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Keywords = glass carbomer

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19 pages, 4297 KiB  
Article
Bioactivity of Glass Carbomer Versus Conventional GICs in Sound Enamel and Dentine: A 12-Month SEM-EDS Study
by Dubravka Turjanski, Suzana Jakovljević, Dragutin Lisjak, Petra Bučević Sojčić, Fran Glavina, Kristina Goršeta and Domagoj Glavina
Materials 2025, 18(15), 3580; https://doi.org/10.3390/ma18153580 - 30 Jul 2025
Viewed by 192
Abstract
Glass ionomer cements (GICs) are bioactive restorative materials valued for their sustained ion release and remineralisation capacity. However, their long-term interactions with sound enamel and dentine remain underexplored. This 12-month in vitro study aimed to evaluate microstructural and compositional changes in sound dental [...] Read more.
Glass ionomer cements (GICs) are bioactive restorative materials valued for their sustained ion release and remineralisation capacity. However, their long-term interactions with sound enamel and dentine remain underexplored. This 12-month in vitro study aimed to evaluate microstructural and compositional changes in sound dental tissues adjacent to four GICs—Ketac Universal, Fuji IX and Equia Forte Fil (conventional GICs) and the advanced Glass Carbomer (incorporating hydroxyapatite nanoparticles)—using field-emission scanning electron microscopy (FE-SEM) and energy-dispersive X-ray spectroscopy (EDS). Glass Carbomer uniquely formed hydroxyapatite nanoparticles and mineralised regions indicative of active biomineralisation—features not observed with conventional GICs. It also demonstrated greater fluoride uptake into dentine and higher silicon incorporation in both enamel and dentine. Conventional GICs exhibited filler particle dissolution and mineral deposition within the matrix over time; among them, Equia Forte released the most fluoride while Fuji IX released the most strontium. Notably, ion uptake was consistently higher in dentine than in enamel for all materials. These findings indicate that Glass Carbomer possesses superior bioactivity and mineralising potential which may contribute to the reinforcement of sound dental tissues and the prevention of demineralisation. However, further in vivo studies are required to confirm these effects under physiological conditions. Full article
(This article belongs to the Special Issue Antibacterial Dental Materials)
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14 pages, 4152 KiB  
Article
Mechanical Properties of Nano-Crystalline Glass-Carbomer Cements Used in Dentistry
by Małgorzata Karolus, Adrian Barylski, Magdalena Fryc and Damian Strzelec
Materials 2024, 17(5), 1186; https://doi.org/10.3390/ma17051186 - 4 Mar 2024
Viewed by 1344
Abstract
The main aim of this study was to assess the impact of the environment on the mechanical and tribological properties of glass-carbomer cements used in dentistry. The properties of the Glass Cements Polyalkene (GCP) Glass Fill material, belonging to glass-polyalkene cements, were tested [...] Read more.
The main aim of this study was to assess the impact of the environment on the mechanical and tribological properties of glass-carbomer cements used in dentistry. The properties of the Glass Cements Polyalkene (GCP) Glass Fill material, belonging to glass-polyalkene cements, were tested after placing it in various environments: air, distilled water, artificial saliva simulating a neutral environment (pH = 7), and simulating inflammation (pH = 4). The research material included four samples and a two-year reference material. The analysis of volumetric consumption and the assessment of the impact of solubility on the stability of glass-carbomer cements were carried out using tribological measurements and Vickers hardness measurements. In addition, microstructural characterization of the materials was performed using scanning electron microscopy (SEM). It was observed that the lowest wear (0.04%), the most stable microstructure, and the lowest average hardness (21.52 HV 0.1) were exhibited by the material stored in artificial saliva simulating a neutral environment (pH = 7). The least stable microstructure and statistically the highest hardness (77.3 HV 0.1) was observed in the test sample, which was stored in air for two years and then in distilled water. The highest consumption (0.11%) was recorded in the case of cement placed in artificial saliva simulating inflammation (pH = 4). The results obtained in this study indicate specific trends in the influence of the environment in which the tested cement is located, such as air, distilled water, air/distilled water, artificial saliva simulating a neutral environment, and simulating inflammation, on its structure, hardness, and wear. Full article
(This article belongs to the Special Issue Biomaterials and Mechanics in Dentistry)
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14 pages, 17211 KiB  
Article
Adhesion and Surface Roughness of Apatite-Containing Carbomer and Improved Ionically Bioactive Resin Compared to Glass Ionomers
by Handan Yıldırım Işık and Aylin Çilingir
J. Funct. Biomater. 2023, 14(7), 367; https://doi.org/10.3390/jfb14070367 - 12 Jul 2023
Cited by 3 | Viewed by 1689
Abstract
The surface roughness of different glass–ionomer-based materials and their shear bond strength with a resin composite with and without thermal cycling were evaluated. Ketac Molar (KM, 3M ESPE, St. Paul, MN, USA), Glass Carbomer (GC, GCP Dental, Leiden, The Netherlands), Bioactive (BA, PULPDENT, [...] Read more.
The surface roughness of different glass–ionomer-based materials and their shear bond strength with a resin composite with and without thermal cycling were evaluated. Ketac Molar (KM, 3M ESPE, St. Paul, MN, USA), Glass Carbomer (GC, GCP Dental, Leiden, The Netherlands), Bioactive (BA, PULPDENT, Corporation, Watertown, MA, USA) and Fuji II LC (FJ, GC, Tokyo, Japan) were used to prepare the specimens and they were kept in distilled water at 37 °C for 24 h. The surface roughness of the specimens was measured with a profilometer (n = 6). A universal adhesive resin was applied on glass–ionomer materials and cylindrical universal composites were applied and polymerized, respectively (n = 16). The specimens were divided into two subgroups. The first subgroup was subjected to thermal cycling. Shear bond strength was investigated for both subgroups (n = 8). Stereomicroscopy and SEM examinations were performed. The roughest surface was obtained in the GC group (p < 0.05). The shear bond strength of the specimens without thermal cycling was higher than that of those with thermal cycling (p < 0.05). The lowest shear bond was measured in the GC group (p < 0.05). Although FJ, KM and BA have been observed to be suitable materials for clinical use, BA, in particular, is evidenced to become the best option among the materials we tested. GC cement’s long-term performance needs to be improved. Full article
(This article belongs to the Special Issue Resin-Matrix Composites and Cements for Dental Restorations)
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8 pages, 319 KiB  
Article
Retention Ability of a Glass Carbomer Pit and Fissure Sealant
by Liana Beresescu, Monika Kovacs, Alexandru Vlasa, Alexandra Mihaela Stoica, Csilla Benedek, Mihai Pop, Denisa Bungardean and Daniela Eșian
Int. J. Environ. Res. Public Health 2022, 19(4), 1966; https://doi.org/10.3390/ijerph19041966 - 10 Feb 2022
Cited by 7 | Viewed by 2658
Abstract
Dental sealants are an excellent means to prevent pits and fissure decay. Currently, there are multiple commercially available sealant materials. The purpose of this study was to assess the retention of glass carbomer fissure sealant and the incidence of secondary caries over a [...] Read more.
Dental sealants are an excellent means to prevent pits and fissure decay. Currently, there are multiple commercially available sealant materials. The purpose of this study was to assess the retention of glass carbomer fissure sealant and the incidence of secondary caries over a period of 24 months in comparison with a resin-based sealant. Materials and Methods: We included 32 children in the study, with ages between six and eight years and an average age of 6.8 years old. For each child, we sealed four permanent molars (totaling 128 teeth). The study group was divided into sub-groups. Sub-group A was represented by 64 first permanent molars which underwent dental sealing procedures with composite resin-based fissure sealant, Helioseal F™, and sub-group B was represented by 64 first permanent molars which underwent dental sealing procedures with glass carbomer cement, GCP Glass Seal™. The sealants were assessed clinically at 6, 12, 18, and 24 months. Results: The 6-month follow-up evaluation showed no statistically significant differences between the two materials neither regarding sealant retention nor new carious lesions formation (p > 0.05). At the 12-month recall, 57 molars had good retention (89.06%) from sub-group A and 44 molars (68.75%) from sub-group B; there was a statistically significant difference (p = 0.0187) between the two treatment choices only regarding material retention. At the last recall after 2 years, sub-group A had a higher number of molars with perfect sealing (47–73.43%) and 8 molars (12.5%) with new caries lesions and sub-group B had 23 (35.93%) molars with perfect sealing and 15 molars (23.44%) with new caries lesions; there was a statistically significant difference (p < 0.0001) between the two treatment choices only regarding material retention. Conclusions: The glass carbomer retention is very inferior to the resin-based material. The glass carbomer sealant was effective in preventing new caries development, comparable with the conventional resin-based sealant. Full article
(This article belongs to the Special Issue Dental Public Health: Issues, Challenges and Opportunities)
15 pages, 516 KiB  
Review
A Review of Glass-Ionomer Cements for Clinical Dentistry
by Sharanbir K. Sidhu and John W. Nicholson
J. Funct. Biomater. 2016, 7(3), 16; https://doi.org/10.3390/jfb7030016 - 28 Jun 2016
Cited by 390 | Viewed by 38569
Abstract
This article is an updated review of the published literature on glass-ionomer cements and covers their structure, properties and clinical uses within dentistry, with an emphasis on findings from the last five years or so. Glass-ionomers are shown to set by an acid-base [...] Read more.
This article is an updated review of the published literature on glass-ionomer cements and covers their structure, properties and clinical uses within dentistry, with an emphasis on findings from the last five years or so. Glass-ionomers are shown to set by an acid-base reaction within 2–3 min and to form hard, reasonably strong materials with acceptable appearance. They release fluoride and are bioactive, so that they gradually develop a strong, durable interfacial ion-exchange layer at the interface with the tooth, which is responsible for their adhesion. Modified forms of glass-ionomers, namely resin-modified glass-ionomers and glass carbomer, are also described and their properties and applications covered. Physical properties of the resin-modified glass-ionomers are shown to be good, and comparable with those of conventional glass-ionomers, but biocompatibility is somewhat compromised by the presence of the resin component, 2 hydroxyethyl methacrylate. Properties of glass carbomer appear to be slightly inferior to those of the best modern conventional glass-ionomers, and there is not yet sufficient information to determine how their bioactivity compares, although they have been formulated to enhance this particular feature. Full article
(This article belongs to the Collection Biocements for Medical/Dental Purposes)
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