Advanced RSM-Driven Optimisation for Enhancing the Mechanical Performance of FDM-Printed PETG: A Correlated Microstructural and Mechanical Property Investigation
Abstract
1. Introduction
2. Materials and Methods
2.1. Materials and Machine
2.2. Parameters Selection and Optimisation
2.3. Design and Mechanical Testing of FDM-Printed Specimens
2.4. Design of Experiments (DOEs) and Statistical Analysis
3. Results
3.1. Tensile Properties
3.1.1. Ultimate Tensile Strength
3.1.2. Modulus of Elasticity
3.1.3. Yield Strength (0.2% Offset)
3.2. Compressive Properties
3.2.1. Compressive Strength
3.2.2. Compressive Modulus
3.3. Microstructural Behaviour of Various Parameters from Printed PETG Specimens
3.4. Statistical Analysis
3.4.1. Statistical Analysis on the Tensile Strength
Statistical Analysis of UTS
- Comparison of Experimental and Predicted Ultimate Tensile Strength
Statistical Analysis of Modulus of Elasticity
- Comparison of Experimental and Predicted Young’s Modulus
Statistical Analysis of Yield Strength
- Comparison of Experimental and Predicted Yield Strength
3.4.2. Statistical Analysis on the Compressive Properties
Statistical Analysis of Compressive Strength
- Comparison of Experimental and Predicted Compressive Strength
Statistical Analysis of Compressive Modulus
- Comparison of Experimental and predicted compressive modulus
3.5. Comparison of Mechanical Properties of PETG Specimens
4. Conclusions
- In contrast to previous investigations, the standard parameters’ average mechanical characteristics demonstrate a greater magnitude. This discrepancy results from the fact that a 100% infill density was used to manufacture the specimens in previous experiments. It is important to highlight that in this study, all specimens were produced with a uniform infill density of 50%.
- The occurrence of this phenomenon can be traced to the increase in the number of solid layers from two to three. The results of this investigation indicate that the concentric pattern is primarily suitable for bearing tensile load. This conclusion was reached as a result of examination due to the fact that the load was distributed evenly from one end to the other end of the structure.
- In the context of normal-parameter printing, the infill pattern holds significant importance in relation to tensile load. On the other hand, when compressive loads are taken into consideration, the raster angle has a greater impact on the specimen’s strength than the infill pattern does.
- A twofold increase in the average mechanical characteristics was seen in the specimens with four and five parameters as compared to the specimens with normal parameters. This phenomenon can be explained by the structural composition of the specimens.
- Additionally, PETG is an excellent material for the production of parts that are both flexible and have a high resistance to shock. These parts include pressure-clad objects and protective components.
- Due to its heat resistance and good mechanical properties, PETG is used in many sectors such as aerospace components, automotive interior components, bio-based applications, electronic insulators, and medical equipment.
- In future studies, it is strongly recommended to reduce layer thickness from 0.1 mm to 0.05 mm, which will increase the chances of interlayer bonding and the surface finish of the products.
- Further research could focus on leveraging these improved properties to enhance the application range of FDM-printed PETG parts, especially considering its suitability for flexible, shock-resistant, heat-resistant components in sectors like aerospace and medical equipment.
Supplementary Materials
Author Contributions
Funding
Institutional Review Board Statement
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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| Inner Pattern | Inner Raster Angle (°) | Top Pattern | Bottom Pattern | Top/Bottom Raster Angle (°) |
|---|---|---|---|---|
| Re | 90 | Re | Li | 45 |
| Re | 90 | Li | Re | 45 |
| Re | 90 | Re | Re | 90 |
| Re | 45 | Co | Li | 45 |
| Li | 0 | Re | Re | 45 |
| Re | 90 | Co | Re | 45 |
| Li | 45 | Li | Re | 45 |
| Re | 45 | Li | Re | 0 |
| Co | 90 | Re | Re | 45 |
| Re | 0 | Co | Re | 45 |
| Co | 45 | Re | Li | 45 |
| Li | 45 | Re | Re | 90 |
| Re | 45 | Re | Re | 45 |
| Re | 45 | Re | Re | 45 |
| Re | 45 | Re | Re | 45 |
| Re | 45 | Re | Re | 45 |
| Re | 0 | Re | Re | 90 |
| Re | 45 | Re | Re | 45 |
| Co | 45 | Re | Re | 90 |
| Re | 45 | Li | Re | 90 |
| Re | 45 | Re | Co | 90 |
| Re | 0 | Re | Re | 0 |
| Co | 45 | Co | Re | 45 |
| Re | 45 | Co | Re | 0 |
| Co | 45 | Li | Re | 45 |
| Re | 45 | Re | Li | 90 |
| Re | 90 | Re | Re | 0 |
| Re | 45 | Re | Re | 45 |
| Co | 0 | Re | Re | 45 |
| Re | 45 | Re | Co | 0 |
| Li | 45 | Re | Re | 0 |
| Re | 90 | Re | Co | 45 |
| Re | 45 | Co | Co | 45 |
| Co | 45 | Re | Re | 0 |
| Re | 0 | Re | Co | 45 |
| Li | 45 | Re | Co | 45 |
| Li | 45 | Re | Li | 45 |
| Re | 45 | Li | Co | 45 |
| Co | 45 | Re | Co | 45 |
| Li | 45 | Co | Re | 45 |
| Re | 45 | Re | Li | 0 |
| Re | 0 | Li | Re | 45 |
| Re | 45 | Co | Re | 90 |
| Li | 90 | Re | Re | 45 |
| Re | 0 | Re | Li | 45 |
| Re | 45 | Li | Li | 45 |
| Inner Pattern | Inner Raster Angle (°) | Top Pattern | Bottom Pattern | Top/Bottom Raster Angle (°) | Tensile Strength (MPa) | Young’s Modulus (GPa) | Yield Strength (MPa) (0.2% Offset) |
|---|---|---|---|---|---|---|---|
| Re | 90 | Re | Li | 45 | 14.94 | 0.85 | 11.35 |
| Re | 90 | Li | Re | 45 | 14.44 | 0.79 | 10.66 |
| Re | 90 | Re | Re | 90 | 37.06 | 1.18 | 21.01 |
| Re | 45 | Co | Li | 45 | 28.77 | 0.94 | 15.73 |
| Li | 0 | Re | Re | 45 | 15.19 | 0.90 | 12.07 |
| Re | 90 | Co | Re | 45 | 32.57 | 1.03 | 18.13 |
| Li | 45 | Li | Re | 45 | 12.85 | 0.63 | 7.96 |
| Re | 45 | Li | Re | 0 | 14.10 | 0.61 | 8.53 |
| Co | 90 | Re | Re | 45 | 15.18 | 0.90 | 12.10 |
| Re | 0 | Co | Re | 45 | 32.30 | 0.97 | 17.10 |
| Co | 45 | Re | Li | 45 | 14.45 | 0.79 | 11.65 |
| Li | 45 | Re | Re | 90 | 34.95 | 1.12 | 20.22 |
| Re | 45 | Re | Re | 45 | 13.84 | 0.87 | 11.16 |
| Re | 45 | Re | Re | 45 | 14.45 | 0.88 | 11.71 |
| Re | 45 | Re | Re | 45 | 13.88 | 0.85 | 11.15 |
| Re | 45 | Re | Re | 45 | 13.77 | 0.90 | 11.56 |
| Re | 0 | Re | Re | 90 | 38.44 | 1.18 | 20.90 |
| Re | 45 | Re | Re | 45 | 13.68 | 0.83 | 9.37 |
| Co | 45 | Re | Re | 90 | 38.03 | 1.14 | 19.82 |
| Re | 45 | Li | Re | 90 | 39.26 | 1.12 | 19.69 |
| Re | 45 | Re | Co | 90 | 43.09 | 1.14 | 20.90 |
| Re | 0 | Re | Re | 0 | 14.40 | 0.51 | 7.15 |
| Co | 45 | Co | Re | 45 | 30.17 | 0.95 | 15.30 |
| Re | 45 | Co | Re | 0 | 26.32 | 0.81 | 13.78 |
| Co | 45 | Li | Re | 45 | 12.94 | 0.65 | 7.83 |
| Re | 45 | Re | Li | 90 | 40.63 | 1.06 | 18.10 |
| Re | 90 | Re | Re | 0 | 14.40 | 0.54 | 7.54 |
| Re | 45 | Re | Re | 45 | 14.04 | 0.79 | 9.46 |
| Co | 0 | Re | Re | 45 | 14.16 | 0.80 | 9.79 |
| Re | 45 | Re | Co | 0 | 27.81 | 0.84 | 13.64 |
| Li | 45 | Re | Re | 0 | 13.52 | 0.50 | 7.55 |
| Re | 90 | Re | Co | 45 | 29.24 | 0.85 | 12.06 |
| Re | 45 | Co | Co | 45 | 34.94 | 1.04 | 17.78 |
| Co | 45 | Re | Re | 0 | 14.13 | 0.52 | 7.65 |
| Re | 0 | Re | Co | 45 | 30.89 | 0.89 | 14.95 |
| Li | 45 | Re | Co | 45 | 31.27 | 0.80 | 12.31 |
| Li | 45 | Re | Li | 45 | 17.76 | 0.67 | 13.73 |
| Re | 45 | Li | Co | 45 | 29.47 | 0.73 | 11.00 |
| Co | 45 | Re | Co | 45 | 29.81 | 0.74 | 10.14 |
| Li | 45 | Co | Re | 45 | 26.94 | 0.83 | 12.96 |
| Re | 45 | Re | Li | 0 | 25.23 | 0.82 | 11.94 |
| Re | 0 | Li | Re | 45 | 14.57 | 0.60 | 8.00 |
| Re | 45 | Co | Re | 90 | 40.16 | 0.89 | 15.31 |
| Li | 90 | Re | Re | 45 | 13.92 | 0.67 | 8.53 |
| Re | 0 | Re | Li | 45 | 17.73 | 0.60 | 7.50 |
| Re | 45 | Li | Li | 45 | 14.77 | 0.45 | 5.43 |
| Inner Pattern | Inner Raster Angle (°) | Top Pattern | Bottom Pattern | Top/ Bottom Raster Angle (°) | Compressive Strength (MPa) | Compressive Modulus (GPa) |
|---|---|---|---|---|---|---|
| Re | 90 | Re | Li | 45 | 21.86 | 2.12 |
| Re | 90 | Li | Re | 45 | 21.35 | 2.15 |
| Re | 90 | Re | Re | 90 | 21.22 | 2.15 |
| Re | 45 | Co | Li | 45 | 20.31 | 2.19 |
| Li | 0 | Re | Re | 45 | 20.69 | 2.42 |
| Re | 90 | Co | Re | 45 | 22.10 | 2.31 |
| Li | 45 | Li | Re | 45 | 21.96 | 2.27 |
| Re | 45 | Li | Re | 0 | 21.32 | 2.37 |
| Co | 90 | Re | Re | 45 | 22.49 | 2.27 |
| Re | 0 | Co | Re | 45 | 25.90 | 2.87 |
| Co | 45 | Re | Li | 45 | 23.09 | 2.44 |
| Li | 45 | Re | Re | 90 | 21.92 | 2.39 |
| Re | 45 | Re | Re | 45 | 22.53 | 2.36 |
| Re | 45 | Re | Re | 45 | 22.24 | 2.66 |
| Re | 45 | Re | Re | 45 | 22.65 | 2.48 |
| Re | 45 | Re | Re | 45 | 22.42 | 2.30 |
| Re | 0 | Re | Re | 90 | 23.55 | 2.56 |
| Re | 45 | Re | Re | 45 | 22.46 | 2.30 |
| Co | 45 | Re | Re | 90 | 22.27 | 2.00 |
| Re | 45 | Li | Re | 90 | 21.72 | 2.35 |
| Re | 45 | Re | Co | 90 | 23.11 | 2.29 |
| Re | 0 | Re | Re | 0 | 22.69 | 2.60 |
| Co | 45 | Co | Re | 45 | 23.72 | 2.46 |
| Re | 45 | Co | Re | 0 | 23.31 | 2.35 |
| Co | 45 | Li | Re | 45 | 23.37 | 2.19 |
| Re | 45 | Re | Li | 90 | 21.77 | 2.17 |
| Re | 90 | Re | Re | 0 | 20.56 | 2.19 |
| Re | 45 | Re | Re | 45 | 22.48 | 2.43 |
| Co | 0 | Re | Re | 45 | 21.90 | 2.21 |
| Re | 45 | Re | Co | 0 | 21.94 | 2.29 |
| Li | 45 | Re | Re | 0 | 21.02 | 2.23 |
| Re | 90 | Re | Co | 45 | 22.43 | 2.16 |
| Re | 45 | Co | Co | 45 | 24.28 | 2.45 |
| Co | 45 | Re | Re | 0 | 24.91 | 2.80 |
| Re | 0 | Re | Co | 45 | 21.35 | 2.29 |
| Li | 45 | Re | Co | 45 | 22.81 | 2.34 |
| Li | 45 | Re | Li | 45 | 22.03 | 2.27 |
| Re | 45 | Li | Co | 45 | 23.56 | 2.36 |
| Co | 45 | Re | Co | 45 | 23.11 | 2.27 |
| Li | 45 | Co | Re | 45 | 22.12 | 2.20 |
| Re | 45 | Re | Li | 0 | 21.75 | 2.27 |
| Re | 0 | Li | Re | 45 | 24.76 | 2.78 |
| Re | 45 | Co | Re | 90 | 22.29 | 2.29 |
| Li | 90 | Re | Re | 45 | 21.29 | 2.15 |
| Re | 0 | Re | Li | 45 | 22.46 | 2.27 |
| Re | 45 | Li | Li | 45 | 23.57 | 2.61 |
| Study | Material | Infill Density | UTS | CS | Relative Improvement |
|---|---|---|---|---|---|
| Current Study | PETG | 50% | 43.09 MPa | 25.90 MPa | - |
| Faidallah et al. [54] | PETG | 100% | 42.0 MPa | N/A | +51.26% UTS |
| Martins et al. [55] | PETG | 50% | 33 MPa | N/A | +23.41% UTS |
| Lacob et al. [56] | PETG | 100 | 43.24 MPa | 30.33 | +49.82% UTS and 41.44% CS |
| Lakshman et al. [57] | PETG | 100% | 44.5 MPa | N/A | +48.36% UTS |
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Kumaresan, R.; Kanny, K. Advanced RSM-Driven Optimisation for Enhancing the Mechanical Performance of FDM-Printed PETG: A Correlated Microstructural and Mechanical Property Investigation. Polymers 2025, 17, 3175. https://doi.org/10.3390/polym17233175
Kumaresan R, Kanny K. Advanced RSM-Driven Optimisation for Enhancing the Mechanical Performance of FDM-Printed PETG: A Correlated Microstructural and Mechanical Property Investigation. Polymers. 2025; 17(23):3175. https://doi.org/10.3390/polym17233175
Chicago/Turabian StyleKumaresan, Rajan, and Krishnan Kanny. 2025. "Advanced RSM-Driven Optimisation for Enhancing the Mechanical Performance of FDM-Printed PETG: A Correlated Microstructural and Mechanical Property Investigation" Polymers 17, no. 23: 3175. https://doi.org/10.3390/polym17233175
APA StyleKumaresan, R., & Kanny, K. (2025). Advanced RSM-Driven Optimisation for Enhancing the Mechanical Performance of FDM-Printed PETG: A Correlated Microstructural and Mechanical Property Investigation. Polymers, 17(23), 3175. https://doi.org/10.3390/polym17233175

