Search Results (44)

A novel parameter optimization method for additively manufacturing nickel–titanium (NiTi) alloys using laser powder bed fusion (LBPF) was developed. Compared with the conventional NiTi alloy and the previously reported LPBF-NiTi alloy, the LBPF-NiTi alloy prepared with these parameters exhibits excellent tensile properties and an anisotropic microstructure. Since distinct regions of orthopedic implants have specific functional requirements, we investigated the anisotropy of this LPBF-NiTi in terms of its osteoinductive capacity to determine the appropriate building direction for prosthesis fabrication. The biosafety of the transverse (XY-NiTi) and longitudinal (XZ-NiTi) planes was assessed through cytotoxicity assays. Comparative analyses of the biological activities of these planes were conducted by evaluating the adherent cell counts, the adhesion morphology, and the expression of osteogenic-related genes and factors in adherent cells. Compared with XZ-NiTi, XY-NiTi exhibited superior cell adhesion properties. Additionally, the expression levels of osteogenic markers (RUNX2, ALP, OPG, and OCN) were significantly greater in bone marrow mesenchymal cells (BMMCs) adhered to XY-NiTi than in those adhered to XZ-NiTi. These results indicate a greater osteogenic potential in the XY-NiTi group. XY-NiTi was more advantageous as an implant–bone contact surface. Building implant products in the direction perpendicular to the load-bearing axis enhances biofixation; thus, this is the preferred orientation for manufacturing orthopedic implants. Full article

The inherent mineralogical alignment in stratified rock formations engenders pronounced mechanical anisotropy, presenting persistent challenges across geological, geotechnical, and petroleum engineering disciplines. While substantial progress has been made in modeling transversely isotropic media, current methodologies exhibit limitations in reconciling theoretical predictions with complex failure mechanisms. This investigation examines the anisotropic response of diverse lithologies through triaxial testing across bedding orientations (0–90°) and confinement levels (0–60 MPa), revealing a pressure-dependent attenuation of directional strength variations. Experimental evidence identifies three dominant failure modes: cross-bedding shear fracturing, bedding-parallel sliding, and hybrid mechanisms combining both, with transition thresholds governed by confinement intensity and bedding angle. Analytical comparisons demonstrate that conventional single weakness plane models produce characteristic shoulder-shaped strength curves with overpredictions, particularly in hybrid failure regimes. Conversely, the modified patchy weakness plane formulation achieves superior predictive accuracy through parametric representation of anisotropy gradation, effectively capturing strength transitions between end-member failure modes. The Pariseau criterion, though marginally less precise in absolute terms, provides critical insights into directional strength contrasts through its explicit differentiation of vertical versus parallel bedding responses. These findings advance the fundamental understanding of anisotropic rock behavior while establishing practical frameworks for optimizing stability assessments in bedded formations, particularly in high-confinement environments characteristic of deep reservoirs and engineered underground structures. Full article

Shear failure is pivotal in fracture evolution and stimulated reservoir volume (SRV) during hydraulic fracturing, particularly in bedded shale formations. However, the limited availability of coupled macro- and mesoscale experimental data on the shear behavior of reservoir shale constrains a comprehensive understanding of its anisotropic shear mechanical properties across scales. This study systematically investigates shear anisotropy at both macro- and mesoscales in shale with varying bedding orientations under different normal stress conditions. The key findings are summarized as follows: (1) At lower normal stresses, the anisotropy of peak shear strength was more pronounced, whereas the anisotropy of residual shear strength was relatively weak. As the normal stress increased, the anisotropic effects of bedding on peak and residual shear strengths exhibited opposite trends. The former exhibited a fluctuating decline, whereas the latter showed a progressive increase. (2) The internal friction angle of shale bedding planes was higher than that of the matrix, whereas cohesion exhibited the opposite trend. The internal friction angle corresponding to the peak shear strength reached its maximum at a bedding angle of 45°, while cohesion peaked at a bedding angle of 60°. (3) At lower normal stresses, the cumulative acoustic emission (AE) ringing count curves for shale shear failure followed an “S”-shaped pattern for bedded and matrix shear, differing from the piecewise linear pattern observed in bedded-matrix coupled shear. As the normal stress increased, the bedding-induced effects on macro- and mesoscale shear behavior evolved from non-uniformity to uniformity, reflecting a transition of anisotropy from uncoordinated to coordinated characteristics. Full article

The purpose of this study is to investigate the effects of process parameters on the microstructure and mechanical properties of the Hastelloy X (HX) alloy using a laser powder bed fusion (L-PBF) process. A combined experimental and numerical approach was used to evaluate the influence of the energy density distribution and temperature evolution on the microstructure, defects, and mechanical properties. After the specimens were built on SUS304 substrate by the L-PBF, the microstructure and defects in the specimens were analyzed by SEM and EBSD analysis methods, and then the hardness and the tensile tests were performed. The cooling rate under different laser conditions was obtained by the finite element method (FEM). The results show that a low volume energy density (VED) was applied to the unmelted powder particles, and a high energy density resulted in spherical defects. In addition, the microstructures were found to coarsen with increasing the energy density along with a tendency to strengthen the (001) texture orientation in both x–y and x–z planes. Compared to the parts with the thermal history from numerical results, the low cooling rate with high energy density had larger crystal grains elongated along the building direction, coarser sub-grains, resulting in a reduction in microhardness and yield strength together with an increase in elongation for the L-PBF HX alloy. The presented results provide new insights into the effects of parameters and the cooling rates. It can play an important role in optimizing the L-PBF processing parameters, identifying the cause of defects, and controlling the cooling rates for the crystallographic texture in such a way as to guide the development of better metrics for designing processing parameters with the desired mechanical properties. Full article

Large-scale hydraulic fracturing is a prevalent technique for exploiting low-porosity and low-permeability shale reservoirs. The propagation and morphology of the hydraulic fracture in the laminated shale formations are significantly influenced by densely developed bedding planes, which can be classified into three categories: continuous, transitional, and discontinuous, with each characterized by distinct properties. This categorization complicates the prediction of the fracture propagation and the optimization of fracturing plans. In this research, a comparative study was proposed to describe fracture propagation and morphology in laminated shale with different types of bedding planes, employing the hydromechanically coupled discrete element method (DEM). The simulation results revealed that bedding planes of different types produce distinct impacts on the fracture propagation, leading to diverse fracture morphologies. In particular, it was found that the plane thickness affected the fracture propagation under low permeability, but the impact was insignificant under high permeability. Under different orientation angles, the continuous bedding planes showed distinct impacts on fracture propagation, while the transitional and discontinuous bedding planes consistently captured the hydraulic fracture. Moreover, the fluid viscosity and injection rate significantly influenced continuous and transitional bedding planes while having a minor effect on the discontinuous bedding planes. The optimal injection schemes incorporating varying injection rates or fluid viscosities were investigated. In addition, the impacts of small-scale bedding planes on fracture propagation were revealed. Furthermore, the bottom hole pressure variation and seismic event distribution were presented to provide complementary evidence of the fracture propagation. The simulation results can promote a comprehensive understanding of the fracture development in shale reservoirs. Full article

The Laser Powder-Bed Fusion Additive Manufacturing (LPBF AM) technique is evaluated for the manufacturing of fully metallic monolithic microwave components. To validate the manufacturing technique, a difference pattern array of 4 × 4 horn antennas is designed to operate at mm-Wave frequencies. The antenna is based on H-plane power dividers and a complex structure to obtain a difference radiation pattern by rotating twisted sections in two different orientations. The prototype is manufactured with a monolithic piece of aluminum alloy AlSi10Mg, providing a lightweight single structure that includes both radiating elements and a feeding network consisting of twisters and power dividers in a waveguide. The prototype was experimentally evaluated in an anechoic chamber and the near-field planar acquisition range, obtaining good agreement with full-wave simulations within an operational bandwidth from 34 to 36 GHz. The results demonstrate that the LPBF AM technique is a suitable candidate to produce challenging monolithic metal-only microwave components in the ${\mathrm{K}}_{\mathrm{a}}$-band, such as monopulse antennas. Full article

This study thoroughly investigated the compressive and tensile strength characteristics of black shale using both experimental and analytical approaches. Uniaxial compression tests were conducted to determine the elastic constants of black shale modeled as idealized, linear elastic, homogeneous, and transversely isotropic. Additionally, Brazilian tests were carried out on shale, considering it a transversely isotropic material. Strain measurements were recorded at the center of disc specimens subjected to diametric loading. By placing strain gages at the disc centers, the five elastic constants were accurately estimated. The effects of experimental methods and diametric loading on the elastic constant determination were evaluated and analyzed, and the indirect shear strength of the black shale, considering anisotropy, was determined using the estimated stress concentration coefficient. This study revealed that the indirect tensile strength of black shale is significantly influenced by the angle between the anisotropic planes and the diametric loading direction. Moreover, it was revealed that the stress concentration coefficients for anisotropic rocks vary from those of isotropic rocks, depending on the inclination angle of the bedding planes. This study confirms that the shear (tensile) strength of anisotropic black shale is not constant but varies with the orientation of the anisotropic planes in relation to the applied load. Full article

Laser Powder Directed Energy Deposition (LP-DED) can produce thin-wall features on the order of 1 mm. These features are essential for large structures operating in extreme environments such as regeneratively cooled nozzles and heat exchangers, which often make use of refractory metals. In this work, the mechanical behavior of LP-DED C103 was investigated via quasi-static tensile testing and low cycle fatigue (LCF) testing. The effects of vacuum stress relief (SR) and hot isostatic pressing (HIP) heat treatments were investigated for specimens in the vertical and horizontal build orientations during tensile testing. The AB and SR properties were lower than literature values for wrought and laser powder bed fusion (L-PBF) bulk components but higher than electron beam powder bed fusion (EB-PBF). The application of a HIP cycle improved strength by 7% and ductility by 27% past the initial as-built condition. Fracture images reveal that interlayer stress concentration sites are responsible for fracture in specimens in the vertical orientation. Meanwhile, fracture in the horizontal specimens mainly propagates at a slanted angle typical of plane stress conditions. The LCF results show cycles to failure ranging from 100 cycles to 8000 cycles for max strain levels of 2% and 0.5%, respectively. Fractography on the fatigue specimens reveals an increasing propagation zone as max strain levels are increased. The impact of these findings and future work are discussed in detail. Full article

Shale is composed of a rock matrix and bedding planes with a layered structure, resulting in significant anisotropy in its mechanical properties. In order to study the anisotropic mechanical properties of shale, the shale samples were prepared in different orientations with respect to the bedding planes, and the composition and microstructure of shale were first analyzed by X-ray diffractometer (XRD) and scanning electron microscope (SEM), and then the uniaxial and triaxial compression experiment on shale samples with five different bedding angles (the angle between the loading direction and the normal direction of the bedding planes, 0°, 30°, 45°, 60°, and 90°) were conducted under five confining pressures (0, 10, 20, 30, and 40 MPa), respectively; meanwhile, the acoustic emission (AE) test was carried out in the uniaxial test. The results indicate that the mechanical properties and parameters of shale have obvious anisotropy, and the AE characteristics of shale samples with different bedding angles are significantly different during uniaxial loading. Furthermore, the compressive strength and elastic modulus of the shale samples first decrease and then increase with the increase in the bedding angle under different confining pressures. Moreover, according to the anisotropic grade of compressive strength, the shale has moderate anisotropy. In addition, the failure mode of the shale samples is also anisotropic, and varies with the bedding angle and confining pressure. Full article

The deformation aspects associated with the micro-mechanical properties of the powder laser bed fusion (P-LBF) additively manufactured stainless steel 316L were investigated in the present work. Toward that, micro-pillars were fabricated on different planes of the stainless steel 316L specimen with respect to build direction, and an in situ compression was carried out inside the chamber of the scanning electron microscope (SEM). The results were compared against the compositionally similar stainless steel 316L, which was fabricated by a conventional method, that is, casting. The post-deformed micro-pillars on the both materials were examined by electron microscopy. The P-LBF processed steel exhibits equiaxed as well as elongated grains of different orientation with the characteristics of the melt-pool type arrangements. In contrast, the cast alloy shows typical circular-type grains in the presence of micro-twins. The yield stress and ultimate compressive stress of P-LBF fabricated steel were about 431.02 ± 15.51 − 474.44 ± 23.49 MPa and 547.78 ± 29.58 − 682.59 ± 21.59 MPa, respectively. Whereas for the cast alloy, it was about 322.38 ± 19.78 MPa and 477.11 ± 25.31 MPa, respectively. Thus, the outcome of this study signifies that the AM-processed samples possess higher mechanical properties than conventionally processed alloy of similar composition. Irrespective of the processing method, both specimens exhibit ductile-type deformation, which is typical for metallic alloys. Full article

After hydraulic fracturing, the geometric characteristics of rock morphology is a crucial means for evaluating the effectiveness of fracture stimulation in enhancing production. In order to quantitatively analyze the surface undulations of marine and continental shale morphology further following hydraulic fracturing, a method for calculating the three-dimensional fractal dimension of fracture surfaces based on optical scanning technology is proposed. This method involves the acquisition of point cloud data using a 3D surface scanner. The obtained data are subsequently subjected to smoothing processes, followed by the reconstruction of the three-dimensional representation of the fractures. The box-counting dimension algorithm is employed to calculate the fractal characteristics of post-fracture morphology. The research results indicate that marine shale, due to its higher proportion of brittle minerals such as quartz and calcite, predominantly exhibits vertically oriented longitudinal fractures, perpendicular to the minimum horizontal stress. The average initiation pressure is 8% higher compared to continental shale, with an average fractal dimension of 2.24397. In contrast, continental shale, characterized by its high clay content and the development of natural fractures and bedding planes, is more prone to capturing hydraulic fracture features, resulting in predominantly single transverse shear fractures. The average fractal dimension is 2.087065, which is 7% lower than that of marine shale. These research findings offer a certain degree of guidance for the optimization of fracturing process parameters for different types of reservoirs. Full article

The mechanical properties of shale are generally influenced by in situ geological conditions. However, the understanding of the effects of in situ geological conditions on the mechanical properties of shale is still immature. To address this problem, this paper provides insight into the elasticity and characteristic stress thresholds (i.e., the crack closure stress σ_cc, crack initiation stress σ_ci, and crack damage stress σ_cd) of shales with differently oriented bedding planes under deep in situ geological conditions. To accurately determine the elastic parameters and crack closure and initiation thresholds, a new method—i.e., the bidirectional iterative approximation (BIA) method—which iteratively approaches the upper and lower limit stresses of the linear elastic stress-strain regime, was proposed. Several triaxial compression experiments were performed on Longmaxi shale samples under coupled in situ stress and temperature conditions reflecting depths of 2000 and 4000 m in the study area. The results showed that the peak deviatoric stress (σ_p) of shale samples with the same bedding plane orientation increases as depth increases from 2000 m to 4000 m. In addition, the elastic modulus of the shale studied is more influenced by bedding plane orientation than by burial depth. However, the Poisson’s ratios of the studied shale samples are very similar, indicating that for the studied depth conditions, the Poisson’s ratio is not influenced by the geological conditions and bedding plane orientation. For the shale samples with the two typical bedding plane orientations tested (i.e., perpendicular and parallel to the axial loading direction) under 2000 and 4000 m geological conditions, the ratio of crack closure stress to peak deviatoric stress (σ_cc/σ_p) ranges from 24.83% to 25.16%, and the ratio of crack initiation stress to peak deviatoric stress (σ_ci/σ_p) ranges from 34.78% to 38.23%, indicating that the σ_cc/σ_p and σ_ci/σ_p ratios do not change much, and are less affected by the bedding plane orientation and depth conditions studied. Furthermore, as the in situ depth increases from 2000 m to 4000 m, the increase in σ_cd is significantly greater than that of σ_cc and σ_ci, indicating that σ_cd is more sensitive to changes in depth, and that the increase in depth has an obvious inhibitory effect on crack extension. The expected experimental results will provide the background for further constitutive modeling and numerical analysis of the shale gas reservoirs. Full article

Deep underground engineering encounters substantial layered hard rock formations, and the engineering triaxial stress path involves an increase in maximum principal stress, constant intermediate principal stress, and a decrease in minimum principal stress. However, previous research has focused on rock layer angles under conventional triaxial stress conditions, disregarding the influence of foliation strike angles in engineering triaxial stress scenarios. This study experimentally investigates the effects of foliation strike angles on layered hard rock under an engineering triaxial stress path. To account for the brittleness of layered hard rock, we propose a specific small sample-processing method tailored to the foliation strike angle. True triaxial loading tests are conducted on steep, thin slate samples with two different loading orientations, accompanied by acoustic emission monitoring. Results indicate that the strength under a traditional true triaxial compression condition is similar for specimens with 90° and 0° strike angles. Stress–strain curves show that larger deformations occur perpendicular to bedding planes, while surface fractures propagate exclusively along the bedding planes. Mechanical responses differ significantly between specimens subjected to the engineering triaxial stress path at 0° and 90° strike angles compared to conventional true triaxial loading tests, with a lower bearing capacity and differentiated intermediate and minimum principal strains in the 0° case. Conversely, the 90° case exhibits a higher bearing capacity, consistent deformation, and more acoustic emission events. Numerical simulations comparing plastic zone sizes during actual underground excavation support these conclusions. These findings highlight the effects of foliation strike angles, favoring the 90° strike-angle configuration for excavation activities and providing enhanced stability in the surrounding rock mass. Full article

Coal permeability data are critical in the prevention and control of coal and gas outbursts in mines and are an important reservoir parameter for the development of coalbed methane. The mechanism by which permeability is affected by gas pressure is complex. We used a self-developed true triaxial seepage experimental device that collects lignite and anthracite coal samples, sets fixed axial pressure and confining pressure, and changes gas pressure by changing the orientation of the coal seam to study the influence of the gas pressure on the permeability of the coal seam under the conditions of different coal types and different bedding orientations. Coal permeability decreased rapidly and then decreased slowly and tended to be stable with the increase in gas pressure. This conformed to the power exponential fitting relationship, and the fitting degree reached more than 99%. The comparison of the two anthracite coal samples showed that the sample’s permeability with a bedding plane vertical to the seepage direction was significantly lower than that of the bedding plane parallel to the seepage direction, indicating that gas seeped more easily along the bedding. The sensitivity coefficient of permeability with the change in gas pressure was calculated. The analysis showed that coal permeability was sensitive to changes in gas pressure during the low-pressure stage. When the gas pressure was greater than 0.8 MPa, the sensitivity coefficient was significantly reduced, which may have been related to the slow increase in the amount of gas absorbed by the coal seam in the high-pressure stage. A theoretical calculation model of coal seam permeability considering adsorption/desorption and seepage effects was proposed and then verified with experimental results showing that the theoretical model better reflected the permeability characteristics of coal and predicted its permeability. Using the finite element simulation software COMSOL, the extraction efficiency of the coal seam gas under different gas pressure conditions was simulated. The results showed that coal permeability and extraction efficiency decreased with an increase in gas pressure. In the low-pressure stage, the reduction in the extraction efficiency was more evident than that in the high-pressure stage. Full article

Rooftop buildings, mountain terrains, rivers, and lake beds may be oriented at different azimuths other than due south (in the northern hemisphere), on which photovoltaic (PV) systems may be installed. The present study presents a comprehensive point of view on the relation between the inter-row spacing and the inter-row shading in multiple-row collectors of PV fields; it analytically formulates the inter-row spacing and the associated shading losses for collectors deployed at any azimuth on horizontal, sloped-planed, and oriented toward the south and north, and is supported by the numerical results. Several criteria for the inter-row spacing are applied in the study; among them is a newly introduced criterion appropriate for the collectors deployed at a given azimuth. This study indicates that shorter spacing results in increased shading; minimum shading is obtained for collectors oriented toward the equator; inter-row spacing for maintenance purposes is used in limited dimensions of the PV fields and, usually, in optimal PV system designs; less shading occurs for systems deployed on sloped planes oriented toward the south; less shading is obtained for collectors based on the new criterion, where collectors are deployed at azimuth equal to the solar azimuth, and larger spacing is required for collectors deployed on northern slopes. Full article