Search Results (31)

This study proposes a multi-via structure as a loss-reduction design technique to mitigate current crowding in a slotless axial flux permanent magnet motor (AFPM) equipped with printed circuit board (PCB) stators. The PCB stator enables high current density operation through parallel copper-foil stacking and supports an ultra-compact structural configuration. However, current concentration in the via regions can increase copper loss and phase resistance. In this work, the via position and diameter were defined as design variables to perform a sensitivity analysis of current distribution and phase resistance variation. The effects of current density dispersion and the potential for copper loss reduction were evaluated using three-dimensional finite-element analysis (FEA). The results confirm that adopting a multi-via structure improves current path uniformity and reduces electrical losses, thereby enhancing overall efficiency. Furthermore, the analysis shows that excessive via enlargement or overuse does not necessarily yield optimal results and, in certain cases, may lead to localized current peaks. These findings demonstrate that the multi-via structure is an effective and appropriate design strategy for PCB stators and highlight the importance of optimized via placement tailored to each stator configuration. Full article

Nano-transfer printing (nTP) has emerged as an effective method for fabricating three-dimensional (3D) nanopatterns on both flat and non-planar substrates. However, most transfer-printed 3D patterns tend to exhibit non-discrete and/or non-porous structures, limiting their application in high-precision nanofabrication. In this study, we introduce a simple and versatile approach to produce highly ordered, porous 3D cross-bar arrays through precise control of the nTP process parameters. By selectively adjusting the polymer solution concentration and spin-coating conditions, we successfully generated discrete, periodic line patterns, which were then stacked at a 90-degree angle to form a porous 3D cross-bar structure. This technique enabled the direct transfer printing of PMMA line patterns with well-defined, square-arrayed holes, without requiring additional deposition of functional materials. This method was applied across diverse substrates, including planar Si wafers, flexible PET, metallic copper foil, and transparent glass, demonstrating its adaptability. These well-defined 3D cross-bar patterns enhance the versatility of nTP and are anticipated to find broad applicability in various nano-to-microscale electronic devices, offering high surface area and structural precision to support enhanced functionality and performance. Full article

Biopolymer blends of polylactic acid (PLA) and polybutylene adipate-co-terephthalate (PBAT) are extruded into flexible monolayer films. These blends are excellent candidates for the realization of environmentally friendly packaging applications. A necessary pre-requisite for that are appropriate tribological properties under mechanical contact. Reasonable wear resistance allows good protection of packed goods, and low friction forces reduce difficulties in stacking. In this research, mechanical embossment under high loads at room temperature was used for the modification of polymer surfaces to exhibit a significant friction reduction under dry conditions. The results particularly show a systematic decrease in the coefficient of friction for biopolymer blends containing 30 wt% and 40 wt% PBAT. FTIR was used to analyze the change in surface composition after mechanical embossing. A sophisticated FTIR calibration method revealed that the blend with 30 wt% PBAT shows a modified distribution of PBAT and PLA at the surface due to mechanical embossment. This leads to a controlled and long-lasting modification of the surface properties without a substantial change in the chemical composition of the polymer in bulk. Without the use of additional coatings, biodegradable packaging foils with improved characteristics are accessible. Full article

Bacterial adhesion and biofilm maturation is significantly influenced by surface properties, encompassing both bare surfaces and single or multi-layered coatings. Hence, there is an utmost interest in exploring the intricacies of gene regulation in sulfate-reducing bacteria (SRB) on copper and graphene-coated copper surfaces. In this study, Oleidesulfovibrio alaskensis G20 was used as the model SRB to elucidate the pathways that govern pivotal roles during biofilm formation on the graphene layers. Employing a potent reporter green fluorescent protein (GFP) tagged to O. alaskensis G20, the spatial structure of O. alaskensis G20 biofilm on copper foil (CuF), single-layer graphene-coated copper (Cu-GrI), and double-layer graphene-coated copper (Cu-GrII) surfaces was investigated. Biofilm formation on CuF, Cu-GrI, and Cu-GrII surfaces was quantified using CLSM z-stack images within COMSTAT v2 software. The results revealed that CuF, Cu-GrI, and Cu-GrII did not affect the formation of the GFP-tagged O. alaskensis G20 biofilm architecture. qPCR expression showed insignificant fold changes for outer membrane components regulating the quorum-sensing system, and global regulatory proteins between the uncoated and coated surfaces. Notably, a significant expression was observed within the sulfate reduction pathway confined to dissimilatory sulfite reductases on the Cu-GrII surface compared to the CuF and Cu-GrI surfaces. Full article

As the prime candidate for plasma-facing materials (PFM), the response of tungsten (W) to thermal shock loads is an important research topic for future fusion devices. Under heat loads, the surface of tungsten plasma-facing materials (W-PFM) can experience thermal damage, including brittle cracking and fatigue cracks. Therefore, exploring solutions for thermal damage of W-PFM remains one of the current research focuses. We propose a novel approach to mitigate thermal radiation damage in PFM, namely, the stacked structure W-PFM. The surface thermal stress distribution of the stacked structure W-PFM under heat loads was simulated and analyzed by the finite element method. As the foil thickness decreases, both the peak thermal stresses in the normal direction (ND) and rolling direction (RD) decrease. When the thickness decreases to a certain value, the peak thermal stress in the RD decreases to about 1384 MPa and no longer decreases; while the peak thermal stress in the ND approaches 0 MPa and can be neglected. In the range of approximately 5–100 mm, the accumulated equivalent plastic strain decreases sharply as the thickness decreases; in other thickness ranges, it decreases slowly. Thermal fatigue experiments were conducted on the stacked structure W composed of W foils with different thicknesses and bulk W using an electron beam facility. The samples were applied with a power density of 30 MW/m² for 10,000 and 20,000 pulses. The cracks on the surface of the stacked structure W extended along the ND direction, while on the surface of bulk W, besides the main crack in the ND direction, a crack network also formed. The experimental results were consistent with finite element simulations. When the pulse number was 10,000, as the thickness of the W foil decreased, the number and width of the cracks on the surface of the stacked structure W decreased. Only four small cracks were present on the surface of stacked structure W (0.05 mm). When the pulse number increased to 20,000, the plastic deformation and number of cracks on the surface of all samples increased. However, the stacked structure W (0.05 mm) only added one small crack and had the smallest surface roughness (Ra = 1.536 μm). Quantitative analysis of the fatigue cracks showed that the stacked structure W-PFM (0.05 mm) exhibited superior thermal fatigue performance. Full article

In this paper, we proposed a miniature quadrupedal piezoelectric robot with a mass of 1.8 g and a body length of 4.6 cm. The robot adopts a novel spatial parallel mechanism as its transmission. Each leg of the robot has two degrees of freedom (DOFs): swing and lift. The trajectory necessary for walking is achieved by the appropriate phasing of these two DOFs. A new manufacturing method for piezoelectric actuators was developed. During the stacking process, discrete patterned PZT pieces are used to avoid dielectric failure caused by laser cutting. Copper-clad FR-4 is used as the solder pad instead of copper foil, making the connection between the pad and the actuator more reliable. The lift powertrain of the robot was modeled and the link length of the powertrain was optimized based on the model. The maximum output force of each leg can reach 26 mN under optimized design parameters, which is 1.38 times the required force for successful walking. The frequency response of the powertrain was measured and fitted to the second-order system, which enabled increased leg amplitudes near the powertrain resonance of approximately 70 Hz with adjusted drive signals. The maximum speed of the robot without load reached 48.66 cm/s (10.58 body lengths per second) and the payload capacity can reach 5.5 g (3.05 times its mass) near the powertrain resonance. Full article

Bast fibre-reinforced plastics are characterised by good strength and stiffness but are often brittle due to the stiff and less ductile fibres. This study uses a biomimetic approach to improve impact strength. Based on the structure of the spicules of a deep-sea glass sponge, in which hard layers of bioglass alternate with soft layers of proteins, the toughness of kenaf/epoxy composites was significantly improved by a multilayer structure of kenaf and cellulose acetate (CA) foils as impact modifiers. Due to the alternating structure, cracks are deflected, and toughness is improved. One to five CA foils were stacked with kenaf layers and processed to composite plates with bio-based epoxy resin by compression moulding. Results have shown a significant improvement in toughness using CA foils due to increased crack propagation. The unnotched Charpy impact strength increased from 9.0 kJ/m² of the pure kenaf/epoxy composite to 36.3 kJ/m² for the sample containing five CA foils. The tensile and flexural strength ranged from 74 to 81 MPa and 112 to 125 MPa, respectively. The tensile modulus reached values between 9100 and 10,600 MPa, and the flexural modulus ranged between 7200 and 8100 MPa. The results demonstrate the successful implementation of an abstract transfer of biological role models to improve the toughness of brittle bast fibre-reinforced plastics. Full article

The cross-sections of the ⁴⁸Ti(p,x)⁴⁷Sc, ^46cSc, ^44mSc, ^44gSc, ⁴³Sc, and ⁴⁸V nuclear reactions were measured from 18 to 70 MeV, with particular attention to ⁴⁷Sc production. Enriched ⁴⁸Ti powder was deposited on an aluminum backing and the obtained targets were characterized via elastic backscattering spectroscopy at the INFN-LNL. Targets were exposed to low-intensity proton irradiation using the stacked-foils technique at the ARRONAX facility. Activated samples were measured using γ-spectrometry; the results were compared with the data int he literature and the theoretical TALYS-based values. A regular trend in the new values obtained from the different irradiation runs was noted, as well as a good agreement with the literature data, for all the radionuclides of interest: ⁴⁷Sc, ^46cSc, ^44mSc, ^44gSc, ⁴³Sc, and ⁴⁸V. ⁴⁷Sc production was also discussed, considering yield and radionuclidic purity, for different ⁴⁷Sc production scenarios. Full article

A series of Mg-Y-Ni alloys with different volume fractions of long-period stacking-ordered (LPSO) phase were prepared, by controlling the alloy composition, heat treatment, and single-pass extrusion, to assess the influence of increasing LPSO phase volume fraction on the hydrogen absorption and desorption properties of the extruded alloys. The LPSO phase volume fraction in the alloys increased with increasing solute concentration, from ~24% LPSO in Mg₉₇Y₂Ni₁ (at.%) to ~60% LPSO in Mg₉₃Y₄Ni₃ (at.%) up to ~92% LPSO in Mg₉₁Y₅Ni₄ (at.%). The most refined microstructure was obtained in the alloy with highest volume fraction of LPSO phase. After 100 s at 300 °C, the Mg₉₁Y₅Ni₄ alloy absorbed 4.6 ± 0.2 wt.% H while the Mg₉₇Y₂Ni₁ and Mg₉₃Y₄Ni₃ alloys each absorbed 3.8 ± 0.2 wt.% H. After 10,000 s at 300 °C, all three alloys had absorbed a maximum of 5.3 ± 0.2 wt.% H with no further significant difference in hydrogen absorption kinetics. The Mg₉₁Y₅Ni₄ alloy desorbed 1.8 ± 0.2 wt.% H after 100 s at 300 °C against a vacuum while the Mg₉₇Y₂Ni₁ and Mg₉₃Y₄Ni₃ alloys desorbed 0.8 ± 0.2 wt. H and 0.6 ± 0.2 wt.% H, respectively. After 10,000 s at 300 °C, the Mg₉₁Y₅Ni₄ and Mg₉₇Y₂Ni₁ alloys completely desorbed 5.2 ± 0.2 wt.% H and 5.4 ± 0.2 wt.% H, respectively, but the Mg₉₃Y₄Ni₃ alloy desorbed only 3.7 ± 0.2 wt.% H. Hydrogen absorption and desorption kinetics were fastest in the Mg₉₁Y₅Ni₄ alloy with the highest LPSO volume fraction, but no consistent trend with LPSO phase volume fraction was observed with the Mg₉₃Y₄Ni₃ alloy, which showed the slowest absorption and desorption kinetics. The hydrogen pressures corresponding to metal–hydride equilibrium did not vary with LPSO phase volume fraction or alloy composition, indicating that the (de)hydrogenation thermodynamics were not significantly changed in any of the alloys. Hydrogen absorption experiments with thin foils, made of extruded Mg₉₁Y₅Ni₄ alloy with the highest LPSO phase fraction, demonstrated that the LPSO structures decompose into Mg phase, Mg₂Ni phase, lamellar Mg/Mg-Y structures, and YH_x particles. This study shows that hydrogen kinetics can be impacted in Mg-Y-Ni alloys by controlling the LPSO phases using common metallurgical techniques. Full article

Nickel hydroxide β-Ni(OH)₂ nanolamellae with high aspect ratios were grown via chemical bath deposition (CBD) on both smooth and textured nickel foil. Depending on bath composition and/or the presence of an additive, thin foam-like nanolamellae to stacked lamellae were obtained. The used CBD method is highly cost-effective, as it is faster and requires less chemicals than typical hydrothermal methods, and it is readily implementable for large-scale production. The influence of surface texture on the final morphology and its effect on capacitive performance was investigated. Herein, we show how subtle changes in the concentration can drastically influence the morphology, which, in turn, drastically impacts the supercapacitive performance of the electrode. Also, the use of a textured surface significantly impacts the morphology, with vastly better cycling performance than samples made on a relatively smooth substrate. The measured specific capacitance values of the best sample were 1961 Fg⁻¹ at 5 mVs⁻¹ and 1998 Fg⁻¹ at 1 Ag⁻¹ under potentiostatic and galvanostatic conditions, respectively. This sample also retained 100% of its initial specific capacitance when discharged at a very high current density of 40 Ag⁻¹. These values are substantially enhanced compared to previously reported data using a nearly analogous method (CBD with higher reagent conc.), with our method, cost-wise, offering economic advantages relative to results obtained with similar materials and other methods (e.g., hydrothermal). Full article

The irradiation of ¹⁷⁶Yb with deuterons offers a promising pathway for the production of the theranostic radionuclide ¹⁷⁷Lu. To optimize this process, calculations integrating deuteron transport, isotope production, and decay have been performed. In pure ¹⁷⁶Yb, the undesired production of ^174g+mLu occurs at higher deuteron energies, corresponding to a distribution slightly shallower than that of ¹⁷⁷Lu. Hence, ^174g+mLu can be effectively filtered out by employing either a low-energy deuteron beam or stacked foils. The utilization of stacked foils enables the production of ¹⁷⁷Lu using a high-energy linear accelerator. Another unwanted isotope, ^176mLu, is produced roughly at the same depth as ¹⁷⁷Lu, but its concentration can be significantly reduced by selecting an appropriate post-irradiation processing time, owing to its relatively short half-life. The modeling approach extended to the mapping of yields as a function of irradiation time and post-irradiation processing time. An optimized processing time window was identified. The study demonstrates that a high-energy deuteron beam can be employed to produce ¹⁷⁷Lu with high specific activity exceeding 3000 GBq/mg. The effect of different purity levels (ranging from 98% to 100%) was also discussed. The impurity levels have a slight impact. The modeling demonstrates the feasibility of obtaining ¹⁷⁷Lu with a specific activity > 3000 GBq/mg and radionuclidic purity > 99.5% when using a commercially available ¹⁷⁶Yb target of 99.6% purity. Full article

SiO₂ films were grown to thicknesses below 15 nm by ozone-assisted atomic layer deposition. The graphene was a chemical vapor deposited on copper foil and transferred wet-chemically to the SiO₂ films. On the top of the graphene layer, either continuous HfO₂ or SiO₂ films were grown by plasma-assisted atomic layer deposition or by electron beam evaporation, respectively. Micro-Raman spectroscopy confirmed the integrity of the graphene after the deposition processes of both the HfO₂ and SiO₂. Stacked nanostructures with graphene layers intermediating the SiO₂ and either the SiO₂ or HfO₂ insulator layers were devised as the resistive switching media between the top Ti and bottom TiN electrodes. The behavior of the devices was studied comparatively with and without graphene interlayers. The switching processes were attained in the devices supplied with graphene interlayers, whereas in the media consisting of the SiO₂-HfO₂ double layers only, the switching effect was not observed. In addition, the endurance characteristics were improved after the insertion of graphene between the wide band gap dielectric layers. Pre-annealing the Si/TiN/SiO₂ substrates before transferring the graphene further improved the performance. Full article

The present paper aims to address the crucial concern of pollution induced by growing plastic waste and electromagnetic interference (EMI). Nanocomposites combining poly(lactic acid) (PLA) and organo-modified montmorillonite (OMMT) are synthesized and compression molded into thin films. A first set of samples, referred as virgin, was kept as is, while a second set of samples were photochemically, thermally and hydrolytically aged before mechanical recycling via extruding and second compression molding, resulting in the so-called recycled composite. The electromagnetic (EM) properties with a focus on microwave absorption performances of virgin and recycled samples are compared for various thicknesses and weight concentrations of OMMT in PLA matrix. The EM performances are gauges by Rozanov and Salisbury structures that consist in one- and two-layer stacks of composite films back-coated by a metal foil. Characterization in Rozanov configuration shows an average absorption index over the Ka band of 29.3% and 21.1% for, respectively, virgin and recycled PLA reinforced with 4 wt.% OMMT. An optimization of the film thickness is proposed; up to 61.85% and 80% of absorption with a thickness of 1.4 mm and 3.75 mm, respectively, is reached with a metal back-coated rPLA-4%OMMT film. Characterization in Salisbury configuration gives advantage to the recycled structure with an average absorption of 49.6% for a total thickness of 1.4 mm. The requirements of EMI shielding are met by PLA-OMMT composites with a certain benefit of recycling process on EM performance. Full article

In the present study, graphene oxide foils 10 μm thick have been irradiated in vacuum using same charge state (one charge state) ions, such as protons, helium and oxygen ions, at the same energies (3 MeV) and fluences (from 5 × 10¹¹ ion/cm² to 5 × 10¹⁴ ion/cm²). The structural changes generated by the ion energy deposition and investigated by X-ray diffraction have suggested the generation of new phases, as reduced GO, GO quantum dots and graphitic nanofibers, carbon nanotubes, amorphous carbon and stacked-cup carbon nanofibers. Further analyses, based on Rutherford Backscattering Spectrometry and Elastic Recoil Detection Analysis, have indicated a reduction of GO connected to the atomic number of implanted ions. The morphological changes in the ion irradiated GO foils have been monitored by Transmission Electron, Atomic Force and Scanning Electron microscopies. The present study aims to better structurally, compositionally and morphologically characterize the GO foils irradiated by different ions at the same conditions and at very low ion fluencies to validate the use of GO for radiation detection and propose it as a promising dosimeter. It has been observed that GO quantum dots are produced on the GO foil when it is irradiated by proton, helium and oxygen ions and their number increases with the atomic number of beam gaseous ion. Full article

The reliable production of high-quality lithium-ion battery components still poses a challenge, which must be met to cope with their rising demand. One key step in the production sequence is the process of cell-internal contacting, during which the electrode carrier foils of the anode and the cathode are joined with the arrester. This is usually done with ultrasonic or laser beam welding. Both joining processes, however, show limitations concerning the quality of the weld. This paper presents a new approach for cell-internal contacting by using micro-friction stir spot welding. Welding experiments were conducted in which joints with high mechanical strengths were produced. It was also shown that large stacks with foil numbers of 100 can be joined in only a few tenths of a second. The process is therefore especially of interest for the fast production of large-scale battery cells or other new types of high-energy-dense battery cells. Full article