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Molbank 2019, 2019(1), M1041; https://doi.org/10.3390/M1041

5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl Phenyl Acetate

1
Center of Technology For Pharmaceutical and Medical, Agency for the Assessment and Application of Technology (BPPT), Jl. M.H Thamrin 8, Jakarta 10340, Indonesia
2
Faculty of Pharmacy, Universitas Indonesia, Depok 1424, Indonesia
*
Author to whom correspondence should be addressed.
Received: 25 November 2018 / Revised: 21 December 2018 / Accepted: 23 December 2018 / Published: 26 December 2018
(This article belongs to the Section Organic Synthesis)
Full-Text   |   PDF [885 KB, uploaded 26 December 2018]   |   Review Reports

Abstract

We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR), 1H-Nuclear Magnetic Resonance (NMR) and 13C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data. View Full-Text
Keywords: 1-O-acetyl-xanthorrhizol; xanthorrizol; oxidation; potassium permanganate 1-O-acetyl-xanthorrhizol; xanthorrizol; oxidation; potassium permanganate
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited (CC BY 4.0).

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Rahayu, M.D.; Kusumaningrum, S.; Hayun, H. 5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl Phenyl Acetate. Molbank 2019, 2019, M1041.

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