2,3,5-Tri-O-benzyl-d-xylofuranose
1
Institut de Chimie Organique et Analytique (ICOA), UMR 7311 CNRS, Université d’Orléans, Pôle de Chimie, Rue de Chartres, BP 6759, 45067 Orléans CEDEX 2, France
2
Institut de Chimie des Substances Naturelles, CNRS UPR 2301, Université Paris-Saclay, 1 Avenue de la Terrasse, 91198 Gif-sur-Yvette CEDEX, France
*
Authors to whom correspondence should be addressed.
Academic Editor: Kristof Van Hecke
Molbank 2022, 2022(2), M1382; https://doi.org/10.3390/M1382
Received: 21 April 2022
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Revised: 31 May 2022
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Accepted: 1 June 2022
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Published: 7 June 2022
(This article belongs to the Section Structure Determination)
The synthesis and crystallization of 2,3,5-tri-O-benzyl-d-xylofuranose permitted us to isolate the alpha anomer with a small contamination of the beta form (ca 10%), whose first crystallographic structure obtained in the P212121 space group was determined at 100 K up to a resolution of sin θmax/λ = 0.71 Å−1 and refined to an R1 value of 0.0171 with a Hirshfeld atom refinement (HAR) approach.
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Keywords:
2,3,5-tri-O-benzyl-d-xylofuranose; synthesis; Hirshfeld atom refinement of X-ray structure; 3-D Hirshfeld surface; crystal packing
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MDPI and ACS Style
Taffoureau, B.; Gillaizeau, I.; Retailleau, P.; Nicolas, C. 2,3,5-Tri-O-benzyl-d-xylofuranose. Molbank 2022, 2022, M1382. https://doi.org/10.3390/M1382
AMA Style
Taffoureau B, Gillaizeau I, Retailleau P, Nicolas C. 2,3,5-Tri-O-benzyl-d-xylofuranose. Molbank. 2022; 2022(2):M1382. https://doi.org/10.3390/M1382
Chicago/Turabian StyleTaffoureau, Baptiste, Isabelle Gillaizeau, Pascal Retailleau, and Cyril Nicolas. 2022. "2,3,5-Tri-O-benzyl-d-xylofuranose" Molbank 2022, no. 2: M1382. https://doi.org/10.3390/M1382
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