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Article

Experimental Study on Particle Settling in Fiber-Containing Non-Newtonian Fluids

1
Sinopec Key Laboratory of Drilling Completion and Fracturing of Shale Oil and Gas, Beijing 102206, China
2
State Key Laboratory of Shale Oil and Gas Enrichment Mechanisms and Efficient Development, Beijing 102206, China
3
SINOPEC Research Institute of Petroleum Engineering Co., Ltd., Beijing 102206, China
4
Sanya Offshore Oil & Gas Research Institute of Northeast Petroleum University, Sanya 572024, China
5
School of Physics, Sun Yat-sen University, Guangzhou 510275, China
*
Author to whom correspondence should be addressed.
Processes 2025, 13(8), 2542; https://doi.org/10.3390/pr13082542
Submission received: 9 July 2025 / Revised: 5 August 2025 / Accepted: 8 August 2025 / Published: 12 August 2025
(This article belongs to the Special Issue Numerical and Process Modelling in Computational Fluid Dynamics)

Abstract

To investigate the settling behavior and drag characteristics of particles in fiber-containing non-Newtonian fluids, a series of systematic single-particle settling experiments were conducted. Power-law and Herschel–Bulkley fluids were prepared as base media, into which polyester fibers of various concentrations and lengths were introduced. The effects of fiber structural parameters on fluid rheology and terminal settling velocity were thoroughly evaluated. First, the rheological changes induced by fiber addition were quantitatively analyzed, revealing a nonlinear increase in both viscosity and yield stress with increasing fiber concentration and length. Subsequently, the total drag force was decomposed into viscous and fiber-induced components, and a predictive model for the fiber-induced drag coefficient was developed based on fiber structural parameters. A power-law fitting approach was employed to characterize the nonlinear relationship between the fiber drag coefficient and the particle Reynolds number. Furthermore, a parametric coupling strategy was employed, in which fiber concentration and length were embedded into the model coefficients to construct a unified and continuous predictive model for the total drag coefficient. Experimental validation demonstrated that the mean relative errors (MREs) of the proposed model were within 5.17% for power-law fluids and 9.95% for Herschel–Bulkley fluids, indicating strong predictive accuracy and applicability. The findings of this study provide a robust theoretical and experimental basis for optimizing fiber-enhanced cutting transport systems and modeling particle transportation under complex drilling conditions.

1. Introduction

In drilling operations, the ability of drilling fluids to transport cuttings significantly influences hole-cleaning efficiency, rate of penetration (ROP), and downhole operational safety—particularly in horizontal and extended-reach wells [1,2,3,4]. In recent years, fiber-reinforced drilling fluids have gained increasing attention for their enhanced suspension stability, modified rheological structure, and improved cutting transport efficiency in complex formations and large-particle environments [5,6].
Compared to conventional drilling fluids, fiber-containing fluids exhibit more intricate rheological behaviors, including nonlinear shear responses, viscoelasticity, and intensified particle–fluid–fiber interactions. The introduction of fibers not only alters macroscopic flow properties but also generates microscale network structures that substantially influence particle settling dynamics. However, the settling behavior of particles in fiber-laden non-Newtonian fluids remains inadequately characterized, with limited experimental data and the absence of a unified predictive framework.
For Newtonian fluids, both theoretical and empirical models describing particle settling and drag coefficients are well established and widely applied [7,8,9,10]. However, drilling fluids often exhibit non-Newtonian characteristics, with viscosity depending strongly on shear rate, making Newtonian-based models insufficient under such conditions [11,12].
To address this, various drag prediction models have been proposed for non-Newtonian fluids. Khan and Richardson [13] incorporated shear-thinning effects, particle size, and interaction forces in their formulation. Wilson et al. [14] introduced a generalized Reynolds number to account for apparent viscosity. Kelessidis and Mpandelis [15] revised the Haider and Levenspiel model [16] to better represent non-Newtonian flow regimes.
Further developments include Shah’s formulation linking drag to flow index and Reynolds number [17], Song’s experimental model of wall factor effects in power-law fluids [18], Okesanya’s quantification of rheological influence on settling velocity using a modified Reynolds numbers [19], and Yan’s drag correlations for spherical and irregular sand particles in both power-law and Herschel–Bulkley fluids [20].
Nonetheless, the presence of fibers introduces significantly more complexity into the multiphase flow dynamics of drilling fluids. Unlike conventional particulate additives, fibers not only alter the bulk rheological properties—often inducing viscoelastic or thixotropic properties—but also impose microscale structural constraints on particle mobility. These effects stem from fiber–particle entanglement, hydrodynamic shielding, and spatial confinement, which together disrupt flow uniformity and introduce anisotropic drag forces not accounted for by classical drag models.
In particular, fibers form interconnected networks that evolve with shear history, resulting in time-dependent resistance effects and potential yield stress amplification. These networks can act as dynamic scaffolds, modifying the effective viscosity non-uniformly across the flow field. This results in heterogeneous shear distributions, altered boundary layer behavior, and secondary flow phenomena, especially under inclined or eccentric annular flow conditions. Furthermore, the orientation and deformability of fibers add further degrees of freedom that influence both macroscopic transport and localized stress fields.
Despite these complexities, existing research on fiber-containing drilling fluids remains fragmented and narrowly focused. Natural fibers—such as lignin, coconut husk, and jute—have primarily been investigated for their environmental compatibility, biodegradability, and cost-effectiveness. However, their inconsistent morphology, batch-to-batch variability, and limited rheological tunability hinder broader applicability in engineered systems. Conversely, synthetic fibers—such as polypropylene, polyester, and nylon—offer greater consistency and design flexibility in terms of aspect ratio, surface chemistry, and thermal resistance, yet research on synthetic fibers has mostly concentrated on formulation and rheological tuning, with relatively few studies devoted to systematically evaluating their effects on particulate transport, drag evolution, or flow stability.
Current studies on particle settling in fiber-laden systems remain dispersed, relying on a mix of numerical simulations and experimental analysis. Harlen et al. [21] showed that neglecting fiber contact forces underestimated drag in low-density fiber suspensions. Feist et al. [22] demonstrated that settling velocity depends on fiber-to-particle size ratio and solution pH. Elgaddafi et al. [23] proposed a semiempirical correlation linking fiber-induced drag to projected area and density differences. Liu et al. [5] confirmed that fiber entanglement forms network structures that impede particle mobility.
In summary, particle settling in fiber-containing non-Newtonian fluids is governed by the interacting effects of fiber concentration, length, orientation, and the base fluid’s viscoelasticity. While various drag models for fiber suspensions have been proposed, none has successfully unified non-Newtonian rheological behavior and fiber structural effects into a comprehensive predictive framework.
This study aimed to systematically examine the settling behavior of spherical particles in power-law and Herschel–Bulkley fluids with varying fiber parameters. The novelty of this study lies in the inclusion of fiber-induced drag, which is absent in existing models based on fiber-free fluids. A composite drag coefficient model incorporating both fiber concentration and length is developed to elucidate the dominant force mechanisms acting on particles. The proposed model seeks to improve generality, parameterization, and engineering applicability, providing a rigorous theoretical basis and experimental support for the optimized design of fiber-containing drilling fluids.

2. Materials and Methods

2.1. Experimental Principles

The settling behavior of particles in fluid results from the combined action of three forces: gravitational force, buoyancy, and hydrodynamic drag. When a particle is released into a fluid, it is driven downward by gravity, while buoyancy opposes this motion as an upward force resulting from fluid displacement [24]. Simultaneously, the relative motion between the particle and the surrounding fluid generates viscous drag. As the particle accelerates, the drag force increases until force equilibrium is reached, at which point the particle settles at a constant velocity, known as the terminal settling velocity (Vt).
The settling velocity is governed by several factors, including the density difference between the particle and the fluid, particle diameter, fluid viscosity, and the flow regime. A larger density difference or particle size leads to a higher net driving force and a greater settling velocity, whereas increased fluid viscosity enhances drag and thus reduces terminal velocity. In laminar flow, particle trajectories are typically axisymmetric and stable. In contrast, turbulent or non-uniform flows may induce lateral drift, rolling, or even resuspension.
Under steady-state force equilibrium, the net force acting on a settling particle is zero, i.e., the total drag force Fdt equals the buoyant weight Fw, which is the difference between the gravitational force FG and the buoyant force FB, and can be expressed as:
F dt = F W = F G F B
The drag force Fdt is defined as:
F dt = π 8 ρ L C D d e 2 V rel 2
The buoyant weight Fw is given by:
F w = π 6 ρ P ρ L g d e 3
where ρP is the particle density, ρL is the fluid density, Vrel is the relative velocity between the particle and fluid, de is the equivalent particle diameter, and CD is the drag coefficient, a dimensionless quantity characterizing the resistance to motion in the fluid.
By combining Equations (1)–(3), the drag coefficient CD can be derived as:
C D = 4 3 ρ P ρ L ρ L g d e V t 2
The particle Reynolds number Res is a key parameter used to characterize flow regimes and viscous effects. Its formulation varies depending on the rheological model of the fluid.
For power-law fluids:
R e s - pl = ρ L V t 2 n d e n K
For Herschel–Bulkley fluids:
R e s - H B = ρ L V t 2 n d e n K + τ 0 ( d e V ) n
where K is the consistency coefficient, n is the flow behavior index, and τ0 is the yield stress of the fluid.

2.2. Settling Test Apparatus

The experimental setup is illustrated in Figure 1. Settling tests were conducted in a transparent acrylic cylinder with a height of 500 mm and an internal diameter of 80 mm. The cylinder was immersed in a thermostatic water bath (200 mm × 200 mm × 500 mm) to maintain a constant temperature, thus minimizing the influence of thermal fluctuations on fluid properties.
A high-speed camera (Revealer 2F04C, Hefei, China; frame rate: 100 fps, resolution: 1920 × 1080 pixels) was used to capture the motion of particles during settling. Video data were processed using image-processing software to extract displacement trajectories and calculate settling velocities with high precision. To improve visibility in opaque fluids, an auxiliary lighting system and colored tracer coatings on particles were employed when necessary.
A calibrated 20 cm ruler was attached externally to the observation cylinder to provide a visual scale for trajectory calibration. Temperature was continuously monitored using a digital thermometer. The entire apparatus was well sealed, stable, and adaptable to different particle–fluid combinations.
The observation zone was set between 50 mm and 150 mm above the bottom to ensure that particles had passed through the acceleration phase and reached terminal settling, while minimizing wall and bottom boundary effects. This region was divided into equidistant segments to validate velocity uniformity. If the variation in velocity between adjacent segments was less than 5%, the particle was considered to have reached terminal settling. The experimental devices and measurement accuracy can be seen in Table 1.

2.3. Materials and Test Fluids

Five types of spherical particles with different densities were used: iron, zirconia, silicon nitride, aluminum, and polyoxymethylene (POM). Although actual drill cuttings are typically irregular in shape, spherical particles were selected to ensure experimental repeatability and to allow systematic investigation across a wide Reynolds number range. This approach facilitated the development of predictive drag models for hole-cleaning applications. The physical properties of the particles are listed in Table 2.
The base fluid was a Carbopol U20 aqueous solution, a cross-linked polyacrylic acid polymer known for its high clarity, strong suspension capability, and stable rheology. Unneutralized Carbopol solutions behave as power-law fluids, which can be described by:
τ = K γ n
where τ is the shear stress and γ is the shear rate.
Upon neutralization with triethanolamine, the fluid transforms into a Herschel–Bulkley fluid with a yield stress term:
τ = τ 0 + K γ n
Rheological parameters under various concentrations and neutralization conditions were measured using a rotational rheometer (Anton Paar MCR 92, Graz, Austria). The fitted rheological parameters are provided in Table 3.

3. Experimental Analysis of Sphere Settling Behavior in Non-Newtonian Fluids

To systematically investigate the settling characteristics of particles in different non-Newtonian fluids, a total of 107 valid datasets were obtained for spherical particle settling in power-law fluids and 81 datasets in Herschel–Bulkley fluids. These datasets span a wide range of particle diameters, densities, and fluid shear parameters, ensuring sufficient representativeness and diversity for comprehensive analysis.
To evaluate the applicability of existing drag coefficient models under such conditions, five representative empirical or semiempirical models were selected from the literature, including those developed by Khan and Richardson [13], Kelessidis et al. [15], Yan et al. [20], and Okesanya et al. [19]. These models, originally derived for power-law or Herschel–Bulkley systems, are summarized in Table 4.
To quantitatively assess the prediction accuracy of these models, two error metrics were employed: Root Mean Square Error (RMSE) and Mean Relative Error (MRE). RMSE reflects the average deviation between predicted and experimental drag coefficients, while MRE provides a normalized measure of overall relative error across the dataset. The definitions are given by:
R M S E = i = 1 N C tsp C tsm 2 N z
M R E = i = 1 N C tsp C tsm C tsm N z × 100 %
where Nz is the number of data points, Ctsm is the experimentally measured drag coefficient, and Ctsp is the predicted value from the model.
The RMSE and MRE values are summarized in Table 5.
As shown in Table 4, the Kelessidis model exhibits the best overall performance for power-law fluids in terms of MRE, with an MRE of 10.71%, indicating robust predictive stability across the dataset. While the Yan model yields the lowest RMSE (1.22), suggesting high local accuracy, its higher MRE (14.41%) implies greater error dispersion across different flow regimes. The Khan model demonstrates moderate performance on both metrics. Taking into account both predictive accuracy and applicability across varied conditions, the Kelessidis model is deemed the most reliable for power-law fluids in engineering contexts.
In terms of terminal settling velocity prediction, further analysis reveals that both the Khan and Yan models yield results that align well with experimental observations. Considering both drag coefficient and terminal velocity predictions, the Kelessidis model consistently demonstrates superior stability and is recommended as a reference model for subsequent development and field application.
For Herschel–Bulkley fluids, as shown in Table 4, the Yan model achieves the lowest RMSE, indicating improved local fitting. However, its MRE remains high at 22.33%, indicating limited global reliability. The Okesanya model, though theoretically incorporating yield stress and shear consistency effects, performs poorly under the present experimental conditions, with both RMSE and MRE reaching 30.77 and 26.90%, respectively, reflecting its narrow applicability range. In contrast, the Khan model, despite a slightly higher RMSE (29.18), produces the lowest MRE (16.31%) among the three, indicating more consistent performance across diverse conditions.
In summary, based on experimental data, the Kelessidis model is recommended for power-law fluids due to its balanced accuracy and engineering applicability, while the Khan model is identified as the most reliable for Herschel–Bulkley fluids, owing to its superior mean relative accuracy across varied rheological scenarios.

4. Rheological Characterization of Fiber-Containing Non-Newtonian Fluids

To elucidate the reinforcement mechanism by which fibers influence the rheological properties of non-Newtonian fluids, this study systematically investigated the effects of polyester fibers with varying concentrations and lengths on two representative base fluid systems: power-law fluids and Herschel–Bulkley fluids. These base fluids were prepared using Carbopol U20 aqueous solutions: unneutralized solutions represented power-law fluids, while neutralized solutions (via triethanolamine) represented Herschel–Bulkley fluids. As seen in Figure 2, polyester fibers with a density of 1330 kg/m3 were selected due to their chemical stability and engineering applicability, making them common additives for borehole stabilization and cutting transport enhancement.
A full-factorial experimental design was employed, covering four fluid concentrations (0.06%, 0.1%, 1%, and 2%), five fiber concentrations (0.03% to 0.15%), and three fiber lengths (6 mm, 9 mm, and 12 mm), resulting in 60 rheological datasets. Rheological measurements and model fitting were performed using an Anton Paar MCR 92 rheometer under controlled temperature conditions. Table 6 summarizes the key nondimensional parameters used in this study, including particle Reynolds number ranges, fiber length, and fiber concentrations.

4.1. Effect of Fiber Concentration on Drilling Fluid Rheology

Figure 3 and Figure 4 illustrate the viscosity trends of power-law and Herschel–Bulkley fluids, respectively, with increasing fiber concentration. The results indicate a nonlinear increase in viscosity, attributed to the interplay between the viscoelasticity of the base fluid and the strength of fiber–fluid interactions.
In low-viscosity base fluids (e.g., 1% power-law or 0.06% Herschel–Bulkley), fiber concentrations below 0.09% had minimal impact on viscosity, suggesting that the fiber network was relatively loose. However, beyond 0.09%, viscosity increased sharply, indicating a critical threshold for fiber entanglement. For example, in a 1% power-law fluid with 9 mm fibers, increasing the fiber concentration from 0 to 0.09% led to a 7.8% rise in viscosity, while increasing it to 0.15% resulted in a 14.5% increase, highlighting the “structural thickening” and percolation effects of the fiber network.
In contrast, in high-viscosity base fluids (e.g., 2% power-law or 0.1% Herschel–Bulkley), the impact of fiber concentration on viscosity was less pronounced. For instance, a 2% power-law fluid with 12 mm fibers exhibited only a 9.1% increase in viscosity across the same fiber concentration range, implying that existing intermolecular interactions in high-viscosity systems limit the additional thickening effects from fiber addition.
Regarding yield stress, Figure 5 shows the relationship between fiber concentration and dynamic yield stress in Herschel–Bulkley fluids. A general increase was observed, but with diminishing marginal gains, especially at higher base fluid viscosities. For instance, in a 0.06% Herschel–Bulkley fluid with 9 mm fibers, increasing fiber concentration from 0.03% to 0.15% raised yield stress by 11.2%, whereas the same increase in a 0.1% base fluid only produced a 3.7% increase.
From a microscopic standpoint, fibers form bridging and entangled structures via van der Waals or electrostatic forces, enhancing internal friction. In low-viscosity systems, the initial low yield stress amplifies fiber effects, while in high-viscosity systems, preexisting network rigidity reduces fiber-induced enhancements.

4.2. Effect of Fiber Length on Drilling Fluid Rheology

Figure 6 and Figure 7 depict the influence of fiber length (6 mm, 9 mm, and 12 mm) on solution viscosity in various base fluids. The influence of fiber length is strongly coupled with fiber concentration.
At low fiber concentrations (e.g., 0.03%), fiber length had a negligible effect on viscosity. For example, in a 1% power-law fluid, increasing fiber length from 6 mm to 12 mm led to only a 1.8% increase in viscosity. However, at higher fiber concentrations (e.g., 0.12%), the effect became more significant, resulting in a 7.6% increase, indicating that effective fiber–fiber networking requires sufficient density.
The correlation between fiber length and viscosity was stronger in high-viscosity fluids, where fiber mobility is restricted, allowing longer fibers to form interconnected and stable microstructures, enhancing bulk resistance.
Yield stress followed a similar trend. As shown in Figure 8, in a 0.06% Herschel–Bulkley fluid with 0.06% fiber concentration, increasing fiber length from 6 mm to 12 mm resulted in a 4.8% increase in yield stress. This effect is due to the greater curvature radius and structural flexibility of long fibers, which promote multi-scale entanglement and generate more uniform three-dimensional networks, unlike shorter fibers, which tend to cluster locally and weaken network integrity.
In summary, fiber concentration controls spatial density, while fiber length determines network connectivity and strength. The base fluid viscosity further modulates these interactions: low-viscosity fluids enable dynamic structure formation, while high-viscosity fluids suppress network development. This section provides critical insights into the nonlinear structure–property relationships of fiber-containing non-Newtonian fluids, forming the foundation for the drag force and particle settling analyses in the subsequent sections.

5. Experimental Investigation of Particle Settling in Fiber-Containing Non-Newtonian Fluids

Building upon the analysis and model validation of fiber-free systems in Section 3, a series of systematic experiments was conducted to examine particle settling behavior in fiber-containing non-Newtonian fluids. The objective was to elucidate the mechanistic role of fibers in regulating particle settling dynamics and to develop a predictive drag coefficient model that incorporates fiber structural effects, thereby enhancing the engineering predictability of settling behavior in practical drilling scenarios.

5.1. Experimental Procedure and Measurement Method

Carbomer U20 aqueous solutions were used to formulate power-law base fluids, which were subsequently neutralized with triethanolamine to produce Herschel–Bulkley fluids. Four fluid concentrations (0.06%, 0.1%, 1%, and 2%) were selected. Polyester fibers with three different lengths (6 mm, 9 mm, and 12 mm) were introduced into these solutions to construct a fiber–fluid matrix.
The preparation procedure was as follows. After thorough mixing and standing to ensure homogeneity, the fluid was carefully poured into the settling column to eliminate trapped air. Rheological parameters were measured under isothermal conditions, and single-particle settling experiments were conducted to determine the terminal settling velocity, as shown in Figure 9. Each test condition was repeated five times, and averaged results were used. Trajectories disturbed by aggregation or off-center descent were excluded. To ensure stability and repeatability, the fluid was stirred between trials to prevent fiber agglomeration.
A total of 201 valid datasets were collected for fiber-containing power-law fluids and 158 datasets for fiber-containing Herschel–Bulkley fluids. These were used to construct drag coefficient prediction models by fitting the relationship between fiber drag and particle Reynolds number, with fiber concentration and fiber length introduced as key parameters in a unified prediction framework.

5.2. Drag Force Decomposition in Fiber-Containing Fluids

In fiber-laden systems, the total drag force Fdt can be decomposed into two components: viscous drag Fdv and fiber-induced drag Fdf, such that:
F dt = F dv + F df
The viscous component was computed using existing empirical models. Although the Kelessidis model performs well in fiber-free power-law fluids and the Khan model in Herschel–Bulkley fluids, subsequent analysis revealed that applying the Kelessidis model in fiber-containing power-law fluids introduced significant deviations. Therefore, for consistency and reliability, the Khan model was adopted uniformly to estimate the viscous drag in both fluid systems.
C dv - Khan = ( 2.25 R e s 0.31 + 0.36 R e s 0.06 ) 3.45

5.3. Relationship Between Fiber Drag Coefficient and Particle Reynolds Number

Inspired by Elgaddafi et al., the fiber-induced drag Fdf is expressed analogously to classical fluid drag, as a function of the fiber drag coefficient Cdf, terminal velocity Vt, projected particle area, and density difference:
F df - E = 1 2 A P ( ρ P ρ L ) C df - E V t 2 = π 8 D e 2 ( ρ P ρ L ) C df - E V t 2
Rearranging yields:
C df - E = 4 D e g 3 V t 2 C dv ρ L ρ P ρ L
Building upon this, Xu et al. introduced fiber structural parameters and proposed:
C df - xu = 4 ( ρ P ρ L ) D e g 3 ρ L V t 2 C dv
Figure 10 illustrates the empirical relationship between the dimensionless drag coefficient Cdf and particle Reynolds number Res for both fluid types. An initial attempt using linear regression showed an apparent trend, but poor fitting performance, with R2 values consistently below 0.8. This suggests that the linear formulation oversimplifies the complex hydrodynamic interactions present in fiber-laden non-Newtonian systems and fails to account for the inherent nonlinearity in the drag–inertia coupling.
Upon reanalysis using a power-law fitting approach, the correlation quality improved substantially, with R2 values exceeding 0.9 across the majority of tested conditions. This significant enhancement confirms that fiber-induced drag in shear-dependent fluids is governed by a nonlinear functional form rather than a proportional relationship. In physical terms, this implies that as inertial effects begin to emerge—especially at moderate-to-high Reynolds numbers—the contribution of fiber-induced resistance grows disproportionately due to microstructural disturbances and complex wake formation around the fiber–particle matrix.
C df = A × R e s B
Furthermore, the improved performance of the power-law model highlights its flexibility in adapting to different flow regimes. At low Res, where viscous forces dominate, fiber networks act primarily as rheological modifiers. However, as the flow transitions toward inertial regimes, the combined effects of yield stress, shear-thinning, and fiber entanglement introduce secondary flow structures that are more accurately described by nonlinear drag scaling. The power-law formulation inherently accommodates this regime-dependent behavior, making it a more physically consistent and scalable tool for practical use.
Fitted parameters A and B under different fiber conditions are listed in Table 7 and Table 8.
To generalize the model and eliminate segmented empirical fitting, a parametric coupling strategy was proposed. The parameters A and B were expressed as continuous functions of fiber concentration Cf and length Lf:
A = a 1 + b 1 x 1 + c 1 x 1 2 + d 1 x 2 + e 1 x 2 2 + f 1 x 1 x 2
B = a 2 + b 2 x 1 + c 2 x 1 2 + d 2 x 2 + e 2 x 2 2 + f 2 x 1 x 2
This coupling enables the integration of fiber structural parameters into a unified, continuous predictive model. It retains the physical interpretability of Cf and Lf while avoiding segmentation-induced errors common in traditional multi-model strategies.
The fitted surface equations for A and B in power-law fluids are shown in Equations (19) and (20), with the corresponding surface plots presented in Figure 11.
A pl = 3.564 0.665 L f + 0.032 L f 2 99.3 C f + 1347 C f 2 + 11.62 L f C f
B pl = 0.754 + 0.041 L f 0.002 L f 2 + 2.268 C f 17.1 C f 2 0.175 L f C f
Similarly, for Herschel–Bulkley fluids, the surface fitting results are expressed through Equations (21) and (22), with Figure 12 illustrating the three-dimensional fitted surfaces corresponding to total drag coefficient and terminal velocity as functions of fiber length and concentration. The regression models achieved high R2 values (0.86–0.99), indicating excellent model robustness. The model captures the transition from dilute to semi-dense regimes and the influence of fiber-induced structure formation, particularly in yield-stress fluids, where threshold stress and microstructural confinement dominate.
The high R2 values suggest that the effects of both fiber length and concentration on hydrodynamic resistance and settling kinetics are well represented within the fitted model surfaces. Specifically, the model successfully encapsulates the transition from dilute fiber regimes—where individual fibers contribute modestly to drag enhancement—to semi-dense regimes, where network effects and entanglement significantly alter the local flow field and lead to nonlinear drag amplification. This progression is particularly relevant in yield-stress fluids, where the interplay between fiber-induced microstructure and apparent viscosity manifests as a shift in both the threshold and slope of drag variation.
Notably, the slightly lower R2 values observed in certain fitting regions (e.g., near the transition between flow initiation and steady settling) can be attributed to local experimental variability and the sensitivity of yield-stress fluids to minor disturbances in stress distribution. Despite this, the overall model behavior remains stable and predictable, indicating strong generalizability across typical operational fiber concentrations and geometries used in drilling fluid formulations.
From a practical standpoint, the availability of such empirical surface models significantly enhances the utility of the unified framework. Engineers can rapidly estimate drag and settling behavior across a spectrum of fluid compositions without resorting to time-consuming numerical simulations or laboratory trials. Moreover, the parametric surfaces serve as a bridge between rheological measurements and field-scale transport predictions, supporting real-time decision-making during fiber-assisted hole-cleaning operations.
A HB = 0.0144 + 0.172 L f + 0.0196 L f 2 + 173.82 C f 171.41 C f 2 + 0.159 L f C f
B HB = 1.697 + 0.069 L f 0.0001 L f 2 + 10.756 C f 21.85 C f 2 0.456 L f C f

5.4. Comparison Between Experimental Data and Model Predictions

A unified model for total drag coefficient was constructed by superimposing viscous and fiber-induced drag:
C dt = C dv + C df
An iterative algorithm was used to solve for the implicit variables and compute the predicted total drag coefficients and terminal velocities under various conditions. After excluding data points with relative errors exceeding 40%, the remaining dataset was used to refit the model and assess its accuracy using mean relative error (MRE) as the performance metric.
Figure 13 and Figure 14 compare predicted and experimental values for power-law and Herschel–Bulkley fluids.
In power-law systems, MRE values for total drag and terminal velocity were 5.17% and 3.57%, respectively, with maximum deviations of 24.65% and 10.43%. These relatively low error margins indicate that the unified prediction model is capable of effectively capturing the composite drag behavior induced by fiber addition, even under the inherent nonlinearity of shear-thinning rheology. The slightly higher maximum deviation for total drag suggests that local fiber–particle interactions or microstructural heterogeneities may introduce intermittent deviations, especially under conditions of low shear rates or inhomogeneous fiber dispersion.
For Herschel–Bulkley systems, which combine yield stress and shear-thinning, the model achieved MREs of 9.95% for total drag and 5.12% for terminal velocity. This performance underscores the robustness of the model’s parameterization strategy, particularly its ability to generalize over the combined effects of yield stress and fiber-induced structural resistance. The slightly elevated error values in these systems can be attributed to the difficulty in accurately resolving the onset of motion (yield point) and its influence on the drag evolution during the settling process.
Importantly, the model exhibited superior performance in power-law systems compared to Herschel–Bulkley fluids. This disparity may reflect the simpler rheological behavior of power-law fluids, where the absence of a yield stress allows for a more straightforward mapping between flow field evolution and fiber–particle drag interactions. In contrast, the presence of a threshold stress in Herschel–Bulkley systems introduces additional complexity, particularly in regimes where fiber networks contribute to an apparent increase in yield threshold or modulate local flow activation.
From an engineering perspective, this unified model provides a reliable predictive tool for optimizing fiber-laden drilling fluids, particularly in horizontal and extended-reach wells, where accurate drag estimation is critical. The unified drag model enhances prior approaches by enabling more accurate prediction of particle settling in fiber-containing non-Newtonian drilling fluids, thereby offering practical utility for real-time cutting transport simulations in complex wellbore environments. The low average and peak errors validate the model’s applicability for design evaluation, real-time parameter optimization, and performance analysis. Furthermore, the model shows potential for integration into field-scale multiphase flow simulators, supporting advanced applications in hole cleaning and sand transport. Future work could explore model extensions to irregular particle shapes, dynamic flow conditions, and integration into CFD simulations for broader engineering applications.
It should be noted that the proposed model was developed based on experiments with spherical particles in dilute suspensions. Its direct applicability to irregularly shaped particles or highly concentrated systems may be limited and requires further investigation. Future work could extend the present model to semi-dilute or concentrated fiber suspensions by incorporating fiber–fiber interactions, orientation dynamics, and local microstructural effects into the drag formulation.

6. Conclusions and Outlook

This study systematically investigated the settling behavior of spherical particles in fiber-containing non-Newtonian fluids, and developed a unified predictive model for total drag by incorporating fiber structural parameters. The main findings are summarized as follows.
  • An increase in fiber concentration and length leads to a marked rise in fluid viscosity and yield stress. This effect is particularly pronounced in low-concentration base fluids, indicating that the fiber network structure plays a key role in modulating the rheological behavior of the system.
  • Experimental results confirmed that fiber-induced drag significantly reduces the terminal settling velocity of particles. Existing drag models for non-Newtonian fluids produce notable prediction errors when directly applied to fiber-laden systems, underscoring the necessity for fiber-specific modeling frameworks.
  • By embedding fiber concentration and length into the parameter expressions of the drag model, the proposed formulation avoids the redundancy of traditional piecewise fitting and enhances continuity, scalability, and engineering applicability across diverse conditions.
  • The unified predictive model demonstrates good agreement with experimental data for both power-law and Herschel–Bulkley fluids. The mean relative errors for both terminal velocity and total drag coefficient remained within acceptable ranges, confirming the model’s robustness and practical utility.
  • Overall, the findings of this study offer both theoretical insights and practical modeling tools for the design optimization of fiber-enhanced drilling fluids, facilitating improved hole-cleaning efficiency and enhanced control over particle settling behavior in complex downhole environments.
Despite these advances, some limitations should be acknowledged. The random orientation and distribution of fibers in the suspension can lead to local variations in resistance forces, which are not explicitly captured by the current model. Additionally, wall effects—particularly for particles settling near the container boundary—may influence settling trajectories despite efforts to mitigate them. Furthermore, time-dependent microstructural changes in the fiber network (e.g., flocculation or shear-induced alignment) are not considered, although the experiments were conducted under quasi-steady-state conditions.
Future work will aim to refine the model by incorporating fiber orientation statistics and exploring the role of dynamic rheological behavior. Expanding the framework to account for higher fiber concentrations and non-spherical particles may also enhance the generalizability of the proposed correlations to more complex real-world applications, such as real-time drilling simulations and fiber-laden hydraulic fracturing fluids.

Author Contributions

Conceptualization, H.Z.; data curation, C.L.; investigation, H.Z.; validation, Y.L.; writing—original draft, L.T. and J.Q.; writing—review and editing, H.W. All authors have read and agreed to the published version of the manuscript.

Funding

This research was funded by the 2023 Open Fund of the Sinopec Key Laboratory of Drilling Completion and Fracturing of Shale Oil and Gas (project title: Study on Cuttings Transport Mechanism and Hole Cleaning Performance Evaluation in Horizontal Wells for Shale Oil and Gas) and by the Hainan Provincial Joint Project of Sanya Yazhou Bay Science and Technology City (grant 2021CXLH0028).

Conflicts of Interest

Author Hui Zhang, Heng Wang was employed by the SINOPEC Research Institute of Petroleum Engineering Co., Ltd. Author Yinsong Liu, Liang Tao, Jingyu Qu was employed by the Sanya Offshore Oil & Gas Research Institute of Northeast Petroleum University. Author Chao Liang was employed by the School of Physics, Sun Yat-Sen University. The remaining authors declare that the research was conducted in the absence of any commercial or financial relationships that could be construed as a potential conflict of interest.

References

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Figure 1. Schematic of the particle settling apparatus.
Figure 1. Schematic of the particle settling apparatus.
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Figure 2. Schematic diagram of three polyester fibers with different lengths.
Figure 2. Schematic diagram of three polyester fibers with different lengths.
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Figure 3. Consistency coefficient variation with fiber mass concentration: (a) 1% power-law fluid; (b) 2% power-law fluid.
Figure 3. Consistency coefficient variation with fiber mass concentration: (a) 1% power-law fluid; (b) 2% power-law fluid.
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Figure 4. Consistency coefficient variation with fiber mass concentration: (a) 0.06% Herschel–Bulkley fluid; (b) 0.1% Herschel–Bulkley fluid.
Figure 4. Consistency coefficient variation with fiber mass concentration: (a) 0.06% Herschel–Bulkley fluid; (b) 0.1% Herschel–Bulkley fluid.
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Figure 5. Yield stress variation with fiber mass concentration: (a) 0.06% Herschel–Bulkley fluid; (b) 0.1% Herschel–Bulkley fluid.
Figure 5. Yield stress variation with fiber mass concentration: (a) 0.06% Herschel–Bulkley fluid; (b) 0.1% Herschel–Bulkley fluid.
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Figure 6. Consistency coefficient variation with fiber length: (a) 1% power-law fluid; (b) 2% power-law fluid.
Figure 6. Consistency coefficient variation with fiber length: (a) 1% power-law fluid; (b) 2% power-law fluid.
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Figure 7. Consistency coefficient variation with fiber length: (a) 0.06% Herschel–Bulkley fluid; (b) 0.1% Herschel–Bulkley fluid.
Figure 7. Consistency coefficient variation with fiber length: (a) 0.06% Herschel–Bulkley fluid; (b) 0.1% Herschel–Bulkley fluid.
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Figure 8. Yield stress variation with fiber length: (a) 0.06% Herschel–Bulkley fluid; (b) 0.1% Herschel–Bulkley fluid.
Figure 8. Yield stress variation with fiber length: (a) 0.06% Herschel–Bulkley fluid; (b) 0.1% Herschel–Bulkley fluid.
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Figure 9. Settling process of a single particle in fiber-containing drilling fluid.
Figure 9. Settling process of a single particle in fiber-containing drilling fluid.
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Figure 10. Relationship between fiber-induced drag coefficient Cdf and particle Reynolds number Res.
Figure 10. Relationship between fiber-induced drag coefficient Cdf and particle Reynolds number Res.
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Figure 11. Fitting results of empirical model parameters in power-law fluid: (a) parameter Apl; (b) parameter Bpl, where red indicates the maximum value and blue indicates the minimum value.
Figure 11. Fitting results of empirical model parameters in power-law fluid: (a) parameter Apl; (b) parameter Bpl, where red indicates the maximum value and blue indicates the minimum value.
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Figure 12. Fitting results of empirical model parameters in Herschel–Bulkley fluid: (a) parameter AHB; (b) parameter BHB, where red indicates the maximum value and blue indicates the minimum value.
Figure 12. Fitting results of empirical model parameters in Herschel–Bulkley fluid: (a) parameter AHB; (b) parameter BHB, where red indicates the maximum value and blue indicates the minimum value.
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Figure 13. Comparison between experimental and predicted values in power-law fluid: (a) total drag coefficient, including contributions from base fluid and suspended fibers; (b) terminal settling velocity.
Figure 13. Comparison between experimental and predicted values in power-law fluid: (a) total drag coefficient, including contributions from base fluid and suspended fibers; (b) terminal settling velocity.
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Figure 14. Comparison between experimental and predicted values in Herschel–Bulkley fluid: (a) total drag coefficient, including contributions from base fluid and suspended fibers; (b) terminal settling velocity.
Figure 14. Comparison between experimental and predicted values in Herschel–Bulkley fluid: (a) total drag coefficient, including contributions from base fluid and suspended fibers; (b) terminal settling velocity.
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Table 1. Experimental devices and measurement accuracy.
Table 1. Experimental devices and measurement accuracy.
DeviceRangeAccuracy
Electronic balance0–200 g±0.1 mg
High-speed camera/100 fps
Rheometer0.01–1000 Pa·s±1%
Temperature sensor−20–150 °C±0.1 °C
Water bathAmbient–ambient + 30 °C±0.1 °C
Table 2. Diameters and densities of test particles.
Table 2. Diameters and densities of test particles.
Particle MaterialParticle Diameter (mm)Density (kg/m3)
Stainless Steel2, 2.5, 3, 4, 57980
Zirconia (ZrO2)2, 3, 4, 56100
Silicon Nitride (Si3N4)2, 3, 4, 53200
Aluminum1, 1.5, 2, 2.5, 3, 3.5, 42700
POM1.5, 2, 3, 41400
Table 3. Rheological parameters of Carbopol U20 test fluids.
Table 3. Rheological parameters of Carbopol U20 test fluids.
Test FluidMass Concentration, wt (%)Temperature (°C)Rheological Parameters
Yield Stress, τ0 (Pa)Consistency Index, K (Pa·sn)Flow Behavior Index, n
Dilute Power-Law Fluid1.026.600.04850.896
Concentrated Power-Law Fluid2.026.600.55310.706
Dilute Herschel–Bulkley Fluid0.0627.40.130.05240.820
Concentrated Herschel–Bulkley Fluid0.1027.41.130.25820.710
Table 4. Drag coefficient models for non-Newtonian fluids.
Table 4. Drag coefficient models for non-Newtonian fluids.
Model SourceApplicable Fluid TypeMathematical Model
Khan and Richardson [13]Power-law and Herschel–Bulkley C D = ( 2.25 R e s 0.31 + 0.36 R e s 0.06 ) 3.45
Kelessidis et al. [15]Power-law C D = 24 R e s ( 1 + 0.1407 R e s 0.6018 ) + 0.2118 1 + 0.4215 / R e s
Yan et al. [20]Power-law C D = 24 R e s ( 1 + 0.1407 R e s 0.6018 ) + 0.2118 1 + 0.4215 / R e s
Okesanya et al. [19]Herschel–Bulkley C D = 24 R e s ( 1 + 0.12 R e s ) 0.35 + 0.398 1 exp ( 0.01 R e s 0.9282 )
Yan et al. [20]Herschel–Bulkley C D = 24 R e s ( 1 + 0.282 R e s 0.229 ) 167.28 1 33000 R e s
Table 5. Model performance for spherical particle settling in power-law fluids.
Table 5. Model performance for spherical particle settling in power-law fluids.
Model SourceApplicable Fluid TypeRMSEMRE
Khan and Richardson [13]Power-law3.8512.78%
Kelessidis et al. [15]Power-law2.6510.71%
Yan et al. [20]Power-law1.2214.41%
Khan and Richardson [13]Herschel–Bulkley29.1816.31%
Okesanya et al. [19]Herschel–Bulkley30.7726.90%
Yan et al. [20]Herschel–Bulkley19.7522.33%
Table 6. Summary of key nondimensional parameters and experimental conditions.
Table 6. Summary of key nondimensional parameters and experimental conditions.
ParameterRange/Values
Particle Reynolds number Res0.018–740.4
Fiber length (mm)0–12
Fiber concentration %0–0.15
Table 7. Parameter fitting results in power-law fluids.
Table 7. Parameter fitting results in power-law fluids.
Fiber Mass Concentration wt (%)Fiber Length L (mm)Parameter AParameter B
60.030.96−0.57
60.063.62−0.55
60.099.27−0.62
90.031.74−0.53
90.065.75−0.58
90.0910.99−0.62
120.032.54−0.56
120.067.27−0.60
120.0915.04−0.67
Table 8. Parameter fitting results in Herschel–Bulkley fluids.
Table 8. Parameter fitting results in Herschel–Bulkley fluids.
Fiber Mass Concentration wt (%)Fiber Length L (mm)Parameter AParameter B
60.036.65−1.13
60.0611.78−0.91
60.0916.12−0.79
90.038.41−1.00
90.0613.16−0.87
90.0917.27−0.78
120.0310.05−0.93
120.0614.56−0.85
120.0919.57−0.77
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Zhang, H.; Wang, H.; Liu, Y.; Tao, L.; Qu, J.; Liang, C. Experimental Study on Particle Settling in Fiber-Containing Non-Newtonian Fluids. Processes 2025, 13, 2542. https://doi.org/10.3390/pr13082542

AMA Style

Zhang H, Wang H, Liu Y, Tao L, Qu J, Liang C. Experimental Study on Particle Settling in Fiber-Containing Non-Newtonian Fluids. Processes. 2025; 13(8):2542. https://doi.org/10.3390/pr13082542

Chicago/Turabian Style

Zhang, Hui, Heng Wang, Yinsong Liu, Liang Tao, Jingyu Qu, and Chao Liang. 2025. "Experimental Study on Particle Settling in Fiber-Containing Non-Newtonian Fluids" Processes 13, no. 8: 2542. https://doi.org/10.3390/pr13082542

APA Style

Zhang, H., Wang, H., Liu, Y., Tao, L., Qu, J., & Liang, C. (2025). Experimental Study on Particle Settling in Fiber-Containing Non-Newtonian Fluids. Processes, 13(8), 2542. https://doi.org/10.3390/pr13082542

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