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Technologies 2015, 3(4), 182-197;

Microwave-Assisted Preparation of High Entropy Alloys

Department of Engineering "Enzo Ferrari", University of Modena and Reggio Emilia, Via Vivarelli 10, 41125 Modena, Italy
These authors contributed equally to this work.
Author to whom correspondence should be addressed.
Academic Editor: Manoj Gupta
Received: 21 August 2015 / Revised: 24 September 2015 / Accepted: 25 September 2015 / Published: 7 October 2015
(This article belongs to the Special Issue Microwave Energy Applications)
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Microwaves at the ISM (Industrial, Scientific and Medical, reserved internationally) frequency of 2450 or 5800 MHz have been used to prepare FeCoNiCuAl, FeCrNiTiAl and FeCoCrNiAl2.5 high entropy alloys by direct heating of pressed mixtures of metal powders. The aim of this work is to explore a new microwave-assisted near-net-shape technology, using a powder metallurgy approach for the preparation of high entropy alloys, able to overcome the limits of current melting technologies (defects formation) or solid state ones (time demanding). High entropy alloy compositions have been selected so as to comprise at least one ferromagnetic element and one highly reactive couple, like Ni-Al, Ti-Al, Co-Al or Fe-Al. Results show that direct microwave heating of the powder precursors occurs, and further heating generation is favored by the ignition of exothermal reactions in the load. Microwaves have been applied both for the ignition and sustaining of such reactions, showing that by the proposed technique, it is possible to control the cooling rate of the newly-synthesized high entropy alloys. Results showed also that microwave heating in predominant magnetic field regions of the microwave applicator is more effective at controlling the cooling rate. The herein proposed microwave-assisted powder metallurgy approach is suitable to retain the shape of the load imparted during forming by uniaxial pressing. The homogeneity of the prepared high entropy alloys in all cases was good, without the dendritic segregation typical of arc melting, even if some partially-unreacted powders were detected in the samples. View Full-Text
Keywords: high entropy alloys; microwave heating; powder metallurgy; microstructure; synthesis high entropy alloys; microwave heating; powder metallurgy; microstructure; synthesis

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Veronesi, P.; Rosa, R.; Colombini, E.; Leonelli, C. Microwave-Assisted Preparation of High Entropy Alloys. Technologies 2015, 3, 182-197.

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