The Various Silane Agents in Universal Adhesives on Repair Strength of Resin Composite to Resin Composite
Abstract
:1. Introduction
2. Materials and Methods
2.1. Aged Resin Composite Preparation
2.2. Surface Treatment Procedures
2.2.1. Phosphoric Acid Treatment
2.2.2. Silane Agent Treatment
2.2.3. Adhesive Agent Treatment
2.3. Bond Specimen Procedures
2.4. Shear Bond Strength (SBS) and Failure Mode Inspection
2.5. Statistical Analysis
3. Results
3.1. SBS Values
3.2. Analysis of Failure Pattern and SEM Surface Fractured
4. Discussion
5. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Materials | Main Compositions |
---|---|
RelyX ceramic primer (3M ESPE, Minnesota, USA) Lot: N988623 | Ethanol, water, methacryloxypropyltrimethoxysilane |
Single bond 2 (3M ESPE, Minnesota, USA) Lot: NE92635 | Bis-GMA, HEMA, DMA, methacrylate functional copolymer, filler, photoinitiators, ethanol, water |
Singlebond universal (3M, Neuss, Germany) Lot: 483316 | 10-MDP, Bis-GMA, HEMA, DMA, methacrylate functional copolymer, silane, filler, initiators, ethanol, water |
Scotchbond universal plus (3M, Neuss, Germany) Lot: 8321974 | HEMA, 2-propenoic acid, 2-methyl-, diesters with 4,6-dibromo-1,3-benzenediol 2-(2-hydroxyethoxy)ethyl 3-hydroxypropyl diethers, 2-propenoic acid, 2-methyl-, reaction products with 1,10-decanediol and phosphorus oxide, 2-propenoic acid, 2-methyl-, 3(triethoxysilyl)propyl ester, reaction products with silica and 3(triethoxysilyl)-1-propanamine, synthetic amorphous silica, fumed, crystalline-free, ethanol, water, (3-aminopropyl)triethoxysilane, camphorquinone, N,N-dimethylbenzocaine, methacrylic acid, Acetic acid, copper(2+) salt, monohydrate |
Clearfil Tri-S bond universal (Kuraray Noritake Dental Inc., Okayama, Japan) Lot: 4K0025 | 10-MDP, Bis-GMA, HEMA, colloidal silica, ethanol, silane, sodium fluoride, camphoquinone, ethanol, water |
Resin composite (Filtex Z350 XT (A3B, A4B), 3M ESPE, Minnesota, USA) Lot: NA77397, NF40326 | Silane treated ceramic, silane treated silica, silane treated zirconia, Bis-EMA-6, Bis-GMA, UDMA, PEGDMA and TEGDMA |
Group | Mean SBS ± SD | Failure Pattern | ||
---|---|---|---|---|
Adhesive | Mixed | Cohesive | ||
1. No surface treatment | 7.69 ± 2.57 a | 100 | 0 | 0 |
2. SU | 14.63 ± 2.05 b | 100 | 0 | 0 |
3. SUP | 22.69 ± 2.21 c | 80 | 20 | 0 |
4. CFU | 15.01 ± 3.07 b | 100 | 0 | 0 |
5. SB2 | 14.59 ± 2.17 b | 100 | 0 | 0 |
6. Si + SU | 22.08 ± 1.83 c | 80 | 20 | 0 |
7. Si + SUP | 28.04 ± 1.62 d | 70 | 30 | 0 |
8. Si + CFU | 21.98 ± 1.54 c | 80 | 20 | 0 |
9. Si + SB2 | 21.85 ± 2.18 c | 80 | 20 | 0 |
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Leelaponglit, S.; Maneenacarith, A.; Wutikhun, T.; Klaisiri, A. The Various Silane Agents in Universal Adhesives on Repair Strength of Resin Composite to Resin Composite. J. Compos. Sci. 2023, 7, 7. https://doi.org/10.3390/jcs7010007
Leelaponglit S, Maneenacarith A, Wutikhun T, Klaisiri A. The Various Silane Agents in Universal Adhesives on Repair Strength of Resin Composite to Resin Composite. Journal of Composites Science. 2023; 7(1):7. https://doi.org/10.3390/jcs7010007
Chicago/Turabian StyleLeelaponglit, Seelassaya, Apichai Maneenacarith, Tuksadon Wutikhun, and Awiruth Klaisiri. 2023. "The Various Silane Agents in Universal Adhesives on Repair Strength of Resin Composite to Resin Composite" Journal of Composites Science 7, no. 1: 7. https://doi.org/10.3390/jcs7010007