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Open AccessShort Note

5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl Phenyl Acetate

1
Center of Technology For Pharmaceutical and Medical, Agency for the Assessment and Application of Technology (BPPT), Jl. M.H Thamrin 8, Jakarta 10340, Indonesia
2
Faculty of Pharmacy, Universitas Indonesia, Depok 1424, Indonesia
*
Author to whom correspondence should be addressed.
Molbank 2019, 2019(1), M1041; https://doi.org/10.3390/M1041
Received: 25 November 2018 / Revised: 21 December 2018 / Accepted: 23 December 2018 / Published: 26 December 2018
(This article belongs to the Section Organic Synthesis)
We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR), 1H-Nuclear Magnetic Resonance (NMR) and 13C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data. View Full-Text
Keywords: 1-O-acetyl-xanthorrhizol; xanthorrizol; oxidation; potassium permanganate 1-O-acetyl-xanthorrhizol; xanthorrizol; oxidation; potassium permanganate
MDPI and ACS Style

Rahayu, M.D.; Kusumaningrum, S.; Hayun, H. 5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl Phenyl Acetate. Molbank 2019, 2019, M1041.

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