1. Introduction
The service environment of concrete structures is subject to constant fluctuations. For example, under solar radiation, the exterior surfaces of buildings can reach significantly high temperatures. These surfaces then rapidly cool due to environmental factors such as wind, cold currents, rain, or hail. The repeated impact of this rapid heating and cooling cycle induces environmental thermal fatigue in structural concrete characterized by alternating cold and hot conditions [
1,
2,
3,
4]. This type of thermal stress leads to damage and cracking in high-performance concrete, significantly reducing its resistance to permeability. These effects compromise the integrity and durability of concrete structures and notably hasten deterioration processes such as salt corrosion, freeze–thaw cycles, and moisture variations, further impairing their durability. As a quasi-brittle material, concrete exhibits inherent brittleness, low tensile strength, and susceptibility to brittle failure. The significant impact of environmental thermal fatigue on concrete’s performance underscores the importance of investigating the mechanical properties and evolutionary trends of 3D-printed cement-based composites subjected to these conditions [
5,
6].
Kraft et al. [
7] discovered that cement paste, mortar, and concrete each have significantly different coefficients of thermal expansion. Given that aggregates constitute the majority of concrete’s volume, they play a pivotal role in determining its thermal expansion coefficient. Baluch [
8] proposed that during thermal cycling, discrepancies in the thermal expansion coefficients between the matrix and aggregate lead to uncoordinated deformation, generating tensile stress at the interfacial transition zone. When this stress surpasses the ultimate strength of the zone, microcracks form, impairing the mechanical properties of concrete. Lin et al. [
9] investigated the effects of temperature cycling from 20 °C to 145 °C on the mechanical properties of cement-based materials, finding that both peak stress and elastic modulus decreased with an increasing number of cycles, detrimentally affecting the macroscopic properties. Kanellopoulos et al. [
10] examined the effect of temperature cycling between 20 °C and 90 °C on the fracture energy of concrete and observed more than a 10% decrease in fracture energy after 90 cycles, largely attributed to microcrack propagation and spreading between the coarse aggregate and matrix. Furthermore, Mahboub et al. [
11] used Ansys 8.0 software to simulate the behavior of road concrete under a temperature field, suggesting that the alternating high and low temperatures exerted a more significant impact on road concrete than vehicular load. Additionally, Wei et al. [
12] explored the influence of temperature fluctuations on early stress development in confined concrete and introduced an enhanced MPS model to predict early tensile stress in concrete, incorporating temperature’s effect on creep.
Numerous scholars have demonstrated that environmental thermal fatigue can result in uncoordinated deformation within concrete, arising from temperature gradients and the disparate thermal properties of its constituents. This misaligned deformation leads to damage and cracking in the material. The existing body of research into the thermal properties of concrete materials, along with the varying behaviors of constituent phases and non-uniform deformation at internal interfaces, lays a foundational framework for investigating the performance evolution mechanisms of 3D-printed cement-based composites under environmental thermal fatigue.
In recent years, extensive research has been conducted on the impact of 3D-printed polymer lattices on the compressive mechanical properties of cement-based composites [
13]. Zeng et al. [
14] developed a novel form of 3D-printed continuous fiber reinforced thermoplastic polymers (CFRTPs) reinforcement for 3D-printed concrete structures, and the tensile behavior of 3D-printed CFRTP bars and grids was conducted. Then, the CFRTP reinforcement was used for 3D-printed high-performance concrete to explore the effectiveness of the reinforcement. Salazar et al. [
15] investigated the mechanical properties of ultra-high-performance concrete reinforced with 3D-printed polymer lattices under uniaxial compression loads. Bogusz et al. [
16] performed quasi-static axial compression tests on a three-dimensional lattice created using stereolithography (SLA), studying the compression curves and deformation processes across five distinct lattice geometries. Tao et al. [
17] utilized fused filament fabrication (FFF) technology to print two types of lattice structures, which were then infused with rigid polyurethane foam (RPUF) to fabricate structural composites. These composites demonstrated significantly enhanced elastic limits, compressive moduli, and energy absorption capacities compared to pure RPUF. Ghannadpour et al. [
18] explored the compressive behavior of six pillar-based topologies printed through digital light processing (DLP) via both experimental tests and numerical simulations. Moreover, Tzortzinis et al. [
19] introduced a novel methodology employing steel-assisted truss lattice reinforcements to contain concrete/mortar materials, observing that the auxiliary lattice provided superior confinement to the mortar matrix under axial compression compared to traditional mortar samples. While research on 3D-printed lattice-reinforced cement-based composites has primarily concentrated on their mechanical properties at room temperature, the influence of environmental thermal fatigue on these properties remains an important area of study.
In this study, two polymer lattices with differing structures were fabricated using multi-jet fusion (MJF) technology [
20,
21,
22,
23], ensuring an identical volume for each configuration by design. These lattices were then integrated into molds to cast the cement matrices, forming lattice-reinforced cement-based samples. Following a standard 28-day curing period, the samples underwent thermal fatigue treatment, experiencing temperature fluctuations of 60 °C over 45, 90, and 145 cycles. Subsequent to this treatment, uniaxial compression tests were performed to assess alterations in mechanical properties [
24,
25,
26,
27]. The deterioration in strength and deformation of the 3D-printed lattice-reinforced cement-based composites were quantitatively analyzed through nondestructive acoustic emission (AE) and digital image correlation (DIC) testing techniques, correlating the findings with the number of thermal cycles experienced. This study advances the field by focusing on RO and SO lattices under thermal fatigue, a context unexamined in prior lattice research. Addressing the critical gap in understanding how 3D-printed lattices modulate thermal fatigue damage in cement composites, whereas earlier work focused on conventional concrete or room-temperature lattice performance. Integrating AE and DIC to unravel the mechanistic links between lattice topology, thermal cycling, and deterioration—providing a more nuanced understanding than traditional mechanical testing alone.
3. Experimental Design
Following a standard curing period of 28 days, the cement-based composite material samples were allowed to acclimate in a room for one week to ensure complete evaporation of surface moisture. Subsequently, these samples were placed in a high-temperature test chamber, as depicted in
Figure 2 High-temperature test chamber (model SET-Z-041LX) (Aspec Environmental Instruments (Shanghai) Co., Ltd., Shanghai, China.). The environment within the control box was pre-programmed.
During the heating process, the heating rate was maintained at or below 3 °C/min to mitigate thermal shock effects on the sample, as detailed in references [
30,
31,
32,
33]. For this experiment, a heating rate of 2 °C/min was employed to raise the temperature in the high-temperature chamber from room temperature to the target of 85 °C. The temperature was then maintained at 85 °C for 1.5 h before being reduced back to room temperature over a period of 1 h. This procedure constituted one thermal cycle, as depicted in
Figure 3 The samples underwent 45, 90, and 145 thermal cycles.
The compression test setup is illustrated in
Figure 4. A universal testing instrument, DNS-100 (Changchun Institute of Mechanical Science Co., Ltd., Changchun, China), capable of handling loads up to 100 kN, was selected to perform quasi-static loading at a rate of 1 mm/min. Uniaxial compression tests were conducted on 3D-printed lattice-reinforced cement-based composite samples. AE technology monitored specimen damage during the loading process, while DIC tracked deformation across the entire specimen.
During the loading process, the DS2-8A (four-channel) full-information AE signal analyzer produced by Ruandao Company (Beijing, China) was used for the collection and analysis of AE signals. The diameter of the sensor is 16 mm. The sensor is connected to the AE signal analyzer through a 40 dB intelligent AE preamplifier. The experimental acquisition accuracy is 16 bits, the sampling rate is 3 M, and the sampling time interval is 0.3333 μs. The threshold triggering mode is adopted. According to existing studies [
34], the channel threshold for 3D-printed cement-based composites is set to 100 mV.
The image acquisition system comprised a cold light source, a BT-23120 telephoto lens, an MV-EM510 M/C CCD camera, and a supporting bracket(provided by Wilkesh Digital Image Technology Co., Ltd. (Beijing, China)). The telecentric lens featured a magnification of 0.072×. The CCD camera boasted a resolution of 2456 × 2058 pixels, amounting to a total of approximately 5 million pixels. Image acquisition software provided by Wilkesh Digital Image Technology Co., Ltd. (Beijing, China), facilitated data capture at a rate of 8 frames per second. A 2D-DIC system from CSI Company (Beijing, China)was utilized for processing the images throughout the entire loading process.
4. Results and Discussion
In this paper, uniaxial compression tests were conducted on cement-based composites reinforced with three types of lattices: no lattice, RO lattice, and SO lattice. Each type consisted of 9 samples, totaling 27 samples. These were evenly distributed into three groups, each subjected to 45, 90, and 145 environmental thermal fatigue cycles, respectively. Following treatment, the samples underwent uniaxial compression loading. For further analysis, the data group representing the highest peak load within each category was selected for AE characteristics analysis and strain field analysis.
4.1. Stress–Strain Curve Analysis
The stress–strain curves of cement-based composite specimens after undergoing various thermal cycles are displayed in
Figure 5 and
Figure 6 shows that after 45, 90, and 145 thermal cycles, the peak loads for the non-reinforced cement-based composites were 17.8 MPa, 12.9 MPa, and 8.8 MPa, respectively. The strength of these specimens diminished to 72.47% and 49.44% of the initial value after 45 and 90 thermal cycles, respectively. For the RO lattice-reinforced samples, the peak loads were 22.4 MPa, 19.3 MPa, and 18.4 MPa, showing a decrease in strength to 91.07% and 82.14% after 45 and 90 cycles, respectively. Similarly, the SO lattice-reinforced samples exhibited peak loads of 24.5 MPa, 20.4 MPa, and 19.1 MPa, with their strengths declining to 83.27% and 77.96% after the same number of cycles. Notably, the specimens reinforced with 3D-printed lattices experienced significantly less reduction in compressive strength across the same number of cycles compared to those without lattice reinforcement.
4.2. AE Signal Analysis
In this study, AE technology was employed to monitor real-time signals such as deformation and fracture in materials or structures under load, a process driven by the strain energy released from stress waves. We utilized key AE parameters including hits, energy, and peak frequency as evaluation indicators to generate time–force, time–hit, time–energy, and time–peak frequency curves. Analysis of these curves enabled the assessment of the mechanical responses and deformation characteristics of cement-based samples under compression. The AE characteristics of the samples during loading were further analyzed by correlating the AE parameters with the stress–strain curves depicted in
Figure 7,
Figure 8 and
Figure 9.
Figure 7, the lattice-unreinforced cement-based control sample initially exhibited elastic deformation. With rapidly increasing loads, the AE hit rates markedly accelerated, leading to a progressive rise in cumulative impacts. As loading continued, the formation of further cracks in the composite resulted in a higher frequency of AE hits. During the plastic deformation phase, the specimen underwent irreversible changes due to the sustained load, leading to extensive internal damage. As loading persisted, this damage intensified, prompting a renewed acceleration in the rate of AE hits. Ultimately, when the specimen’s load-bearing capacity was surpassed, it experienced significant levels of damage, although to a lesser extent than in earlier stages, leading to a reduction in AE hits.
Figure 8 illustrates that the AE parameters of RO lattice-reinforced cement-based composites during uniaxial compression are comparable to those observed in non-lattice-reinforced cement-based specimens.
All results indicated an increase in the number of AE hits during the initial stage of cement matrix compression. Throughout this stage, changes in energy and peak frequency were relatively minor.
The time–force curve (in
Figure 9) shows that the 3D-printed lattice delayed the failure of the sample. When combined with the time–hit curve from AE data, it is evident that the number of hits for RO and SO lattice-reinforced cement-based samples plateaued during the initial loading phase. This suggests that the lattice structure in these samples significantly alters the failure mode of cement-based composites under uniaxial compression, effectively diminishing material damage. For lattice-reinforced specimens, this characteristic remained consistent despite an increase in the number of thermal cycles. However, the accumulated number of impacts reveals that a higher number of thermal cycles exacerbates material damage in the initial compression stage.
4.3. DIC Signal Analysis
In this study, deformation images of cement-based composite samples were captured throughout the loading process and analyzed using VIC-2D 6 (Beijing Ruituo Shichuang Technology Co., Ltd. Beijing China) to obtain strain maps after various thermal cycles. These images revealed significant alterations in the horizontal strain field (exx), whereas the vertical strain field (eyy) showed minimal changes. This section focuses on analyzing the strain distribution within the horizontal strain field during uniaxial compression tests. By integrating the stress–strain properties of the samples at different stages with the time–force curves, DIC images corresponding to specific feature points were selected for detailed analysis.
Figure 10,
Figure 11 and
Figure 12 show the strain maps for cement-based samples without lattice reinforcement subjected to varying thermal fatigue cycles at different time points. The analysis of these strain maps for the unreinforced cement-based material reveals that the area of strain within the sample expanded progressively with an increase in the number of thermal cycles. Notably, the sample failed at 145 thermal cycles. This observation indicates that continuous thermal cycling significantly diminishes the compressive properties of the material. Despite these changes in mechanical properties, the ambient temperature did not alter the brittleness of the material. Consequently, the deformation of the material primarily appeared as a large crack, resulting from significant localized strain.
Figure 11 illustrates the strain maps of 3D-printed lattice-reinforced cement-based samples subjected to varying numbers of environmental thermal fatigue cycles at different time points during uniaxial compression tests.
Figure 12 presents the strain maps of 3D-printed lattice-reinforced cement-based samples featuring SO structures, captured at various time points during uniaxial compression tests following 45, 90, and 145 environmental thermal fatigue cycles, respectively.
As can be seen from
Table 6, for specimens of the same type under different numbers of thermal cycles, the maximum strain of the three types of specimens (control, RO, and SO) generally increases with the increase in the number of thermal fatigue cycles. This indicates that the lateral expansion deformation of the specimens becomes more obvious as the number of cycles accumulates, and also confirms that thermal fatigue cycles do promote material deformation. However, although the strain of all three types of specimens increases, the strain growth of RO and SO specimens with lattice reinforcement is much slower than that of the control group without lattice reinforcement. This intuitively reflects that the lattice can play a role in inhibiting deformation. Further analysis shows that thermal fatigue treatment does reduce the mechanical properties of 3D-printed lattice-reinforced cement-based composites, specifically in the form of increased strain and weakened load-bearing capacity. But compared with the control group of cement-based specimens without lattice reinforcement, the addition of 3D-printed lattices can significantly reduce the damage to the mechanical properties of cement-based materials caused by alternating high and low temperature environments by virtue of their own structural constraint effect.
By further comparing the specimens with two different lattice structures (RO and SO), the maximum strains of RO lattice after 45, 90, and 145 thermal fatigue cycles are 0.0442, 0.0515, and 0.0545, respectively, while the maximum strains of SO lattice under the same number of cycles reach 0.0525, 0.09, and 0.067, respectively. It can be seen from the data that the maximum strain of RO lattice is smaller than that of SO lattice under all three cycle numbers. Moreover, with the increase in the number of cycles, the strain of RO increases from 0.0442 to 0.0545, with an increase of approximately 23.3%; the strain of SO increases from 0.0525 to 0.067, with an increase of approximately 27.6%. This indicates that after the action of environmental thermal fatigue, RO lattice has a better inhibitory effect on lateral expansion deformation and stronger deformation resistance than SO lattice.
By comparing the DIC strain contour maps of RO and SO lattice-reinforced cement-based composites under different thermal cycle counts, it is evident that environmental thermal fatigue does not alter the stress redistribution effect of 3D-printed lattices on the specimens. Compared with cement-based composites without lattice reinforcement under the same number of cycles, the addition of lattices can effectively delay the cracking of the specimens.
4.4. Morphological Analysis
Following the uniaxial compression tests, the cement matrix that was peeled off the surface of the specimens revealed the failure morphology of cement-based specimens reinforced with various lattice structures, as presented in
Figure 13. This observation suggests that the 3D-printed lattice influenced the phase composition of the cement matrix. During compression, this modification enabled the sample to withstand higher loads, thereby enhancing its compressive strength.
This study investigated the compressive mechanical properties of cement-based materials with lattice reinforcements of different structural forms under various thermal cycle conditions. The lattice structure was found to enhance the compressive load-bearing capacity of the materials, and deformation characteristics were analyzed, as detailed in
Table 7. Sections (a)–(c) of
Table 7 demonstrate that the cement-based samples lacking lattice reinforcements predominantly failed due to large cracks that compromised their load-bearing capacity. The deformation process involved friction between the sample and both the upper and lower indenters of the testing machine, leading to larger deformations at both surfaces of the sample due to external constraints, while the middle part contracted. This constrained deformation resulted in increased internal stress, ultimately causing the material to crack. Moreover, the data revealed that with an increasing number of thermal fatigue cycles, the compressive strength of the non-reinforced cement-based samples decreased, and the incidence of cracking in these samples increased.
Table 7d–i illustrates that for the cement-based composites with RO and SO lattice reinforcements, the lattice structure effectively constrained the cement matrix. Further, it redistributed the internal stresses through deformation, thereby enhancing the structure’s load-bearing capacity. This study compared the deformation characteristics of cement-based samples reinforced with an RO lattice after 45, 90, and 145 thermal cycles. With an increase in the number of thermal fatigue cycles, the constricting effect of the lattice on the cement matrix diminished, leading to an escalation in the extent of crack damage on the specimen surfaces. Although the compressive deformation characteristics of the SO lattice-reinforced samples were similar to those of the RO-reinforced samples, the RO lattice exhibited a stronger constraining impact on the cement matrix.