Comparative Study on Viscoelastic Evaluation Methods of Polymer Materials Based on Ultrasonic Method
Abstract
:1. Introduction
2. Ultrasonic-based Viscoelastic Evaluation Method
2.1. Viscoelastic Evaluation Method
2.2. Bottom Reflection Method to Evaluate Material Viscoelasticity
2.3. Evaluation of Viscoelastic Properties of Materials by the Surface Reflection Method
3. Viscoelastic Evaluation of Different Rubber Materials by the BRM
3.1. Simulation Analysis Feasibility Verification
3.2. Research on the BRM through Experimentation and Simulation
4. Viscoelastic Evaluation by the SRM and Comparative Analysis of Results
4.1. Research on the SRM through Experimentation and Simulation
4.2. Result Analysis and Optimization
4.3. Verification of optimization method
5. Conclusions
Author Contributions
Funding
Conflicts of Interest
References
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Specification of the pulser/receiver | |
Pulse configuration | square burst pulse or chirp waves |
Bandwidth | 300 Hz~10 MHz |
Low pass (MHz) | 1.00, 2.00, 5.00 |
High pass (MHz) | 0.01, 0.20, 1.00 |
Gain | 0 to 80 dB |
Output impedance | 50 Ω |
Specification of the A/D transition | |
Sampling Clock | 100 MHz |
Analogue bandwidth | DC~50 MHz |
Input impedance | 50 Ω or 10 kΩ |
Sample Name | Filler | Hardness (HA) of Material | Glass Transition Temperature by DMA (°C) | Velocity (m/s) | Density ρ2 (kg/mm3) |
---|---|---|---|---|---|
EPX-46 | Silica | 41 | −66 | 1463 | 0.98 |
OR4Si | Silica | 45 | −50 | 1546 | 1.077 |
ORHS4Si | Silica | 48 | −24 | 1723 | 1.106 |
B4Si | Silica | 45 | −105 | 1520 | 1.059 |
Sample | By Experiment | By Analysis | Difference Rate |
---|---|---|---|
EPX-46 | 0.377 | 0.402 | 6.31% |
OR4Si | 0.688 | 0.744 | 7.53% |
ORHS4Si | 2.036 | 2.228 | 8.62% |
B4Si | 0.102 | 0.114 | 10.68% |
Sample | By Experiment | By Analysis | Difference Rate |
---|---|---|---|
EPX-46 | 0.018 | 0.0198 | 9.2% |
OR4Si | 0.034 | 0.0357 | 4.6% |
ORHS4Si | 0.105 | 0.108 | 3.0% |
B4Si | 0.005 | 0.0056 | 10.7% |
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Li, Y.-y.; Chang, J.-j.; Huang, L.; Tang, Y.-h. Comparative Study on Viscoelastic Evaluation Methods of Polymer Materials Based on Ultrasonic Method. Materials 2019, 12, 2948. https://doi.org/10.3390/ma12182948
Li Y-y, Chang J-j, Huang L, Tang Y-h. Comparative Study on Viscoelastic Evaluation Methods of Polymer Materials Based on Ultrasonic Method. Materials. 2019; 12(18):2948. https://doi.org/10.3390/ma12182948
Chicago/Turabian StyleLi, Yuan-yuan, Jun-jie Chang, Lin Huang, and Yong-hui Tang. 2019. "Comparative Study on Viscoelastic Evaluation Methods of Polymer Materials Based on Ultrasonic Method" Materials 12, no. 18: 2948. https://doi.org/10.3390/ma12182948