Multi-Residue Screening of Pesticides in Aquaculture Waters through Ultra-High-Performance Liquid Chromatography-Q/Orbitrap Mass Spectrometry
Abstract
:1. Introduction
2. Materials and Methods
2.1. Reagents and Chemicals
2.2. Samples
2.3. Sample Preparation
2.4. Instrument
2.5. Identification and Validation
3. Results and Discussion
3.1. Data Acquisition with UHPLC-Q/Orbi-MS and the Ionization of Compounds
3.2. Selection of Extraction Cartridges
3.3. Optimazation of Eluents
3.4. Effect of the Cartridge Capacity on Pesticide Recovery
3.5. Method Performance and Matrix Effect
3.6. Application to Real Samples
4. Conclusions
Supplementary Materials
Author Contributions
Funding
Conflicts of Interest
References
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Wang, S.-Y.; Fodjo, E.K.; Kong, C.; Yu, H.-J. Multi-Residue Screening of Pesticides in Aquaculture Waters through Ultra-High-Performance Liquid Chromatography-Q/Orbitrap Mass Spectrometry. Water 2020, 12, 1238. https://doi.org/10.3390/w12051238
Wang S-Y, Fodjo EK, Kong C, Yu H-J. Multi-Residue Screening of Pesticides in Aquaculture Waters through Ultra-High-Performance Liquid Chromatography-Q/Orbitrap Mass Spectrometry. Water. 2020; 12(5):1238. https://doi.org/10.3390/w12051238
Chicago/Turabian StyleWang, Shou-Ying, Essy Kouadio Fodjo, Cong Kong, and Hui-Juan Yu. 2020. "Multi-Residue Screening of Pesticides in Aquaculture Waters through Ultra-High-Performance Liquid Chromatography-Q/Orbitrap Mass Spectrometry" Water 12, no. 5: 1238. https://doi.org/10.3390/w12051238
APA StyleWang, S. -Y., Fodjo, E. K., Kong, C., & Yu, H. -J. (2020). Multi-Residue Screening of Pesticides in Aquaculture Waters through Ultra-High-Performance Liquid Chromatography-Q/Orbitrap Mass Spectrometry. Water, 12(5), 1238. https://doi.org/10.3390/w12051238