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(1R,2S,5R)-2-Isopropyl-5-methylcyclohexyl 4-Aminobutyrate Hydrochloride

1
Department of Pharmaceutical Chemistry, I.I. Mechnikov Odessa National University, Odessa 65026, Ukraine
2
SSI “Institute for Single Crystals”, National Academy of Sciences of Ukraine, Kharkiv 61001, Ukraine
3
“INTERCHEM SLC”, Odessa 65080, Ukraine
4
A.V. Bogatsky Physico-Chemical Institute, National Academy of Sciences of Ukraine, Odessa 65080, Ukraine
5
Department of Organic and Pharmaceutical Technology, Odessa National Polytechnic University, Odessa 65044, Ukraine
*
Author to whom correspondence should be addressed.
Molbank 2017, 2017(3), M956; https://doi.org/10.3390/M956
Received: 29 July 2017 / Revised: 11 August 2017 / Accepted: 20 August 2017 / Published: 22 August 2017
(This article belongs to the Section Structure Determination)
The title ester (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 4-aminobutyrate hydrochloride was obtained in 96% yield via Steglich esterification. The structure of the target compound was established by FTIR, HR-MS, 1H-NMR, 13C-NMR spectral analysis, and single crystal X-ray diffraction study. Single crystals of the title ester suitable for X-ray investigation were obtained by slow evaporation of the methanolic solution at room temperature. The purity of compound was assessed using HPLC coupled to mass spectrometry. View Full-Text
Keywords: terpene; l-menthol; ester; X-ray diffraction terpene; l-menthol; ester; X-ray diffraction
MDPI and ACS Style

Nesterkina, M.; Shishkina, S.; Maltsev, G.; Rakipov, I.; Kravchenko, I. (1R,2S,5R)-2-Isopropyl-5-methylcyclohexyl 4-Aminobutyrate Hydrochloride. Molbank 2017, 2017, M956.

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