In-Situ Synchrotron SAXS and WAXS Investigation on the Deformation of Single and Coaxial Electrospun P(VDF-TrFE)-Based Nanofibers
Abstract
:1. Introduction
2. Results
2.1. Deformation Mechanism of Single and Coaxial Electrospun Membranes in RD
2.2. Deformation Mechanism of Single and Coaxial Electrospun Membranes in CD
3. Discussion
4. Materials and Methods
4.1. Sample Preparation
4.2. Electrospinning
4.3. Structural Characterization
4.4. Synchrotron Small and Wide-Angle X-ray Diffraction
5. Conclusions
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
Abbreviations
Electroactive polymers | EAPs |
Poly(vinylidene fluoride-trifluoroethylene) | P(VDF-TrEE) |
Chlorotrifluoroethylene | CTFE |
Poly(vinylidene fluoride-trifluoroethylene-chlorotrifluoroethylene) | P(VDF-TrFE-CTFE) |
Relaxor ferroelectric | RFE |
Ferroelectric | FE |
Revolving direction | RD |
Cross direction | CD |
Stress–strain | S-S |
Fourier-transform infrared spectroscopy | FTIR |
Wide-angle X-ray diffraction | WAXD |
Two-dimensional | 2D |
One-dimensional | 1D |
Maxwell-Wagner-Sillars | MWS |
Piezoresponse force microscopy | PFM |
Scanning electron microscopy | SEM |
National Synchrotron Radiation Research Center | NSRRC |
Atomic force microscopy | AFM |
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Huang, Y.-J.; Chen, Y.-F.; Hsiao, P.-H.; Lam, T.-N.; Ko, W.-C.; Luo, M.-Y.; Chuang, W.-T.; Su, C.-J.; Chang, J.-H.; Chung, C.F.; et al. In-Situ Synchrotron SAXS and WAXS Investigation on the Deformation of Single and Coaxial Electrospun P(VDF-TrFE)-Based Nanofibers. Int. J. Mol. Sci. 2021, 22, 12669. https://doi.org/10.3390/ijms222312669
Huang Y-J, Chen Y-F, Hsiao P-H, Lam T-N, Ko W-C, Luo M-Y, Chuang W-T, Su C-J, Chang J-H, Chung CF, et al. In-Situ Synchrotron SAXS and WAXS Investigation on the Deformation of Single and Coaxial Electrospun P(VDF-TrFE)-Based Nanofibers. International Journal of Molecular Sciences. 2021; 22(23):12669. https://doi.org/10.3390/ijms222312669
Chicago/Turabian StyleHuang, Yi-Jen, Yi-Fan Chen, Po-Han Hsiao, Tu-Ngoc Lam, Wen-Ching Ko, Mao-Yuan Luo, Wei-Tsung Chuang, Chun-Jen Su, Jen-Hao Chang, Cho Fan Chung, and et al. 2021. "In-Situ Synchrotron SAXS and WAXS Investigation on the Deformation of Single and Coaxial Electrospun P(VDF-TrFE)-Based Nanofibers" International Journal of Molecular Sciences 22, no. 23: 12669. https://doi.org/10.3390/ijms222312669