Silver Nanoplates for Colorimetric Determination of Xanthine in Human Plasma and in Fish Meat via Etching/Aggregation/Fusion Steps
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Instrument
2.3. Preparation of Ag Nanoplates
2.4. The Optimization of PVP in the Synthesis of AgP
2.5. Analytical Procedures
2.6. Determination of Xan in Fish Meat
2.7. Effects of Interfering Compounds
2.8. Xan Determination in Human Plasma
3. Results and Discussion
3.1. The Role of PVP Role in AgP Synthesis
3.2. Sensing Principle for Xan
3.3. Absorption Titration Curve of Xan
3.4. Xan Determination in Fish Meat
3.5. Effects of Interfering Compounds in Plasma
3.6. Xan Determination in Human Plasma
4. Conclusions
Supplementary Materials
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
References
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Material | Linear Range (μM) | Limit of Detection (μM) | Ref. |
---|---|---|---|
BSA−Au clusters a | 1.0−200 | 0.5 | [11] |
Se−g−C3N4 b | 0.16–40 | 0.016 | [27] |
AuNPs c | 0.125–6.0 | 0.023 | [9] |
BSA−DTT−CuNCs d (nanoclusters) | 0.50–100 | 0.38 | [28] |
WO3 nanosheets−TMB e | 25–200 | 1.24 | [8] |
Hemin@CDs f | 0.17−33 | 0.11 | [29] |
AgP | 0.15–0.60 0.61–3.00 | 0.001 | This work |
Xan Added (M) b | Commercial Assay Kit (M) a | Our Proposed Method (M) | Recovery (%) | R.S.D. (%) c |
---|---|---|---|---|
0.0 | 5.76 ± 0.54 | 5.47 ± 0.49 | / | 8.96 |
31.3 | 33.7 ± 3.98 | 33.8 ± 2.47 | 107.9 | 7.30 |
61.5 | 56.8 ± 6.96 | 59.6 ± 5.93 | 97.0 | 9.94 |
80.0 | 80.2 ± 4.97 | 82.4 ± 5.51 | 103.0 | 6.68 |
123.0 | 111.7 ± 10.56 | 128.3 ± 11.1 | 104.3 | 8.66 |
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Hsu, H.-C.; Liao, P.-W.; Lee, H.-T.; Liu, W.-C.; Ho, M.-L. Silver Nanoplates for Colorimetric Determination of Xanthine in Human Plasma and in Fish Meat via Etching/Aggregation/Fusion Steps. Sensors 2020, 20, 5739. https://doi.org/10.3390/s20205739
Hsu H-C, Liao P-W, Lee H-T, Liu W-C, Ho M-L. Silver Nanoplates for Colorimetric Determination of Xanthine in Human Plasma and in Fish Meat via Etching/Aggregation/Fusion Steps. Sensors. 2020; 20(20):5739. https://doi.org/10.3390/s20205739
Chicago/Turabian StyleHsu, Hung-Cheng, Pei-Wen Liao, Hsiang-Tzu Lee, Wei-Chen Liu, and Mei-Lin Ho. 2020. "Silver Nanoplates for Colorimetric Determination of Xanthine in Human Plasma and in Fish Meat via Etching/Aggregation/Fusion Steps" Sensors 20, no. 20: 5739. https://doi.org/10.3390/s20205739