Preparation and Properties of a Novel Microcrystalline Cellulose-Filled Composites Based on Polyamide 6/High-Density Polyethylene
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Sample Preparation
2.3. Characterization
2.3.1. Differential Scanning Calorimetry
2.3.2. Thermogravimetric Analysis
2.3.3. Mechanical Testing
2.3.4. Morphological Analysis
2.3.5. Dynamic Mechanical Analysis
3. Results and Discussion
3.1. Differential Scanning Calorimetry Analysis
3.2. Thermal Analysis
3.3. Mechanical Analysis
3.4. Morphology Analysis
3.5. Dynamic Mechanical Analysis
4. Conclusions
Acknowledgments
Author Contributions
Conflicts of Interest
References
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Samples | LiCl (wt %) | MAPE (wt %) | Processing Temperature (°C) |
---|---|---|---|
L0 | 0 | 10 | 240 |
L0.5 | 0.5 | 10 | 235 |
L1.0 | 1 | 10 | 230 |
L1.5 | 1.5 | 10 | 225 |
L2.0 | 2 | 10 | 220 |
L2.5 | 2.5 | 10 | 210 |
L3.0 | 3 | 10 | 200 |
M5 | 1 | 5 | 230 |
M15 | 1 | 15 | 230 |
M20 | 1 | 20 | 230 |
R | 0 | 0 | 240 |
Samples | Tm (°C) | Tp (°C) | Crystallization Time (s) | Xc (%) |
---|---|---|---|---|
L0 | 220.4 | 188.6 | 47 | 20.0 |
L0.5 | 213.4 | 179.7 | 64 | 19.2 |
L1.0 | 209.9 | 171.1 | 78 | 17.8 |
L1.5 | 204.5 | 161.3 | 107 | 15.3 |
L2.0 | 197.0 | 143.3 | 169 | 10.9 |
L2.5 | 187.5 | - | - | 9.4 |
L3.0 | - | - | - | - |
Samples | Tp (°C) | ||
---|---|---|---|
Peak A | Peak B | Peak C | |
L0 | 366.2 | 442.5 | 482.7 |
L0.5 | 350.8 | 429.9 | 483.7 |
L1.0 | 343.0 | 422.9 | 480.8 |
L1.5 | 336.2 | 420.6 | 480.6 |
L2.0 | 319.8 | 418.5 | 479.8 |
L2.5 | 317.1 | 423.2 | 482.5 |
L3.0 | 314.6 | 421.0 | 483.1 |
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Xu, S.; Yi, S.; He, J.; Wang, H.; Fang, Y.; Wang, Q. Preparation and Properties of a Novel Microcrystalline Cellulose-Filled Composites Based on Polyamide 6/High-Density Polyethylene. Materials 2017, 10, 808. https://doi.org/10.3390/ma10070808
Xu S, Yi S, He J, Wang H, Fang Y, Wang Q. Preparation and Properties of a Novel Microcrystalline Cellulose-Filled Composites Based on Polyamide 6/High-Density Polyethylene. Materials. 2017; 10(7):808. https://doi.org/10.3390/ma10070808
Chicago/Turabian StyleXu, Shihua, Shunmin Yi, Jun He, Haigang Wang, Yiqun Fang, and Qingwen Wang. 2017. "Preparation and Properties of a Novel Microcrystalline Cellulose-Filled Composites Based on Polyamide 6/High-Density Polyethylene" Materials 10, no. 7: 808. https://doi.org/10.3390/ma10070808
APA StyleXu, S., Yi, S., He, J., Wang, H., Fang, Y., & Wang, Q. (2017). Preparation and Properties of a Novel Microcrystalline Cellulose-Filled Composites Based on Polyamide 6/High-Density Polyethylene. Materials, 10(7), 808. https://doi.org/10.3390/ma10070808