Preparation, Characterization and Catalytic Activity of Nickel Molybdate (NiMoO4) Nanoparticles
Abstract
:1. Introduction
2. Experimental
2.1. Catalyst Preparation
2.2. Characterization
2.3. Test of Nitrophenol Isomers Reduction
3. Results and Discussion
3.1. Characterizations of the Complex
3.2. Nickel Molybdate Characterization
3.2.1. X-ray Diffraction
3.2.2. Specific Surface Area Determination
3.2.3. Transmission Electron Microscopy
3.3. Reduction Test of Nitrophenol Isomers
4. Conclusions
Author Contributions
Conflicts of Interest
References
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Sample Availability: Samples of the compounds nickel molybdate (α-NiMOO4) are available from the authors. |
Catalyst | Type | Concentration of NP (mol/L) | Reaction Time (min) | References |
---|---|---|---|---|
NiMoO4 | Nanoparticles | 2 × 10−4 | 8 for 4-NP 3 for 3-NP 8 for 2-NP | This work |
CuFe2O4 | Nanoparticles | 3.6 × 10−5 | 4 for 4-NP 5 for 3-NP 3 for 2-NP | [44] |
NiFe2O4 | Nanoparticles | 3.6 × 10−5 | 38 for 4-NP 36 for 3-NP 28 for 2-NP | [44] |
CuO/γAl2O3 | Nanocomposites | 2.9 × 10−5 | 12 for 4-NP 20 for 3-NP 15 for 2-NP | [45] |
Ni/C black | Nanocomposites | 5.0 × 10−4 | 15 for 4-NP 15 for 3-NP 15 for 2-NP | [46] |
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Oudghiri-Hassani, H.; Al Wadaani, F. Preparation, Characterization and Catalytic Activity of Nickel Molybdate (NiMoO4) Nanoparticles. Molecules 2018, 23, 273. https://doi.org/10.3390/molecules23020273
Oudghiri-Hassani H, Al Wadaani F. Preparation, Characterization and Catalytic Activity of Nickel Molybdate (NiMoO4) Nanoparticles. Molecules. 2018; 23(2):273. https://doi.org/10.3390/molecules23020273
Chicago/Turabian StyleOudghiri-Hassani, Hicham, and Fahd Al Wadaani. 2018. "Preparation, Characterization and Catalytic Activity of Nickel Molybdate (NiMoO4) Nanoparticles" Molecules 23, no. 2: 273. https://doi.org/10.3390/molecules23020273