Effect of Fe3O4 Nanoparticles Modified by Citric and Oleic Acids on the Physicochemical and Magnetic Properties of Hybrid Electrospun P(VDF-TrFE) Scaffolds
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Synthesis of Magnetite Nanoparticles Modified by Citric and Oleic Acids
2.3. Preparation of Electrospinning Solutions
2.4. Electrospinning Parameters
2.5. Characterization of the Samples
3. Results and Discussion
4. Conclusions
Author Contributions
Funding
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Sample | Ms, emu/g | Mra, emu/g | Hc, Oe |
---|---|---|---|
Fe3O4-CA | 61.9 ± 1.9 | 0.5 ± 0.1 | 10.0 ± 0.5 |
Fe3O4-OA | 72.6 ± 3.6 | 0.6 ± 0.03 | 8.0 ± 0.4 |
Sample | Tm, °C | ΔHm, J/g | Xc,% |
---|---|---|---|
P(VDF-TrFE) | 147.4 | 27.30 | 60.7 |
P(VDF-TrFE)/Fe3O4-CA 5% | 147.7 | 25.58 | 59.8 |
P(VDF-TrFE)/Fe3O4-CA 10% | 147.8 | 22.80 | 56.3 |
P(VDF-TrFE)/Fe3O4-CA 15% | 148.4 | 29.04 | 75.9 |
P(VDF-TrFE)/Fe3O4-OA 5% | 148.2 | 32.00 | 74.8 |
P(VDF-TrFE)/Fe3O4-OA 10% | 148.4 | 26.68 | 65.9 |
P(VDF-TrFE)/Fe3O4-OA 15% | 147.9 | 29.42 | 76.9 |
Sample | Ms, emu/g | Mra, emu/g | Hc, Oe |
---|---|---|---|
P(VDF-TrFE)/Fe3O4-CA (5 wt.%) | 4.4 ± 0.2 | 0.14 | 28 ± 1 |
P(VDF-TrFE)/Fe3O4-CA (10 wt.%) | 7.9 ± 0.4 | 0.18 | 22 ± 1 |
P(VDF-TrFE)/Fe3O4-CA (15 wt.%) | 10.0 ± 0.5 | 0.26 | 24 ± 1 |
P(VDF-TrFE)/Fe3O4-OA (5 wt.%) | 4.2 ± 0.2 | 0.16 | 35 ± 2 |
P(VDF-TrFE)/Fe3O4-OA (10 wt.%) | 6.8 ± 0.3 | 0.23 | 30 ± 2 |
P(VDF-TrFE)/Fe3O4-OA (15 wt.%) | 8.8 ± 0.4 | 0.16 | 17 ± 1 |
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Botvin, V.; Fetisova, A.; Mukhortova, Y.; Wagner, D.; Kazantsev, S.; Surmeneva, M.; Kholkin, A.; Surmenev, R. Effect of Fe3O4 Nanoparticles Modified by Citric and Oleic Acids on the Physicochemical and Magnetic Properties of Hybrid Electrospun P(VDF-TrFE) Scaffolds. Polymers 2023, 15, 3135. https://doi.org/10.3390/polym15143135
Botvin V, Fetisova A, Mukhortova Y, Wagner D, Kazantsev S, Surmeneva M, Kholkin A, Surmenev R. Effect of Fe3O4 Nanoparticles Modified by Citric and Oleic Acids on the Physicochemical and Magnetic Properties of Hybrid Electrospun P(VDF-TrFE) Scaffolds. Polymers. 2023; 15(14):3135. https://doi.org/10.3390/polym15143135
Chicago/Turabian StyleBotvin, Vladimir, Anastasia Fetisova, Yulia Mukhortova, Dmitry Wagner, Sergey Kazantsev, Maria Surmeneva, Andrei Kholkin, and Roman Surmenev. 2023. "Effect of Fe3O4 Nanoparticles Modified by Citric and Oleic Acids on the Physicochemical and Magnetic Properties of Hybrid Electrospun P(VDF-TrFE) Scaffolds" Polymers 15, no. 14: 3135. https://doi.org/10.3390/polym15143135