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Materials 2018, 11(2), 199; https://doi.org/10.3390/ma11020199

Phase Transformation Induced Self-Healing Behavior of Al-Ag Alloy

1
Department of Metals and Corrosion Engineering, University of Chemistry and Technology in Prague, Technická 5, 166 28 Prague 6, Czech Republic
2
Department of Inorganic Chemistry, University of Chemistry and Technology in Prague, Technická 5, 166 28 Prague 6, Czech Republic
*
Author to whom correspondence should be addressed.
Received: 19 November 2017 / Revised: 24 January 2018 / Accepted: 25 January 2018 / Published: 27 January 2018
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Abstract

Self-healing alloys are promising materials that can decrease the consequences of accidents. To detect crack formation in a material is simple task that can be performed by e.g., sonic or ultrasound detection, but it is not always possible to immediately replace the damaged parts. In this situation, it is very advantageous to have the chance to heal the crack during operation, which can be done e.g., by annealing. In this paper, self-healing behavior was proven by TEM (Transmission electron microscope) observation of crack healing after annealing. The crack was observed in the rapidly solidified Al-30Ag alloy with non-equilibrium phase composition formed by a minor amount of Ag2Al and a supersaturated solid solution of Ag in an fcc-Al matrix (fcc = face centered cubic). After annealing at 450 °C, equilibrium phase composition was obtained by forming a higher amount of Ag2Al. This phase transformation did not allow the crack to be healed. Subsequent annealing at 550 °C caused recrystallization to a supersaturated solid solution of Ag in fcc-Al, followed by a return to the mixture of fcc-Al and Ag2Al by cooling, and this process was accompanied by the closing of the crack. This observation proved the self-healing possibilities of the Ag2Al phase. Practical application of this self-healing behavior could be achieved through the dispersion of fine Ag2Al particles in a structural material, which will enrich the material with self-healing properties. View Full-Text
Keywords: self-healing; Al alloys; TEM self-healing; Al alloys; TEM
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This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited (CC BY 4.0).
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Michalcová, A.; Marek, I.; Knaislová, A.; Sofer, Z.; Vojtěch, D. Phase Transformation Induced Self-Healing Behavior of Al-Ag Alloy. Materials 2018, 11, 199.

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