4.1. Tan δ Analysis and Discussion
The Tan δ, a non-destructive diagnostic procedural measurement was performed on accelerated-aged XLPE power cable samples following the South African National Standard (SANS) 1339. According to SANS 1339, the accelerated aging procedure involved thermal pre-conditioning at 50 ± 5 °C for 1000 h on the cable samples without electrical stress, followed by electrical aging for 3000 h. One cable sample was not thermally pre-conditioned and electrically aged (unaged cable). The unaged cable sample was used as a reference to monitor and verify the effect of aging on the XLPE power cable samples under test, including their residual strength and condition assessment during the 500 Hz accelerated aging. To ascertain the impact of thermal pre-conditioning at 50 ± 5 °C for 1000 h on the cable samples, Tan δ measurements were conducted on the cable samples, and the results obtained were compared with those of an unaged cable sample.
Figure 7 presents the Tan δ measurements of the thermally and non-thermally pre-conditioned (unaged) cable samples.
The Tan δ of the thermally pre-conditioned and non-thermally pre-conditioned cable samples at 2 kV, as illustrated in
Figure 7, is below the threshold (boundary or limit) value. The measured Tan δ value (1.01 × 10
−2) remains constant for all voltage levels in the non-thermally pre-conditioned (unaged) cable. All repeated measurements yielded the same result, indicating that the cable insulation was in perfect condition. The Tan δ values of all thermally pre-conditioned cable samples (3.70 × 10
−2) were observed to be constant. This indicates that the thermal pre-conditioning effect on the dielectric properties of the aged XLPE power cable samples is constant. However, it is worth noting that the Tan δ value of the thermally pre-conditioned cable samples increased by 72.7% compared to that of the non-thermally pre-conditioned (unaged) cable sample due to constant exposure to sustained heat.
The hopping conduction mechanism in polymers explains current as a function of temperature. This mechanism displays peaks in the conduction current as a function of temperature, along with the corresponding dielectric loss peak. At temperatures below Tg, the conductivity increases progressively. The constant exposure of the XLPE dielectric to sustained heat alters the internal stress state of the insulating material, which is a precursor to insulation degradation. Temperature influences the polarization of molecules, which causes them to move farther apart. This reduces the density of the material, and as a result, decreases the relative permittivity of the cable samples. The phase transition (crystallization) caused by the constant exposure to heat significantly alters the relative permittivity. The relative permittivity exhibits a negative temperature coefficient (NTC), which decreases with an increase in temperature. The constant exposure of the XLPE power cable samples to heat also influences the moisture content in the insulating material, which impacts the Tan δ measurements.
Thermal pre-conditioning accelerates the insulation deterioration. This decreases the insulation resistance and slightly increases the leakage current; conduction, polarization, and ionization cause dielectric loss.
After the cable samples were thermally pre-conditioned, electrical aging was performed according to SANS 1339.
Figure 8a depicts the threshold of the measured Tan δ values of the XLPE power cable samples at 2 kV.
To validate the laboratory Tan δ test measurement results of the accelerated-aged XLPE power cable samples, a Python (Version 3.12) analytical simulation script model was employed, which is a quantitative paradigm that uses equations based on principles, such as physics or mathematics, to provide exact or approximate solutions. This model enables an understanding of the behavior and a prediction. The analytical simulation results are shown in
Figure 8b.
The analytical simulation results agree with the laboratory Tan δ-measured results for the XLPE power cable samples. The conductivity (σ) of the dielectric is a parameter that represents the losses due to conduction that occurs in the dielectric material in the presence of an electric field. The greater the angle, the more deteriorated the cable insulation.
As expressed in Equation (2), Tan δ is a function of the test voltage and permittivity of the dielectric material. At non-variable frequencies, Tan δ is exclusively dependent on the permittivity (εr). Therefore, any response to Tan δ as a function of temperature is due to changes in permittivity (εr) in response to temperature variations and electrical aging. The energy stored in a dielectric material is proportional to its permittivity (εr).
At a 2 kV test voltage, the Tan δ values of cable samples one (3.70 × 10
−3), two (3.70 × 10
−3), and three (3.70 × 10
−3) were below the threshold value (IEEE criteria) [
25]. A strip increase in the Tan δ value of cable sample four (4.63 × 10
−3) was observed. This shows that the cable sample undergoes a transition in its degradation process due to constant exposure to sustained heat and oxidation. The Tan δ values were above the threshold in cable samples five (5.08 × 10
−3), six (5.12 × 10
−3), eight (5.16 × 10
−3), nine (5.19 × 10
−3), and ten (5.24 × 10
−3). The trend of the measured Tan δ values in the aged cable samples at 1500 h (cable sample five) and thereafter showed a linear increase with the aging period.
The aged cable samples exhibited higher values of Tan δ as the applied voltage increased. Moreover, the mean values of Tan δ of cable samples one, two, and three were slightly constant, whereas in cable sample four, Tan δ was higher. Compared to the IEEE criteria [
25], the mean values of cable samples, one, two, and three were all less than 5 × 10
−3, the allowed limit. Therefore, the Tan δ values of cable samples one, two, and three indicate the low deterioration of the XLPE power cable insulation compared to the unaged cable sample. In contrast, in cable samples five, six, eight, nine, and ten, the level of XLPE power cable insulation deterioration was high.
Comparing the Tan δ values of the aged cable samples with those of an unaged cable sample, the Tan δ value of the unaged cable sample remained constant irrespective of the applied voltage. In contrast, the Tan δ of the accelerated-aged cable samples increased as the applied voltage increased. The Tan δ values of the accelerated-aged cable samples were high because the insulation of the power cable lost strength, causing the ionic mobility to increase and influence the conductivity level within the insulation. Thermal pre-conditioning of the insulating materials of the cable samples was a precursor to and impacted the electrical aging processes. The increase in Tan δ was attributed to a decrease in the dielectric permittivity. The cable samples exhibited a steady inclination. However, the threshold of the measured Tan δ values increased with the aging period.
4.2. Isothermal Relaxation Current Analysis and Discussion
Isothermal relaxation current measurements were performed on accelerated-aged and unaged cable samples. The results obtained were then compared. The unaged cable sample was used as a reference to monitor and verify the effect of aging on the XLPE power cable samples under test, their residual strength, and the condition assessment during the 500 Hz accelerated aging. Isothermal relaxation current measurement involved the application of an external electric field to XLPE cable samples. This resulted in dipole alignment and charge displacement, which led to the polarization of the dielectric materials. The time-dependent reaction followed after the electric field was removed, where the dipole tended to return to its random state. There was steady-state current flow under a constant electric field. In accelerated-aged XLPE power cables, this increase was due to oxidation, the formation of polar groups, and moisture ingress.
According to Simons and Tam’s theory, trap levels are discrete and distributed over the complete energy band in XLPE cable insulation. For different insulation statuses, the time constant and magnitude of the trap level differ [
15,
22]. The integration of the trapped carrier currents in the measured external circuit at a constant temperature describes the current–time characteristics. The number of energy traps is linearly proportional to the product of instantaneous current and time. The defects in cable samples, which have a discrete set of energy levels above the Fermi level, determine the isothermal relaxation current. Traps lying energetically above E
Tp are mainly free of electrons, whereas those trapped below the E
Tp level are still occupied by the internal density of charges.
The charge traps in the tested XLPE cable samples contained discrete trap levels distributed over the entire energy band. When the tested XLPE cable samples were energized and the energizing source was removed at a constant temperature, the depolarization current decreased monotonically with time.
The energy stored in a dielectric material is proportional to its permittivity (εr). The thermal pre-conditioning of the cable samples reduced the permittivity of the insulation of the accelerated-aged cable samples; as a result, more current was trapped in the dielectric of the accelerated-aged cable samples compared to the unaged cable sample. Permittivity influences the polarization and depolarization in XLPE power cable samples, directly affecting IRC measurements. As the aging period increased, the relative permittivity decreased, the dielectric degradation increased, and more current was trapped in the XLPE power cable dielectric. The degraded insulation had fewer molecules in which the electric field could polarize, reducing the ability of the material to store energy.
The aging process creates N(ETr) in the XLPE power cable insulation. These traps capture and release the charge carriers. fo(E) accounts for the energy distribution of electrons, whereas the exponential term represents the activation of trapped charges. As the XLPE power cable ages, the distribution of charge carriers within the material changes, thereby affecting its electrical properties.
Figure 9a depicts the laboratory depolarization current (IRC) measured on the accelerated-aged and unaged XLPE power cable samples.
A Python analytical simulation script model was used to validate the laboratory IRC test measurement results of the accelerated-aged XLPE power cable samples. The analytical simulation results are presented in
Figure 9b.
The analytical simulated results were in complete agreement with the laboratory test results of the accelerated-aged and unaged XLPE power cable samples. As presented in this study, they were consistent with theoretical expectations within acceptable tolerances. It was observed that the value of the current trapped in the accelerated-aged XLPE power cable samples increased with the aging period, and the curve of the depolarization current was offset upward. The trap density increased owing to aging. The current trapped in the accelerated-aged XLPE power cable sample at 300 h (cable sample one) of the aging period was (87.45 pico-ampere (pA)) low, as compared to the current trapped in an unaged cable sample (59.1 pA). The relative permittivity was moderate, and more molecules were polarized.
There is no significant increase in the amount of current trapped in the cable sample after 600 h (cable sample two), 89.42 pA, and cable sample after 900 h (cable sample three), 94.53 pA, as compared to the cable sample after 300 h (cable sample one), 87.45 pA. A strip increase was noticed in the cable sample after 1200 h (cable sample four) of 103.28 pA, suggesting a transition in the degradation process. It was observed that the trapped current became more pronounced (115.5 pA) at 1500 h (cable sample five) of electrical aging. The depolarization currents of 140.71 pA, 148.39 pA, 155.89 pA, and 159.76 pA were measured in the cable samples after 1800 h (cable sample six), 2400 h (cable sample eight), 2700 h (cable sample nine), and 3000 h (cable sample ten), respectively. It was observed that, as the aging period increased, the permittivity of the accelerated-aged XLPE power cable samples decreased, the residual strength decreased, and more currents were trapped in the tested XLPE power cable dielectric during the 500 Hz accelerated aging.
The accelerated-aged XPLE power cable samples required more time to decay than the unaged cable sample. When comparing the accelerated-aged and unaged XLPE power cable samples, there was a consistent relationship between the trapped energy and the rate at which it was released. Electrical aging increased the magnitude of the IRC due to moisture absorption, material degradation, and interface effects.
The aging factor (A-factor), which is the ratio of the trapped charge in the insulation defect to the trapped charge in the semiconductor, describes the level of damage to the XLPE power cable insulation. The aging factors of the accelerated-aged and unaged XLPE power cable samples are shown in
Figure 10.
The aging factor is determined using the depolarization current and time constant. The A-factor is independent of temperature, whereas the time at which the maximum peak occurs is independent of the cable length. Analysis of the A-factor shows that the aging factor for the unaged cable sample is 1.39, which indicates that the cable is perfect, while the cable sample after 300 h (cable sample one) is 1.75, indicating mid-life. There is a slight increase in the aging factor of the cable sample after 600 h (cable sample two), at 1.76, and the cable sample after 900 h (cable sample three), at 1.77; the aging factors indicate a mid-life. A strip increase was observed in the cable sample after 1200 h (cable sample four), at 1.89, revealing a transition in the degradation process due to constant exposure to sustained heat and oxidation. As depicted in
Figure 10, as the aging period increased, the aging factor increased. In the aging prognosis of the tested XLPE power cable samples, the aging factor of cable samples after 1500 h (cable sample five) of 2.0, 1800 h (cable sample six) of 2.01, 2400 h (cable sample eight) of 2.02, 2700 h (cable sample nine) of 2.04, and 3000 h (cable sample ten) of 2.07, respectively, show a steady increase, which agrees with the laboratory test measurements on the XLPE power cable samples.
4.3. Return Voltage Measurement Analysis and Discussion
The RVM diagnostic method diagnoses deterioration by detecting the polarization phenomenon in XLPE power cable insulation. This involves three processes: charging, discharging, and recovering. RVM was performed on accelerated-aged cable samples and compared to an unaged cable sample. The analysis of the RVM on the XLPE power cable samples was based on proven normalization factors and threshold values.
The magnitude of the leakage current in the tested XLPE power cable samples was proportional to the height of the return voltage. The change in the return voltage with time resulted from the gradual relaxation of the excited dipoles and a decrease in the polarization. As a result of the applied voltage, conduction and polarization currents flow in the circuit, and the dielectric response is observed. The RVM reflects the surface conductivity and charge mobility. The peak voltage and time to peak indicate the relaxation processes, leakage, and/or conduction paths.
Figure 11a depicts the laboratory RVM test measurements of the accelerated-aged and unaged XLPE power cable samples.
The electrical viscosity of the material is related to the exposure time of the electric field on which the recovery voltage depends. Insulation that contains moisture may become susceptible to electrical aging processes, such as tracking and erosion, which could cause insulation to deteriorate and perform poorly.
The laboratory RVM test measurement results for the accelerated-aged and unaged XLPE power cable samples were validated using a Python analytical simulation script model. The analytical simulation results are shown in
Figure 11b.
The moisture content was attributed to the thermal pre-conditioning effect on the XLPE power cable dielectric. Moisture absorption during aging increases the RVM due to the higher dielectric constant of water. The moisture content reflects its strongly polar character, which increases the recovery voltage and reduces the energy storage capacity of the cable.
The RVM result for the unaged XLPE power cable sample was 0.55 V. In the cable sample after 300 h (cable sample one), an RVM of 0.63 V was recorded, while in the cable sample after 600 h (cable sample two) and the cable sample after 900 h (cable sample three), RVMs of 0.70 V and 0.75 V were measured, respectively.
The measured RVMs on cable samples one, two, and three show a minor decline in the insulation compared to an unaged cable sample. There is a lower degree of aging and moisture in the insulation. A strip increase in the cable sample after 1200 h (cable sample four) of 0.94 V is observed. This is attributed to thermal pre-conditioning and the period of electrical aging.
The return voltages of 1.09 V, 1.14 V, 1.15 V, 1.17 V, and 1.19 V were measured in the cable samples after 1500 h (cable sample five), 1800 h (cable sample six), 2400 h (cable sample eight), 2700 h (cable sample nine), and 3000 h (cable sample ten), respectively. Compared to the unaged cable sample, this indicates degradation. The permittivity of the accelerated-aged XLPE power cable samples decreased. Consequently, there was a decrease in the dielectric residual strength of the tested XLPE power cable, with the highest moisture content in the cable samples nine (2700 h) and ten (3000 h). The moisture content increased with an increasing aging period.
The RVM results show an increase in the recovery voltage as the electrical aging period increases. Aging creates an interface between the materials, leading to changes in the RVM. It also introduces a non-linear effect that makes the return voltage dependent on the strength of the electric field.
The Q-factor, which is the ratio of the energy dissipated per cycle to the maximum energy stored, is used to determine the non-linearity of the initial slope of the return voltage. The empirical evaluation of the Q-factor is as follows:
2.00… 1.87 dry;
1.86… 1.65 moist;
<1.65 wet.
Figure 12 shows the Q-factors of the accelerated-aged and unaged XLPE power cable samples.
Referring to the empirical evaluation of the Q-factor, as depicted in
Figure 12, the unaged cable sample was dry with a Q-factor of 1.894. In contrast, cable sample one (300 h) with a Q-factor of 1.799, cable sample two (600 h) with a Q-factor of 1.792, and cable sample three (900 h) with a Q-factor of 1.788 indicated some moisture content in their respective dielectrics. Cable sample four (1200 h) had a slightly high moisture content (Q-factor 1.689), but it was below the threshold. The cable samples, with Q-factors of 1.603, 1.592, 1.562, 1.559, and 1.552, for five (1500 h), six (1800 h), eight (2400 h), nine (2700 h), and ten (3000 h), respectively, were above the threshold, indicating aging. The Q-factor of the cable samples show a non-linearity of the initial slope of the return voltage, suggesting that thermal pre-conditioning and electrical aging affect the XLPE power cable insulation.
The influence of the measurement resistance can be eliminated; therefore, the amount of water in the cellulose indicates degradation.
Figure 13 shows the P-factor of the cable samples.
As expressed in Equation (7), the P-factor is based on the shape of the return voltage curve, which is determined by evaluating the maximum value of the voltage Umax (V), time until the maximum voltage tmax (s), and initial slope S (V/s).
Notably, the P-factor increased with aging and was independent of the geometric dimensions of the cable under test. The P factor did not depend on the height of the poling voltage and was independent of the geometric parameters of the cable. Aging and degradation increased the P factor. There was a 16.96% difference between the P-factor of the accelerated-aged cable sample after 300 h and the unaged cable sample. A 22.83% difference was observed in the P-factor of the accelerated-aged cable sample after 1500 h, whereas a 27.55% difference was recorded in the accelerated-aged cable sample after 3000 h of aging.
The comparative effectiveness of non-destructive diagnostic techniques was revealed by laboratory test measurement results obtained on accelerated-aged and unaged XLPE power cable samples. The Tan δ prognosis measured the quality, overall dissipation factor, and degradation level of the accelerated-aged and unaged XLPE power cable samples, providing a general indication of their status. The measured Tan δ values can be tracked to monitor the dielectric degradation. In contrast, the IRC technique measured the insulation integrity and revealed the residual strength, extent of aging, and degradation of the insulation of the tested XLPE power cable samples. The RVM offers a more direct assessment of degradation and moisture, emphasizing the moisture ingress and aging indicator of the accelerated-aged and unaged XLPE power cable samples.
The non-destructive diagnostic test measurements were compared, revealed, and agreed upon, considering their respective prognoses for the residual strength and condition of the accelerated-aged and unaged XLPE power cable samples. The best approach was to use non-destructive techniques in conjunction with each other to gain a comprehensive understanding of the dielectric status of the XLPE power cable.