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Article

Static Solid Relaxation Ordered Spectroscopy: SS-ROSY

1
Department of Physics, Brooklyn College of the City University of New York, 2900 Bedford Avenue, Brooklyn, NY 11210, USA
2
Department of Physics, The Graduate Center of the City University of New York, 365 5th Ave, New York, NY 10016, USA
3
Schlumberger-Doll Research, 1 Hampshire Street, Cambridge, MA 02139, USA
*
Author to whom correspondence should be addressed.
Int. J. Mol. Sci. 2019, 20(23), 5888; https://doi.org/10.3390/ijms20235888
Received: 19 October 2019 / Revised: 19 November 2019 / Accepted: 21 November 2019 / Published: 24 November 2019
(This article belongs to the Special Issue NMR Characterization of Amorphous and Disordered Materials)
A two-dimensional pulse sequence is introduced for correlating nuclear magnetic resonance anisotropic chemical shifts to a relaxation time (e.g., T1) in solids under static conditions. The sequence begins with a preparatory stage for measuring relaxation times, and is followed by a multiple pulse sequence for homonuclear dipolar decoupling. Data analysis involves the use of Fourier transform, followed by a one-dimensional inverse Laplace transform for each frequency index. Experimental results acquired on solid samples demonstrate the general approach, and additional variations involving heteronuclear decoupling and magic angle spinning are discussed. View Full-Text
Keywords: inverse Laplace transform; multiple pulse NMR; correlation spectroscopy inverse Laplace transform; multiple pulse NMR; correlation spectroscopy
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MDPI and ACS Style

Boutis, G.S.; Kausik, R. Static Solid Relaxation Ordered Spectroscopy: SS-ROSY. Int. J. Mol. Sci. 2019, 20, 5888. https://doi.org/10.3390/ijms20235888

AMA Style

Boutis GS, Kausik R. Static Solid Relaxation Ordered Spectroscopy: SS-ROSY. International Journal of Molecular Sciences. 2019; 20(23):5888. https://doi.org/10.3390/ijms20235888

Chicago/Turabian Style

Boutis, Gregory S., and Ravinath Kausik. 2019. "Static Solid Relaxation Ordered Spectroscopy: SS-ROSY" International Journal of Molecular Sciences 20, no. 23: 5888. https://doi.org/10.3390/ijms20235888

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