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Keywords = L-DED AISI 316L stainless steel

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23 pages, 6167 KiB  
Article
Microstructural Characterization of Martensitic Stainless Steel Blades Manufactured by Directed Energy Deposition (DED)
by Caroline Cristine de Andrade Ferreira, Rafael Humberto Mota de Siqueira, Johan Grass Nuñez, Fábio Edson Mariani, Reginaldo Teixeira Coelho, Daolun Chen and Milton Sérgio Fernandes de Lima
Metals 2025, 15(6), 612; https://doi.org/10.3390/met15060612 - 29 May 2025
Viewed by 625
Abstract
This study explores the feasibility of manufacturing martensitic stainless steel turbine blades via a directed energy deposition (DED) process using a powder precursor. Five different blade geometries were fabricated using AISI 431 L martensitic stainless steel deposited onto an AISI 304 L austenitic [...] Read more.
This study explores the feasibility of manufacturing martensitic stainless steel turbine blades via a directed energy deposition (DED) process using a powder precursor. Five different blade geometries were fabricated using AISI 431 L martensitic stainless steel deposited onto an AISI 304 L austenitic stainless steel substrate. The produced components were characterized in terms of microstructure, surface roughness, porosity, hardness, and residual stresses in both the as-processed condition and after heat treatment at 260 and 593 °C. Optical and scanning electron microscopy (SEM) analyses revealed a predominantly martensitic microstructure with well-defined grain boundaries. Heat treatment influenced the phase distribution and grain size, but did not have a significant impact on the surface roughness or modulus of elasticity. Tomographic assessments confirmed the absence of aligned or coalesced pores, which are critical sites for crack initiation. Residual stress analysis indicated the presence of compressive stresses in all blade geometries, which were effectively relieved by heat treatment. In addition, salt spray corrosion tests demonstrated that the corrosion resistance of the manufactured blades was similar to that of the base material. These findings suggest that DED is a viable technique for producing and repairing turbine blades, providing structural integrity and mechanical properties suitable for high-performance applications. Full article
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16 pages, 3392 KiB  
Article
DED Powder Modification for Single-Layer Coatings on High-Strength Steels
by Unai Garate, Enara Mardaras, Jon Arruabarrena, Garikoitz Artola, Aitzol Lamikiz and Luis Norberto López de Lacalle
J. Manuf. Mater. Process. 2025, 9(5), 152; https://doi.org/10.3390/jmmp9050152 - 6 May 2025
Cited by 1 | Viewed by 586
Abstract
In the design of L-DED (laser-directed energy deposition) cladding processes, the chemical composition of the metallic powders is typically assumed to match that of the intended coating. However, during the deposition of the first layer, dilution with the substrate alters the weld metal [...] Read more.
In the design of L-DED (laser-directed energy deposition) cladding processes, the chemical composition of the metallic powders is typically assumed to match that of the intended coating. However, during the deposition of the first layer, dilution with the substrate alters the weld metal composition, deviating from the nominal powder chemistry. Although the application of multiple layers can gradually reduce this dilution effect, it introduces additional complexity and processing time. This study proposes an alternative strategy to counteract substrate dilution from the very first deposited layer, eliminating the need for multilayer coatings. Specifically, to achieve a corrosion-resistant monolayer of AISI 316L stainless steel on a high-strength, quenched-and-tempered AISI 4140 steel substrate, a dilution-compensating alloy powder is added to the standard AISI 316L feedstock. Single-layer coatings, both with and without compensation, were evaluated in terms of chemical composition, microstructure, and corrosion resistance. The results show that unmodified coatings suffered a chromium depletion of approximately 2 wt.%, leading to a reduced pitting potential of Ep = 725 ± 6 mV in synthetic seawater. In contrast, the use of the compensation alloy preserved chromium content and significantly improved corrosion resistance, achieving a pitting potential of Ep = 890 ± 9 mV. Full article
(This article belongs to the Special Issue Advances in Directed Energy Deposition Additive Manufacturing)
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13 pages, 3291 KiB  
Article
Effect of Substrate Temperature on Bead Track Geometry of 316L in Directed Energy Deposition: Investigation and Regression Modeling
by Deviprasad Chalicheemalapalli Jayasankar, Stefan Gnaase, Dennis Lehnert, Artur Walter, Robin Rohling and Thomas Tröster
Metals 2024, 14(12), 1353; https://doi.org/10.3390/met14121353 - 27 Nov 2024
Cited by 1 | Viewed by 1058
Abstract
The optimization of process parameters in powder Directed Energy Deposition (DED) is essential for achieving consistent, high-quality bead geometries, which directly influence the performance and structural integrity of fabricated components. As a subset of additive manufacturing (AM), the DED process, also referred to [...] Read more.
The optimization of process parameters in powder Directed Energy Deposition (DED) is essential for achieving consistent, high-quality bead geometries, which directly influence the performance and structural integrity of fabricated components. As a subset of additive manufacturing (AM), the DED process, also referred to as laser metal deposition (LMD), enables precise, layer-by-layer material deposition, making it highly suitable for complex geometries and part repair applications. Critical parameters, such as the laser power, feed rate, powder mass flow, and substrate temperature govern the deposition process, impacting the bead height, width, contact angle, and dilution. Inconsistent control over these variables can lead to defects, such as poor bonding, dimensional inaccuracies, and material weaknesses, ultimately compromising the final product. This paper investigates the effects of various process parameters, specifically the substrate temperature, on bead track geometry in DED processes for stainless steel (1.4404). A specialized experimental setup, integrated within a DED machine, facilitates the controlled thermal conditioning of sample sheets. Using Design of Experiments (DoE) methods, individual bead marks are generated and analyzed to assess geometric characteristics. Regression models, including both linear and quadratic approaches, are constructed to predict machine parameters for achieving the desired bead geometry at different substrate temperatures. Validation experiments confirm the accuracy and reliability of the models, particularly in predicting the bead height, bead width, and contact angle across a broad range of substrate temperatures. However, the models demonstrated limitations in accurately predicting dilution, indicating the need for further refinement. Despite some deviations in measured values, successful fabrication is achieved, demonstrating robust bonding between the bead and substrate. The developed models offer insights into optimizing DED process parameters to achieve desired bead characteristics, advancing the precision and reliability of additive manufacturing technology. Future work will focus on refining the regression models to improve predictions, particularly for dilution, and further investigate non-linear interactions between process variables. Full article
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18 pages, 6007 KiB  
Article
Direct Energy Depositions of a 17-4 PH Stainless Steel: Geometrical and Microstructural Characterizations
by Cindy Morales, Mattia Merlin, Annalisa Fortini and Alessandro Fortunato
Coatings 2023, 13(3), 636; https://doi.org/10.3390/coatings13030636 - 17 Mar 2023
Cited by 9 | Viewed by 3262
Abstract
Direct energy deposition (DED) is a widely accepted additive manufacturing process and a possible alternative to the subtractive manufacturing processes due to its high flexibility in fabricating new 3D parts. DED enables the manufacture of complex parts without using costly and time-consuming conventional [...] Read more.
Direct energy deposition (DED) is a widely accepted additive manufacturing process and a possible alternative to the subtractive manufacturing processes due to its high flexibility in fabricating new 3D parts. DED enables the manufacture of complex parts without using costly and time-consuming conventional processes, even though building parameters need to be accurately determined. In the present investigation, the effect of different process parameters on geometrical features, quality, microstructure, and microhardness of 17-4 PH stainless steel single tracks deposited onto an AISI 316L stainless steel substrate was investigated. Four sets of process parameters, considering different values of laser power, scanning speed, and powder feed rate, were selected in the manufacturing strategy, and specimens drawn from each single-track deposition were analyzed by stereomicroscopy, optical microscopy (OM), scanning electron microscopy (SEM-EDS), and X-ray diffraction (XRD). The results show that the optimized geometrical features of the track, together with the best microstructural and hardness properties, were obtained with the highest values of the laser energy input. Full article
(This article belongs to the Special Issue Surface Treatments for Stainless Steels)
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15 pages, 4943 KiB  
Article
Measuring and Predicting the Effects of Residual Stresses from Full-Field Data in Laser-Directed Energy Deposition
by Efstratios Polyzos, Hendrik Pulju, Peter Mäckel, Michael Hinderdael, Julien Ertveldt, Danny Van Hemelrijck and Lincy Pyl
Materials 2023, 16(4), 1444; https://doi.org/10.3390/ma16041444 - 8 Feb 2023
Cited by 4 | Viewed by 2752
Abstract
This article presents a novel approach for assessing the effects of residual stresses in laser-directed energy deposition (L-DED). The approach focuses on exploiting the potential of rapidly growing tools such as machine learning and polynomial chaos expansion for handling full-field data for measurements [...] Read more.
This article presents a novel approach for assessing the effects of residual stresses in laser-directed energy deposition (L-DED). The approach focuses on exploiting the potential of rapidly growing tools such as machine learning and polynomial chaos expansion for handling full-field data for measurements and predictions. In particular, the thermal expansion coefficient of thin-wall L-DED steel specimens is measured and then used to predict the displacement fields around the drilling hole in incremental hole-drilling tests. The incremental hole-drilling test is performed on cubic L-DED steel specimens and the displacement fields are visualized using a 3D micro-digital image correlation setup. A good agreement is achieved between predictions and experimental measurements. Full article
(This article belongs to the Section Advanced Materials Characterization)
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15 pages, 26634 KiB  
Article
The Influence of Intralayer Porosity and Phase Transition on Corrosion Fatigue of Additively Manufactured 316L Stainless Steel Obtained by Direct Energy Deposition Process
by Maxim Bassis, Tomer Ron, Avi Leon, Abram Kotliar, Rony Kotliar, Amnon Shirizly and Eli Aghion
Materials 2022, 15(16), 5481; https://doi.org/10.3390/ma15165481 - 9 Aug 2022
Cited by 12 | Viewed by 2539
Abstract
A direct energy deposition (DED) process using wires is considered an additive manufacturing technology that can produce large components at an affordable cost. However, the high deposition rate of the DED process is usually accompanied by poor surface quality and inherent printing defects. [...] Read more.
A direct energy deposition (DED) process using wires is considered an additive manufacturing technology that can produce large components at an affordable cost. However, the high deposition rate of the DED process is usually accompanied by poor surface quality and inherent printing defects. These imperfections can have a detrimental effect on fatigue endurance and corrosion fatigue resistance. The aim of this study was to evaluate the critical effect of phase transition and printing defects on the corrosion fatigue behavior of 316L stainless steel produced by a wire laser additive manufacturing (WLAM) process. For comparison, a standard AISI 316L stainless steel with a regular austenitic microstructure was studied as a counterpart alloy. The structural assessment of printing defects was performed using a three-dimensional non-destructive method in the form of X-ray microtomography (CT) analysis. The microstructure was evaluated by optical and scanning electron microscopy, while general electrochemical characteristics and corrosion performance were assessed by cyclic potentiodynamic polarization (CCP) analysis and immersion tests. The fatigue endurance in air and in a simulated corrosive environment was examined using a rotating fatigue setup. The obtained results clearly demonstrate the inferior corrosion fatigue endurance of the 316L alloy produced by the WLAM process compared to its AISI counterpart alloy. This was mainly related to the drawbacks of WLAM alloys in terms of having a duplex microstructure (austenitic matrix and secondary delta-ferrite phase), reduced passivity, and a significantly increased amount of intralayer porosity that acts as a stress intensifier of fatigue cracking. Full article
(This article belongs to the Special Issue 3D Printing: Materials, Properties, and Applications)
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27 pages, 21103 KiB  
Article
Prediction of Behaviour of Thin-Walled DED-Processed Structure: Experimental-Numerical Approach
by Miroslav Urbánek, Josef Hodek, Daniel Melzer, Martina Koukolíková, Antonín Prantl, Jaroslav Vavřík, Michal Brázda, Petr Martínek, Sylwia Rzepa and Jan Džugan
Materials 2022, 15(3), 806; https://doi.org/10.3390/ma15030806 - 21 Jan 2022
Cited by 11 | Viewed by 2227
Abstract
Additive manufacturing (AM) becomes a more and more standard process in different fields of industry. There is still only limited knowledge of the relationship between measured material data and the overall behaviour of directed energy deposition (DED)-processed complex structures. The understanding of the [...] Read more.
Additive manufacturing (AM) becomes a more and more standard process in different fields of industry. There is still only limited knowledge of the relationship between measured material data and the overall behaviour of directed energy deposition (DED)-processed complex structures. The understanding of the structural performance, including flow curves and local damage properties of additively manufactured parts by DED, becomes increasingly important. DED can be used for creating functional surfaces, component repairing using multiple powder feeders, and creating a heterogeneous structure with defined chemical composition. For thin parts that are used with the as-deposited surface, this evaluation is even highly crucial. The main goal of the study was to predict the behaviour of thin-walled structures manufactured by the DED process under static loading by finite element analysis (FEA). Moreover, in this study, the mechanical performance of partly machined and fully machined miniaturized samples produced from the structure was compared. The structure studied in this research resembles a honeycomb shape made of austenitic stainless steel AISI 316L, which is characterized by high strength and ductility. The uncoupled damage models based on a hybrid experimental-numerical approach were used. The microstructure and hardness were examined to comprehend the structural behaviour. Full article
(This article belongs to the Special Issue Numerical and Experimental Investigations in Metal Forming)
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12 pages, 3661 KiB  
Article
Directed Energy Deposition of AISI 316L Stainless Steel Powder: Effect of Process Parameters
by Alberta Aversa, Giulio Marchese and Emilio Bassini
Metals 2021, 11(6), 932; https://doi.org/10.3390/met11060932 - 8 Jun 2021
Cited by 40 | Viewed by 7028
Abstract
During Laser Powder-Directed Energy Deposition (LP-DED), many complex phenomena occur. These phenomena, which are strictly related to the conditions used during the building process, can affect the quality of the parts in terms of microstructural features and mechanical behavior. This paper investigates the [...] Read more.
During Laser Powder-Directed Energy Deposition (LP-DED), many complex phenomena occur. These phenomena, which are strictly related to the conditions used during the building process, can affect the quality of the parts in terms of microstructural features and mechanical behavior. This paper investigates the effect of building parameters on the microstructure and the tensile properties of AISI 316L stainless-steel samples produced via LP-DED. Firstly, the building parameters were selected starting from single scan tracks by studying their morphology and geometrical features. Next, 316L LP-DED bulk samples built with two sets of parameters were characterized in terms of porosity, geometrical accuracy, microstructure, and mechanical properties. The tensile tests data were analyzed using the Voce model and a correlation between the tensile properties and the dislocation free path was found. Overall, the data indicate that porosity should not be considered the unique indicator of the quality of an LP-DED part and that a mechanical characterization should also be performed. Full article
(This article belongs to the Special Issue Directed Energy Deposition of Metal Alloys)
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23 pages, 15513 KiB  
Review
Microstructure and Mechanical Properties of AISI 316L Produced by Directed Energy Deposition-Based Additive Manufacturing: A Review
by Abdollah Saboori, Alberta Aversa, Giulio Marchese, Sara Biamino, Mariangela Lombardi and Paolo Fino
Appl. Sci. 2020, 10(9), 3310; https://doi.org/10.3390/app10093310 - 9 May 2020
Cited by 160 | Viewed by 15494
Abstract
Directed energy deposition (DED) as a metal additive manufacturing technology can be used to produce or repair complex shape parts in a layer-wise process using powder or wire. Thanks to its advantages in the fabrication of net-shape and functionally graded components, DED could [...] Read more.
Directed energy deposition (DED) as a metal additive manufacturing technology can be used to produce or repair complex shape parts in a layer-wise process using powder or wire. Thanks to its advantages in the fabrication of net-shape and functionally graded components, DED could attract significant interest in the production of high-value parts for different engineering applications. Nevertheless, the industrialization of this technology remains challenging, mainly because of the lack of knowledge regarding the microstructure and mechanical characteristics of as-built parts, as well as the trustworthiness/durability of engineering parts produced by the DED process. Hence, this paper reviews the published data about the microstructure and mechanical performance of DED AISI 316L stainless steel. The data show that building conditions play key roles in the determination of the microstructure and mechanical characteristics of the final components produced via DED. Moreover, this review article sheds light on the major advancements and challenges in the production of AISI 316L parts by the DED process. In addition, it is found that in spite of different investigations carried out on the optimization of process parameters, further research efforts into the production of AISI 316L components via DED technology is required. Full article
(This article belongs to the Special Issue Materials Development by Additive Manufacturing Techniques)
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