Comparing Polyphosphate and Orthophosphate Treatments of Solution-Precipitated Aragonite Powders
Abstract
:1. Introduction
2. Materials and Methods
2.1. Precipitation
2.2. Annealing
2.3. Aqueous Treatments
2.4. Characterization
3. Results
3.1. Before Aqueous Treatments
3.2. After Aqueous Treatments
3.3. Time Trends pH during Aqueous Treatments
3.4. Thermal Stability after Aqueous Treatments
4. Discussion
5. Conclusions
Supplementary Materials
Author Contributions
Funding
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Sample/Mass (%) | Low T Loss | High T Loss | Assumed CaO | Excess Mass |
---|---|---|---|---|
(20–575 C) | (575–750 C) | Mass Remaining | Remaining | |
ideal | 0.0% | 43.0% | 57.0% | 0.0% |
as-precipitated | 1.1% | 40.9% | 54.2% | 3.8% |
pH 10.5 | 1.6% | 39.4% | 52.2% | 6.8% |
pH 9.5 | 2.9% | 37.0% | 49.0% | 11.1 % |
pH 8 | 3.0% | 36.7% | 48.6% | 11.7 % |
pH 7 | 3.3% | 34.2% | 45.3% | 17.2 % |
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Gao, B.; Poduska, K.M. Comparing Polyphosphate and Orthophosphate Treatments of Solution-Precipitated Aragonite Powders. Solids 2022, 3, 684-696. https://doi.org/10.3390/solids3040042
Gao B, Poduska KM. Comparing Polyphosphate and Orthophosphate Treatments of Solution-Precipitated Aragonite Powders. Solids. 2022; 3(4):684-696. https://doi.org/10.3390/solids3040042
Chicago/Turabian StyleGao, Boyang, and Kristin M. Poduska. 2022. "Comparing Polyphosphate and Orthophosphate Treatments of Solution-Precipitated Aragonite Powders" Solids 3, no. 4: 684-696. https://doi.org/10.3390/solids3040042