Spectrum in the 4000–400 cm−1 range. The precision was eight and two scans. Sample extracts were spread on KBR cells, inserted into the cell holder, and placed in the FT-IR spectrophotometer |
2 | Gas chromatography | This was obtained with a combined 7890A Agilent Technology GC system. During the process, oil was split into its chemical constituents. The column features of this machinery are as follows: HP5MS, 30 m × 0.320 mm, 0.25 m width, helium carrier gas, and 2.5 mL/min flow rate. At a rate of 10 °C/min, the temperature range was configured between 80 and 280 °C. The splitless injector and detector were kept at 250 and 200 °C, respectively. |
3 | Crude oil pH | A digital pH meter was used to determine the pH of raw mango oil. |
4 | Specific gravity | This was obtained based on ASTM D287 procedure and was further calculated using Equation (1) [20]. |
5 | % Oil yield | The percentage oil yield was calculated using Equation (2). |
6 | Viscosity | This was determined using an Oswald kinematic viscometer in the temperature range of 40–80 °C, and was further evaluated using Equation (3). |
7 | Oil color | The color of the oil was evaluated using a spectrophotometer and the Cc 13c -50 AOCS standard technique was adopted. |
8 | Pour point | This was examined with a Stanhope–Seta pour and cloud point KT16 8AP machinery based on ASTM D97 standards [21]. |
9 | Cloud point | This was measured with Stanhope–Seta cloud/pour point KT16 8AP machinery and carried out according to ASTM D2500 [22]. |
10 | Flashpoint | The flashpoint was measured by using an ASTM D92 conventional method [23]. |
11 | Fire point | This was measured according to the ASTM D92 method with a Pensky–Martens setup. |
Assay No | A (mL) | B (mL) | C (mL) | D (mL) | Vol. of Water (mL) |
---|---|---|---|---|---|
1 | 8 | 1 | 0.5 | 0.5 | 70 |
2 | 12 | 1 | 0.5 | 0.5 | 66 |
3 | 8 | 2 | 0.5 | 0.5 | 69 |
4 | 12 | 2 | 0.5 | 0.5 | 65 |
5 | 8 | 1 | 1.0 | 0.5 | 69.5 |
6 | 12 | 1 | 1.0 | 0.5 | 65.5 |
7 | 8 | 2 | 1.0 | 0.5 | 68.5 |
8 | 12 | 2 | 1.0 | 0.5 | 64.5 |
9 | 8 | 1 | 0.5 | 1.0 | 69.5 |
10 | 12 | 1 | 0.5 | 1.0 | 65.5 |
11 | 8 | 2 | 0.5 | 1.0 | 68.5 |
12 | 12 | 2 | 0.5 | 1.0 | 64.5 |
13 | 8 | 1 | 1.0 | 1.0 | 69 |
14 | 12 | 1 | 1.0 | 1.0 | 65 |
15 | 8 | 2 | 1.0 | 1.0 | 68 |
16 | 12 | 2 | 1.0 | 1.0 | 64 |
Trial No. | Cutting Parameter | ||
---|---|---|---|
Spindle Speed (rev/min) | Feed Rate (mm/rev) | Depth of Cut (mm) | |
1 | 355 | 0.1 | 0.75 |
2 | 355 | 0.15 | 1.00 |
3 | 355 | 0.20 | 1.25 |
4 | 500 | 0.1 | 1.00 |
5 | 500 | 0.15 | 1.25 |
6 | 500 | 0.20 | 0.75 |
7 | 710 | 0.1 | 1.25 |
8 | 710 | 0.15 | 0.75 |
9 | 710 | 0.20 | 1.00 |
Oil | Chromatography Peak | Compound Nomenclature | Molecular Formula | Molecular Weight | Retention Time (min) | Percentage Content |
---|---|---|---|---|---|---|
1 | cis-vaccenic acid | C18H34O2 | 282 | 19.822 | 55.28 | |
Mango kernel seed oil | 2 | n-hexadecanoic acid | C16H32O2 | 256 | 17.627 | 38.76 |
3 | 3-pentadecyl phenol | C21H36O | 304 | 26.488 | 4.18 | |
4 | Squalene | C30H50 | 410 | 29.898 | 2.51 |
Parameter | Result |
---|---|
pH | 6.5 |
Specific gravity | 0.833 |
% Oil yield | 12.5 |
Viscosity | 16.8 cP |
Oil color | Brownish Yellow |
Pour point | 36 |
Cloud point | 39 |
Flashpoint | 158 |
Fire point | 167 |
Element | % Composition |
---|---|
C | 0.2505 |
Si | 0.2215 |
Mn | 1.2340 |
S | 0.0235 |
P | 0.0135 |
Cr | 0.1135 |
Ni | 0.1155 |
Cu | 0.0480 |
Al | 0.0120 |
Ti | 0.0395 |
Fe | 97.9285 |
Properties | Result |
---|---|
Tensile Strength | 604.74 MPa |
Yield Strength | 7599.34 MPa |
Elastic Modulus | 35106.19MPa |
Energy at Maximum Tensile Stress | 31.24909 J |
Energy at Break | 47.35634 J |
Spindle Speed (rev/min) | Feed Rate (mm/rev) | Depth of Cut (mm) | Surface Roughness (µm) | Cutting Temp. (°C) | Sound Level (dB) | Machine Vibration (m/s2) |
---|---|---|---|---|---|---|
355 | 0.1 | 0.75 | 2.53 | 36.7 | 96.5 | 14.5 |
355 | 0.15 | 1 | 3.73 | 55.8 | 102.5 | 25.42 |
355 | 0.2 | 1.25 | 9.01 | 50.2 | 106.1 | 51.7 |
500 | 0.1 | 1 | 6.35 | 57.2 | 106.2 | 43.9 |
500 | 0.15 | 1.25 | 8.65 | 51.8 | 106.3 | 31.7 |
500 | 0.2 | 0.75 | 8.83 | 68.9 | 103.1 | 45.2 |
710 | 0.1 | 1.25 | 6.29 | 82.7 | 103.9 | 61.4 |
710 | 0.15 | 0.75 | 7.84 | 49.4 | 105.4 | 59.8 |
710 | 0.2 | 1 | 9.63 | 50.5 | 105.9 | 67.8 |
Spindle Speed (rev/min) | Feed Rate (mm/rev) | Depth of Cut (mm) | Surface Roughness (µm) | Cutting Temp. (°C) | Sound Level (dB) | Machine Vibration (m/s2) |
---|---|---|---|---|---|---|
355 | 0.1 | 0.75 | 2.545 | 46.8 | 85.7 | 27.03 |
355 | 0.15 | 1 | 3.521 | 57.2 | 85.9 | 7.91 |
355 | 0.2 | 1.25 | 8.47 | 59.8 | 86 | 28.7 |
500 | 0.1 | 1 | 6.22 | 76.6 | 85.7 | 15.5 |
500 | 0.15 | 1.25 | 7.41 | 60.2 | 95.5 | 42.9 |
500 | 0.2 | 0.75 | 8.83 | 105.5 | 108.8 | 21.4 |
710 | 0.1 | 1.25 | 6.5 | 106.2 | 106.9 | 29.2 |
710 | 0.15 | 0.75 | 7.7 | 109.2 | 111.1 | 12.9 |
710 | 0.2 | 1 | 8.8 | 111.8 | 109 | 29.95 |
Step | Action |
---|---|
1. | To avoid using different units and to reduce variability, the data must first be standardized. It is generally required since the variation of one datum differs from other data. The array is made between 0 and 1 by calculating an appropriate value from the original value [37]. It is a way of converting original data to equivalent data in general. If the response is to be reduced, Equation (5) is used to normalize it into an appropriate range using smaller-is-better characteristics. From the relation, j = 1, …, u; n = 1, …, q; n is the number of responses, while p is the number of experimental results. yj (n) represents the real series, max yj (n) represents the highest value of yj (n), min yj (n) represents the lowest value of yj (n), y*j (n) represents the series after the result pre-processing, and y is the desired value [37]. |
2. | Equation (6) is used to compute the Grey relational coefficient, , from the normalized data. The in the equation is divergence series of the reference series and the comparability series and . refers to the reference series and is known as comparability series. χmax and χmin are the maximum and minimum values of the absolute differences χoj of all series being compared. is a distinguishing coefficient and ranges between 0 and 1. Most times, the value of is 0.5. |
3. | The Grey relational grade (GRG) is calculated with Equation (7). From the equation, is the necessary GRG for th trial and = no. of response characteristics. The GRG denotes the level of correlation between the comparability series and the reference series and is the all-encompassing representation of all qualitative attributes [37]. Therefore, using GRA and the Taguchi technique, the multiple response optimization models is reduced to just one response optimization model. |
4. | Then, using a higher GRG, an appropriate level of process variables is obtained, indicating the greater quality of the product. To determine this, the mean grade values for individual level of process parameters are to be obtained, which can be shown as a mean response chart. From the mean response chart, the greater value of mean grade values is selected as the best parametric combination for multiple responses. |
5. | After determining the best combination, the analysis of variance (ANOVA) is used to find the major parameters affecting the multiple responses at a 95% confidence level, providing useful information on the experimental results. Since the Taguchi technique cannot assess the influence of each parameter on multiple responses, the ANOVA will be useful in determining the percentage of contribution to evaluate the influence. The ANOVA approach divides the entire variability of the output (sum of squared deviations around the weighted score) into contributions from each parameter and error [37]. |
Spindle Speed (rev/min) | Feed Rate (mm/rev) | Depth of Cut (mm) | Surface Roughness (µm) | Cutting Temp. (°C) | Sound Level (dB) | Machine Vibration (m/s2) |
---|---|---|---|---|---|---|
355 | 0.1 | 0.75 | 2.53 | 36.7 | 96.5 | 14.5 |
355 | 0.15 | 1 | 3.73 | 55.8 | 102.5 | 25.42 |
355 | 0.2 | 1.25 | 9.01 | 50.2 | 106.1 | 51.7 |
500 | 0.1 | 1 | 6.35 | 57.2 | 106.2 | 43.9 |
500 | 0.15 | 1.25 | 8.65 | 51.8 | 106.3 | 31.7 |
500 | 0.2 | 0.75 | 8.83 | 68.9 | 103.1 | 45.2 |
710 | 0.1 | 1.25 | 6.29 | 82.7 | 103.9 | 61.4 |
710 | 0.15 | 0.75 | 7.84 | 49.4 | 105.4 | 59.8 |
710 | 0.2 | 1 | 9.63 | 50.5 | 105.9 | 67.8 |
Min | 2.53 | 36.7 | 96.5 | 14.5 | ||
Max | 9.63 | 82.7 | 106.3 | 67.8 |
Spindle Speed (rev/min) | Feed Rate (mm/rev) | Depth of Cut (mm) | Surface Roughness (µm) | Cutting Temp. (°C) | Sound Level (dB) | Machine Vibration (m/s2) |
---|---|---|---|---|---|---|
355 | 0.1 | 0.75 | 2.545 | 46.8 | 85.7 | 27.03 |
355 | 0.15 | 1 | 3.521 | 57.2 | 85.9 | 7.91 |
355 | 0.2 | 1.25 | 8.47 | 59.8 | 86 | 28.7 |
500 | 0.1 | 1 | 6.22 | 76.6 | 85.7 | 15.5 |
500 | 0.15 | 1.25 | 7.41 | 60.2 | 95.5 | 42.9 |
500 | 0.2 | 0.75 | 8.83 | 105.5 | 108.8 | 21.4 |
710 | 0.1 | 1.25 | 6.5 | 106.2 | 106.9 | 29.2 |
710 | 0.15 | 0.75 | 7.7 | 109.2 | 111.1 | 12.9 |
710 | 0.2 | 1 | 8.8 | 111.8 | 109 | 29.95 |
Min | 2.545 | 46.8 | 85.7 | 7.91 | ||
Max | 8.83 | 111.8 | 111.1 | 42.9 |
Normalization | |||
---|---|---|---|
Surface Roughness (µm) | Cutting Temp. (°C) | Sound Level (dB) | Machine Vibration (m/s2) |
1.000 | 1.000 | 1.000 | 1.000 |
0.831 | 0.585 | 0.388 | 0.795 |
0.087 | 0.707 | 0.020 | 0.302 |
0.462 | 0.554 | 0.010 | 0.448 |
0.138 | 0.672 | 0.000 | 0.677 |
0.113 | 0.300 | 0.327 | 0.424 |
0.470 | 0.000 | 0.245 | 0.120 |
0.252 | 0.724 | 0.092 | 0.150 |
0.000 | 0.700 | 0.041 | 0.000 |
Normalization | |||
---|---|---|---|
Surface Roughness (µm) | Cutting Temp. (°C) | Sound Level (dB) | Machine Vibration (m/s2) |
1.000 | 1.000 | 1.000 | 0.454 |
0.845 | 0.840 | 0.992 | 1.000 |
0.057 | 0.800 | 0.988 | 0.406 |
0.415 | 0.542 | 1.000 | 0.783 |
0.226 | 0.794 | 0.614 | 0.000 |
0.000 | 0.097 | 0.091 | 0.614 |
0.371 | 0.086 | 0.165 | 0.392 |
0.180 | 0.040 | 0.000 | 0.857 |
0.005 | 0.000 | 0.083 | 0.370 |
Surface Roughness (µm) | Cutting Temp. (°C) | Sound Level (dB) | Machine Vibration (m/s2) |
---|---|---|---|
0.000 | 0.000 | 0.000 | 0.000 |
0.169 | 0.415 | 0.612 | 0.205 |
0.913 | 0.293 | 0.980 | 0.698 |
0.538 | 0.446 | 0.990 | 0.552 |
0.862 | 0.328 | 1.000 | 0.323 |
0.887 | 0.700 | 0.673 | 0.576 |
0.530 | 1.000 | 0.755 | 0.880 |
0.748 | 0.276 | 0.908 | 0.850 |
1.000 | 0.300 | 0.959 | 1.000 |
Surface Roughness (µm) | Cutting Temp. (°C) | Sound Level (dB) | Machine Vibration (m/s2) |
---|---|---|---|
0.000 | 0.000 | 0.000 | 0.546 |
0.155 | 0.160 | 0.008 | 0.000 |
0.943 | 0.200 | 0.012 | 0.594 |
0.585 | 0.458 | 0.000 | 0.217 |
0.774 | 0.206 | 0.386 | 1.000 |
1.000 | 0.903 | 0.909 | 0.386 |
0.629 | 0.914 | 0.835 | 0.608 |
0.820 | 0.960 | 1.000 | 0.143 |
0.995 | 1.000 | 0.917 | 0.630 |
Surface Roughness (µm) | Cutting Temp. (°C) | Sound Level (dB) | Machine Vibration (m/s2) | Grade | Rank |
---|---|---|---|---|---|
1.000 | 1.000 | 1.000 | 1.000 | 1.000 | 1 |
0.747 | 0.546 | 0.450 | 0.709 | 0.613 | 2 |
0.354 | 0.630 | 0.338 | 0.417 | 0.435 | 6 |
0.482 | 0.529 | 0.336 | 0.475 | 0.455 | 4 |
0.367 | 0.604 | 0.333 | 0.608 | 0.478 | 3 |
0.360 | 0.417 | 0.426 | 0.465 | 0.417 | 7 |
0.486 | 0.333 | 0.398 | 0.362 | 0.395 | 9 |
0.401 | 0.644 | 0.355 | 0.370 | 0.443 | 5 |
0.333 | 0.625 | 0.343 | 0.333 | 0.409 | 8 |
Surface Roughness (µm) | Cutting Temp. (°C) | Sound Level (dB) | Machine Vibration (m/s2) | Grade | Rank |
---|---|---|---|---|---|
1.000 | 1.000 | 1.000 | 0.478 | 0.869 | 2 |
0.763 | 0.758 | 0.984 | 1.000 | 0.876 | 1 |
0.347 | 0.714 | 0.977 | 0.457 | 0.624 | 4 |
0.461 | 0.522 | 1.000 | 0.697 | 0.670 | 3 |
0.392 | 0.708 | 0.564 | 0.333 | 0.500 | 5 |
0.333 | 0.356 | 0.355 | 0.565 | 0.402 | 8 |
0.443 | 0.354 | 0.375 | 0.451 | 0.406 | 7 |
0.379 | 0.342 | 0.333 | 0.778 | 0.458 | 6 |
0.334 | 0.333 | 0.353 | 0.443 | 0.366 | 9 |
Parameter | Level 1 | Level 2 | Level 3 | Max-Min | Rank |
---|---|---|---|---|---|
Spindle Speed | 0.683 | 0.450 | 0.415 | 0.267 | 1 |
Feed Rate | 0.617 | 0.511 | 0.420 | 0.197 | 2 |
Depth of Cut | 0.620 | 0.492 | 0.436 | 0.184 | 3 |
Parameter | Level 1 | Level 2 | Level 3 | Max-Min | Rank |
---|---|---|---|---|---|
Spindle Speed | 0.7898 | 0.5239 | 0.4098 | 0.3800 | 1 |
Feed Rate | 0.6483 | 0.6113 | 0.4639 | 0.1844 | 2 |
Depth of Cut | 0.5766 | 0.6373 | 0.5096 | 0.1278 | 3 |
Source | DF | Adj SS | Adj MS | F-Value | % Contribution |
---|---|---|---|---|---|
Spindle Speed (rev/min) | 2 | 0.12674 | 0.06337 | 2.16 | 42.7036 |
Feed Rate (mm/rev) | 2 | 0.05810 | 0.02905 | 0.99 | 19.5761 |
Depth of Cut (mm) | 2 | 0.05327 | 0.02664 | 0.91 | 17.9487 |
Error | 2 | 0.05868 | 0.02934 | 19.7716 | |
Total | 8 | 0.29679 | 100 |
Source | DF | Adj SS | Adj MS | F-Value | % Contribution |
---|---|---|---|---|---|
Spindle Speed (rev/min) | 2 | 0.228100 | 0.114050 | 275.31 | 73.4513 |
Feed Rate (mm/rev) | 2 | 0.057117 | 0.028559 | 68.94 | 18.3924 |
Depth of Cut (mm) | 2 | 0.024501 | 0.012250 | 29.57 | 7.8897 |
Error | 2 | 0.000829 | 0.000414 | 0.2669 | |
Total | 8 | 0.310546 | 100 |
S | R2 | R2 (adj) | R2 (pred) |
---|---|---|---|
1.40745 | 79.92% | 67.88% | 48.48% |
S | R2 | R2 (adj) | R2 (pred) |
---|---|---|---|
14.0329 | 28.56% | 0.00% | 0.00% |
S | R2 | R2 (adj) | R2 (pred) |
---|---|---|---|
1.35966 | 77.57% | 64.12% | 41.08% |
S | R2 | R2 (adj) | R2 (pred) |
---|---|---|---|
11.0372 | 89.15% | 82.64% | 59.03% |
S | R2 | R2 (adj) | R2 (pred) |
---|---|---|---|
2.1124 | 92.63% | 66.14% | 62.65% |
S | R2 | R2 (adj) | R2 (pred) |
---|---|---|---|
114.4545 | 94.03% | 57.29% | 51.71% |
S | R2 | R2 (adj) | R2 (pred) |
---|---|---|---|
3.2422 | 99.21% | 36.49% | 38.37% |
S | R2 | R2 (adj) | R2 (pred) |
---|---|---|---|
63.1425 | 98.21% | 47.92% | 72.01% |
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Kazeem, R.A.; Fadare, D.A.; Ikumapayi, O.M.; Akinlabi, S.A.; Akinlabi, E.T. Evaluation of Mango Kernel Seed (Mangifera indica) Oil as Cutting Fluid in Turning of AISI 1525 Steel Using the Taguchi-Grey Relation Analysis Approach. Lubricants 2022, 10, 52. https://doi.org/10.3390/lubricants10040052
Kazeem RA, Fadare DA, Ikumapayi OM, Akinlabi SA, Akinlabi ET. Evaluation of Mango Kernel Seed (Mangifera indica) Oil as Cutting Fluid in Turning of AISI 1525 Steel Using the Taguchi-Grey Relation Analysis Approach. Lubricants. 2022; 10(4):52. https://doi.org/10.3390/lubricants10040052
Chicago/Turabian StyleKazeem, Rasaq A., David A. Fadare, Omolayo M. Ikumapayi, Stephen A. Akinlabi, and Esther T. Akinlabi. 2022. "Evaluation of Mango Kernel Seed (Mangifera indica) Oil as Cutting Fluid in Turning of AISI 1525 Steel Using the Taguchi-Grey Relation Analysis Approach" Lubricants 10, no. 4: 52. https://doi.org/10.3390/lubricants10040052
APA StyleKazeem, R. A., Fadare, D. A., Ikumapayi, O. M., Akinlabi, S. A., & Akinlabi, E. T. (2022). Evaluation of Mango Kernel Seed (Mangifera indica) Oil as Cutting Fluid in Turning of AISI 1525 Steel Using the Taguchi-Grey Relation Analysis Approach. Lubricants, 10(4), 52. https://doi.org/10.3390/lubricants10040052