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Short Note

5-Amino-3-methyl-1,2,4-thiadiazole

EaStCHEM School of Chemistry, University of St Andrews, North Haugh, St Andrews, Fife KY16 9ST, UK
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Molbank 2018, 2018(1), M977; https://doi.org/10.3390/M977
Received: 12 December 2017 / Revised: 11 January 2018 / Accepted: 19 January 2018 / Published: 21 January 2018
(This article belongs to the Special Issue Heterocycles)
An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C-NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules. View Full-Text
Keywords: 1,2,4-thiadiazole; NMR spectra; IR spectrum; X-ray structure 1,2,4-thiadiazole; NMR spectra; IR spectrum; X-ray structure
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MDPI and ACS Style

Aitken, R.A.; Slawin, A.M.Z. 5-Amino-3-methyl-1,2,4-thiadiazole. Molbank 2018, 2018, M977. https://doi.org/10.3390/M977

AMA Style

Aitken RA, Slawin AMZ. 5-Amino-3-methyl-1,2,4-thiadiazole. Molbank. 2018; 2018(1):M977. https://doi.org/10.3390/M977

Chicago/Turabian Style

Aitken, R. A., and Alexandra M.Z. Slawin 2018. "5-Amino-3-methyl-1,2,4-thiadiazole" Molbank 2018, no. 1: M977. https://doi.org/10.3390/M977

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