Enhancing the Compressibility of Seasonally Frozen Subgrade Clay Subjected to Freeze-Thaw Cycles Using Lignin Fibers
Abstract
1. Introduction
2. Compression Tests and Results Analysis
2.1. Materials and Experimental Procedures
2.1.1. Materials
2.1.2. Specimen Preparation
2.1.3. Application of Freeze-Thaw Cycles
2.1.4. One-Dimensional Compression Tests
2.2. Results and Discussion
2.2.1. Effect of Lignin Fiber Content
2.2.2. Effect of Freeze-Thaw Cycles
3. Microstructural Tests and Results Analysis
3.1. Microstructural Test Procedures
- Small cubic samples approximately 10 mm in size were cut from compacted specimens after freeze-thaw treatment. These samples were rapidly frozen using liquid nitrogen, followed by freeze-drying to preserve the original microstructure by removing pore water.
- After freeze-drying, samples were carefully trimmed to approximately 5 mm cubes using diamond tools, ensuring flat and even surfaces.
- The specimens were then gold-coated to enhance surface conductivity and reduce charging effects under electron beam irradiation. SEM imaging was conducted using a JEM-2100 scanning electron microscope (Tokyo, Japan) at a magnification of 200×.
- The MIP procedure was as follows:
- Small clay samples weighing 1–2 g were taken from similarly treated specimens, rapidly frozen in liquid nitrogen, and subsequently freeze-dried to retain the original pore structure.
- After drying, samples were gently ground to particles smaller than 2 mm, avoiding pore structure damage. The prepared samples were placed into a PoreMaster 33GT mercury porosimeter (Quantachrome Instruments, Boynton Beach, FL, USA), where pressure was gradually increased from vacuum to a maximum of 400 MPa.
- The pore size distribution was determined by measuring mercury intrusion volume as a function of applied pressure, converted into pore diameter via the Washburn equation.
3.2. Analysis and Discussion
3.2.1. SEM Analysis
3.2.2. MIP Analysis
4. Compression Model
4.1. Modified Van Genuchten Model for Clay Compression
4.2. Coupling Effect of Fiber Content and Freeze-Thaw Cycles on the Parameters in the Model
4.3. Integrated Compression Model Development
5. Discussion
- Optimization of lignin fiber content and economic considerations: The experimental results indicate that fiber contents ranging from 0.5% to 2.0% are effective, with the range of 1.0 to 1.5% identified as offering optimal performance-to-cost ratios. Below 1.0%, the reinforcement effect deteriorates rapidly with increasing numbers of freeze-thaw cycles, while above 1.5%, further improvements are marginal despite increased cost. The selection of fiber content in engineering practice should therefore be based on the anticipated severity of freeze-thaw conditions and settlement control requirements.
- Key construction procedures: To ensure optimal fiber performance, uniform dispersion must be prioritized, as shown in Figure 11. It is recommended that procedures similar to those adopted in this study be implemented: pre-sieving of fibers, dry mixing in layers with soil followed by the gradual addition of water, and sufficient resting time to ensure moisture equilibrium. Bulk mixing of fibers or direct incorporation into wet soil should be avoided to prevent fiber clumping.
- Compression model applicability: The proposed compression model can be directly embedded into numerical simulations or simplified design analyses for foundation settlement in seasonally frozen regions. By inputting the expected equivalent number of freeze-thaw cycles over the service life and the selected fiber content, the compressibility characteristics (e-lgσv relationship) of the modified soil can be predicted, thereby providing more reliable design parameters and overcoming the limitations of conventional methods that cannot account for long-term environmental effects.
- Long-term performance and durability: While this study focused on the effects of up to 10 freeze-thaw cycles, during which mechanical degradation tended to stabilize, actual engineering applications may involve dozens or even hundreds of cycles, as well as additional environmental stressors such as wetting–drying alternation and microbial activity. Although the lignin fiber-reinforced clay specimens exhibited stable mechanical and microstructural performance under the tested conditions, long-term durability under more extreme environmental exposures remains to be evaluated. While the aromatic structure of lignin provides some inherent resistance to biodegradation, its sustained performance in complex soil environments warrants further experimental verification to support its use in infrastructure projects with extended service lifespans.
- Engineering applicability and sustainable deployment scenarios: The use of lignin fiber-reinforced clay is not only technically effective, but is also well-aligned with current sustainability goals in geotechnical engineering. Its application is particularly advantageous in scenarios requiring minimal environmental impact, such as temporary embankments, ecological slope protection, low-volume roads, and other infrastructure within natural reserves or water conservation zones. In such contexts, lignin fiber can serve as a viable substitute for traditional chemical stabilizers, reducing both carbon emissions and the risk of secondary pollution while maintaining adequate soil performance. This highlights its potential as an eco-friendly and practical solution for sustainable infrastructure development, especially under conditions where environmental constraints limit the use of conventional treatment methods.
6. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Properties | Values |
---|---|
Specific gravity, Gs | 2.68 |
Liquid limit, wL/% | 54.0 |
Plastic limit, wP/% | 24.4 |
Maximum dry density, dmax/(g/cm3) | 1.75 |
Optimum water content, wopt/% | 22.7 |
Sand, % | 11 |
Silt, % | 48 |
Clay, % | 41 |
Classification | CL |
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Tao, Y.; Li, Z.; Xu, S. Enhancing the Compressibility of Seasonally Frozen Subgrade Clay Subjected to Freeze-Thaw Cycles Using Lignin Fibers. Sustainability 2025, 17, 7303. https://doi.org/10.3390/su17167303
Tao Y, Li Z, Xu S. Enhancing the Compressibility of Seasonally Frozen Subgrade Clay Subjected to Freeze-Thaw Cycles Using Lignin Fibers. Sustainability. 2025; 17(16):7303. https://doi.org/10.3390/su17167303
Chicago/Turabian StyleTao, Yi, Zhibin Li, and Siyuan Xu. 2025. "Enhancing the Compressibility of Seasonally Frozen Subgrade Clay Subjected to Freeze-Thaw Cycles Using Lignin Fibers" Sustainability 17, no. 16: 7303. https://doi.org/10.3390/su17167303
APA StyleTao, Y., Li, Z., & Xu, S. (2025). Enhancing the Compressibility of Seasonally Frozen Subgrade Clay Subjected to Freeze-Thaw Cycles Using Lignin Fibers. Sustainability, 17(16), 7303. https://doi.org/10.3390/su17167303