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3-Ethyl-2-(ethylimino)-4-methyl-2,3-dihydro-1,3-thiazole-5-carboxylate Ethyl Ester

School of Pharmacy, Health Science Center, Xi’an Jiaotong University, Xi’an, Shaanxi 710061, China
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Author to whom correspondence should be addressed.
Academic Editor: Norbert Haider
Molbank 2016, 2016(4), M919; https://doi.org/10.3390/M919
Received: 2 November 2016 / Revised: 22 November 2016 / Accepted: 22 November 2016 / Published: 29 November 2016
(This article belongs to the Section Organic Synthesis)
An efficient procedure to obtain the new compound 1a from ethyl acetoacetate (2a), NBS and N,N′-diethylthiourea (4a) was reported. In comparison with the traditional method to synthesize its analogues, this efficient, catalyst-free, and one-pot synthetic method is facile. The work-up procedure is easy and gives the pure target compound under milder reaction conditions in a relatively high yield of 75%. View Full-Text
Keywords: 2,3-dihydro-1,3-thiazole; one-pot synthesis; N,N′-diethylthiourea 2,3-dihydro-1,3-thiazole; one-pot synthesis; N,N′-diethylthiourea
MDPI and ACS Style

Meng, G.; Wang, M.; Cheng, Y.-N.; Chen, K.; Tong, J.; Zhang, J.-H. 3-Ethyl-2-(ethylimino)-4-methyl-2,3-dihydro-1,3-thiazole-5-carboxylate Ethyl Ester. Molbank 2016, 2016, M919.

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