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Open AccessShort Note

4’-Methyl-2’-(quinolin-8-ylcarbamoyl)-biphenyl-4-carboxylic Acid Ethyl Ester

Department of Chemistry, College of Science, Sultan Qaboos University, PO Box 36, Al Khoudh, PC 123, Muscat, Oman
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Molbank 2020, 2020(2), M1132; https://doi.org/10.3390/M1132
Received: 20 April 2020 / Revised: 30 April 2020 / Accepted: 2 May 2020 / Published: 8 May 2020
(This article belongs to the Section Organic Synthesis)
In this short note communication, we report the synthesis of a novel amide 4’-methyl-2’-(quinolin-8-ylcarbamoyl)-biphenyl-4-carboxylic acid ethyl ester by the Ru-catalyzed C(sp2)-H bond arylation reaction. The catalytic C-H bond functionalization reaction was employed, amongst other reaction reagents and conditions, [RuCl2(p-cymene)]2 as a precatalyst and (p-tol)3P as a ligand. The arylation product was characterized by various spectroscopic methods (1H NMR, 13C NMR, IR, GC-MS, and IR spectroscopy), and its composition was confirmed by elemental analysis.
Keywords: organic synthesis; catalysis; bidentate directing groups; benzamides; chelation assistance; C-H bond functionalization organic synthesis; catalysis; bidentate directing groups; benzamides; chelation assistance; C-H bond functionalization
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MDPI and ACS Style

Mamari, H.H.A.; Hasani, A.A. 4’-Methyl-2’-(quinolin-8-ylcarbamoyl)-biphenyl-4-carboxylic Acid Ethyl Ester. Molbank 2020, 2020, M1132.

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