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Open AccessArticle

In-Situ Direct Synthesis of HKUST-1 in Wool Fabric for the Improvement of Antibacterial Properties

1
Institute of Textile Research and Cooperation of Terrassa, Polytechnic University of Catalonia, C/Colom 15, Terrassa, 08222 Barcelona, Spain
2
Textile Engineering, Federal University of Technology—Paraná, 635 Marcilio Dias St., Apucarana, 86812-60 Parana, Brazil
3
Chemistry Engineering, Federal University of Technology—Paraná, 635 Marcilio Dias St., Apucarana, 86812-60 Parana, Brazil
4
Núcleo de Inovação Industria (NI2), Federal University of Technology—Paraná, 635 Marcilio Dias St., Apucarana, 86812-60 Parana, Brazil
*
Author to whom correspondence should be addressed.
Polymers 2019, 11(4), 713; https://doi.org/10.3390/polym11040713
Received: 23 January 2019 / Revised: 15 April 2019 / Accepted: 16 April 2019 / Published: 19 April 2019
(This article belongs to the Special Issue Polymeric Materials for Tissue Engineering)
The use of Metal-Organic Frameworks (MOF) such as HKUST-1 in textiles is an alternative with regard to the development of technologies that are increasingly seeking for functionalities, mainly in the fields of health and hygiene, named biofunctional fabrics. However, the application of the MOF under the surface of the wool fiber can lead to a low durability finish due to its low fixation. Thus, this project aims to perform the direct synthesis of HKUST in the wool fiber, so that a product with good washing durability can be obtained. The purpose of this study was to incorporate metal-organic frameworks, composed of copper and trimesic acid, into woolen fabrics, to improve the antibacterial properties. The synthesis was performed directly in the wool fabric, at time intervals of 24 and 48 h. The resulting fabrics were characterized by Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDS), X-Ray Diffractometry (XRD), Fourier Transform Spectroscopy Infrared-Attenuated Total Reflectance (FTIR-ATR), and colorimetric analysis (CIElab), and the Antimicrobial Activity Test (American Association of Textile Chemist and Colourists - AATCC Test Method 61-2007-2A) was performed. The results suggested that the application produced textiles with antibacterial properties, showing activity against Escherichia coli. View Full-Text
Keywords: HKUST-1; wool; antibacterial HKUST-1; wool; antibacterial
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Lis, M.J.; Caruzi, B.B.; Gil, G.A.; Samulewski, R.B.; Bail, A.; Scacchetti, F.A.P.; Moisés, M.P.; Maestá Bezerra, F. In-Situ Direct Synthesis of HKUST-1 in Wool Fabric for the Improvement of Antibacterial Properties. Polymers 2019, 11, 713.

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