Effect of Ultraviolet Light on the Shear Bond Strength of Commercial Dental Adhesives
Abstract
1. Introduction
2. Materials and Methods
2.1. Investigated Dental Adhesives
2.2. Sample Preparation
2.3. UV-Light Exposure
2.4. Shear Bond Testing
2.5. Statistical Analysis
3. Results
4. Discussion
5. Conclusions
Author Contributions
Funding
Data Availability Statement
Acknowledgments
Conflicts of Interest
Abbreviations
MDPI | Multidisciplinary Digital Publishing Institute |
DOAJ | Directory of open access journals |
LCU | Light-curing unit |
UV | Ultraviolet |
SBS | Shear bond strength |
TLA | Three letter acronym |
LD | Linear dichroism |
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Name | Manufacturer | LOT | Ingredients | |
---|---|---|---|---|
Universal Adhesives | Ecosite Bond® | DMG®, Hamburg, Germany | 283939 | HEMA, bis-GMA, ethanol, MDP, water, EHA, 2-ethylhexyl 4-(dimenthylamino)benzoate |
Scotchbond™ Universal Plus® | 3M™®, Neuss, Germany | 9952921 | Bromilated dimethacrylate, methacrylate (HEMA), phosphorylated methacrylate, ethyl-alcohol, silanized silica, water, polymeric acid, campherquinone, aromatic amine | |
Adhese® Universal | Ivoclar®, Schaan, Liechtenstein | Z04XF0 | HEMA, bis-GMA, D3MA, MDP, ethanol, water, methacrylate-modified polyacrylic acid, silicon dioxide, campherquinone, ethyl p-dimethylamino-benzoate, 2-dimethylaminoethyl-methacrylate | |
Etch-and-Rinse Adhesives | iBOND® Total Etch | Kulzer® Mitsui Chemicals Group, Hanau, Germany | N010608 | UDMA, Ethanol, HEMA, water, methacrylated polycarboxylic acid, 4-META, glutardialdehyde |
Syntac classic© | Ivoclar®, Ellwangen, Germany | Primer: Z05CNM Adhesive: Z05BTZ Heliobond: Z0591M | PEG-dimethylacrylate, glutaraldehyde, water, acetone, TEGDEMA, maleic acid, bis-GMA | |
Solobond M© | Voco®, Cuxhaven, Germany | 2324174 | Acetone, bis-GMA, HEMA, catalyst, BHT, acid adhesive monomer | |
Prime and Bond XP© | Dentsply Sirona®, Charlotte, NC, USA | 2302000793 | TCB-resin, PENTA, UDMA, TEGDEMA, HEMA, butylated benzenediol, campherquinone, acetone, water |
Adhesive | Application Procedure | LCU-PolymeriZation Time | |
---|---|---|---|
Universal Adhesives | Ecosite Bond® | application time 10 s exposure time 20 s air-drying 5 s | 10 s |
Scotchbond™ Universal Plus® | comprehensive application exposure time 20 s air-drying 5 s | 10 s | |
Adhese® Universal | comprehensive application exposure time 20 s gently air-drying | 10 s | |
Etch-and-Rinse Adhesives | iBOND® Total Etch | active application exposure time 15 s air-drying 5 s | 20 s |
Syntac classic© | Syntac Primer: active application, exposure time 15 s, air-drying Syntac Adhesive: active application, exposure time 10 s, sufficient air drying Heliobond: application, exposure, air-blowing to thin layer | Heliobond: 10 s | |
Solobond M© | comprehensive application exposure time 30 s gently air-drying | 20 s | |
Prime and Bond XP© | comprehensive application exposure time 20 s air-drying 5 s | 10 s |
Universal Adhesives | Etch-and-Rinse Adhesives | ||||||
---|---|---|---|---|---|---|---|
Ecosite Bond® | Scotchbond™ Universal Plus® | Adhese® Universal | iBOND® Total Etch | Prime & Bond XP© | Solobond M© | Syntac© classic | |
mean SBS LCU-polymerization [MPa] | 2.63 ± 1.47 | 6.09 ± 2.63 | 3.96 ± 2.16 | 15.48 ± 8.35 | 15.20 ± 4.70 | 9.94 ± 4.53 | 17.60 ± 5.38 |
mean SBS post UV-exposure [MPa] | 1.52 ± 1.59 | 8.63 ± 5.55 | 5.48 ± 3.76 | 5.24 ± 4.24 | 12.91 ± 4.27 | 3.65 ± 1.89 | 24.12 ± 9.09 |
mean change in SBS [MPa] | −1.11 ± 2.03 | +2.54 ± 6.2 | +1.52 ± 3.89 | −10.24 ± 9.50 | −2.27 ± 4.84 | −6.29 ± 3.24 | +6.55 ± 10.24 |
p-value | 0.878 | 0.333 | 0.139 | 0.009 | 0.126 | 0.005 | 0.047 |
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© 2025 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
Share and Cite
Heyder, M.; Kranz, S.; Woelfel, J.S.; Raabe, T.; Guellmar, A.; Mrozinska, A.; Gottschaldt, M.; Schubert, U.S.; Sigusch, B.W.; Reise, M. Effect of Ultraviolet Light on the Shear Bond Strength of Commercial Dental Adhesives. Materials 2025, 18, 3772. https://doi.org/10.3390/ma18163772
Heyder M, Kranz S, Woelfel JS, Raabe T, Guellmar A, Mrozinska A, Gottschaldt M, Schubert US, Sigusch BW, Reise M. Effect of Ultraviolet Light on the Shear Bond Strength of Commercial Dental Adhesives. Materials. 2025; 18(16):3772. https://doi.org/10.3390/ma18163772
Chicago/Turabian StyleHeyder, Markus, Stefan Kranz, Johanna Sandra Woelfel, Tabea Raabe, André Guellmar, Anna Mrozinska, Michael Gottschaldt, Ulrich S. Schubert, Bernd W. Sigusch, and Markus Reise. 2025. "Effect of Ultraviolet Light on the Shear Bond Strength of Commercial Dental Adhesives" Materials 18, no. 16: 3772. https://doi.org/10.3390/ma18163772
APA StyleHeyder, M., Kranz, S., Woelfel, J. S., Raabe, T., Guellmar, A., Mrozinska, A., Gottschaldt, M., Schubert, U. S., Sigusch, B. W., & Reise, M. (2025). Effect of Ultraviolet Light on the Shear Bond Strength of Commercial Dental Adhesives. Materials, 18(16), 3772. https://doi.org/10.3390/ma18163772