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Keywords = polarized neutron off-specular scattering

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21 pages, 2171 KiB  
Article
Artificial Magnetic Pattern Arrays Probed by Polarized Neutron Reflectivity
by Dmitry Gorkov, Boris P. Toperverg and Hartmut Zabel
Nanomaterials 2020, 10(5), 851; https://doi.org/10.3390/nano10050851 - 28 Apr 2020
Cited by 5 | Viewed by 3430
Abstract
Traditionally, neutron scattering is an essential method for the analysis of spin structures and spin excitations in bulk materials. Over the last 30 years, polarized neutron scattering in terms of reflectometry has also contributed largely to the analysis of magnetic thin films and [...] Read more.
Traditionally, neutron scattering is an essential method for the analysis of spin structures and spin excitations in bulk materials. Over the last 30 years, polarized neutron scattering in terms of reflectometry has also contributed largely to the analysis of magnetic thin films and magnetic multilayers. More recently it has been shown that polarized neutron reflectivity is, in addition, a suitable tool for the study of thin films laterally patterned with magnetic stripes or islands. We provide a brief overview of the fundamental properties of polarized neutron reflectivity, considering different domain states, domain fluctuations, and different domain sizes with respect to the neutron coherence volume. The discussion is exemplified by a set of simulated reflectivities assuming either complete polarization and polarization analysis, or a reduced form of polarized neutron reflectivity without polarization analysis. Furthermore, we emphasize the importance of the neutron coherence volume for the interpretation of specular and off-specular intensity maps, in particular when studying laterally non-homogeneous magnetic films. Finally, experimental results, fits, and simulations are shown for specular and off-specular scattering from a magnetic film that has been lithographically patterned into a periodic stripe array. These experiments demonstrate the different and mutually complementary information that can be gained when orienting the stripe array parallel or perpendicular to the scattering plane. Full article
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23 pages, 4166 KiB  
Article
Magnetic Structure of Ion-Beam Imprinted Stripe Domains Determined by Neutron Scattering
by Thomas Saerbeck, Henning Huckfeldt, Boris P. Toperverg and Arno Ehresmann
Nanomaterials 2020, 10(4), 752; https://doi.org/10.3390/nano10040752 - 15 Apr 2020
Cited by 7 | Viewed by 3247
Abstract
We present a detailed analysis of the in-plane magnetic vector configuration in head-to-head/tail-to-tail stripe domain patterns of nominal 5 μm width. The patterns have been created by He-ion bombardment induced magnetic patterning of a CoFe/IrMn3 exchange bias thin-film system. Quantitative information about [...] Read more.
We present a detailed analysis of the in-plane magnetic vector configuration in head-to-head/tail-to-tail stripe domain patterns of nominal 5 μm width. The patterns have been created by He-ion bombardment induced magnetic patterning of a CoFe/IrMn3 exchange bias thin-film system. Quantitative information about the chemical and magnetic structure is obtained from polarized neutron reflectometry (PNR) and off-specular scattering (OSS). The technique provides information on the magnetic vector orientation and magnitude along the lateral coordinate of the sample, as well as the chemical and magnetic layer structure as a function of depth. Additional sensitivity to magnetic features is obtained through a neutron wave field resonance, which is fully accounted for in the presented analysis. The scattering reveals a domain width imbalance of 5.3 to 3.7 μm of virgin and bombarded stripes, respectively. Further, we report that the magnetization in the bombarded stripe significantly deviates from the head-to-head arrangement. A domain wall of 0.6 μm with homogeneous magnetization direction is found to separate the two neighboring domains. The results contain detailed information on length scales and magnetization vectors provided by PNR and OSS in absolute units. We illustrate the complementarity of the technique to microscopy techniques for obtaining a quantitative description of imprinted magnetic domain patterns and illustrate its applicability to different sample systems. Full article
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13 pages, 837 KiB  
Article
Coherent Magnetization Rotation of a Layered System Observed by Polarized Neutron Scattering under Grazing Incidence Geometry
by Ryuji Maruyama, Thierry Bigault, Thomas Saerbeck, Dirk Honecker, Kazuhiko Soyama and Pierre Courtois
Crystals 2019, 9(8), 383; https://doi.org/10.3390/cryst9080383 - 26 Jul 2019
Cited by 8 | Viewed by 3757
Abstract
The in-plane magnetic structure of a layered system composed of polycrystalline grains smaller than the ferromagnetic exchange length was studied to elucidate the mechanism controlling the magnetic properties considerably different from the bulk using polarized neutron scattering under grazing incidence geometry. The measured [...] Read more.
The in-plane magnetic structure of a layered system composed of polycrystalline grains smaller than the ferromagnetic exchange length was studied to elucidate the mechanism controlling the magnetic properties considerably different from the bulk using polarized neutron scattering under grazing incidence geometry. The measured result, together with quantitative analysis based on the distorted wave Born approximation, showed that the in-plane length of the area with a uniform orientation of moments ranging from 0.5–1.1 μ m was not significantly varied during the process of demagnetization followed by remagnetization. The obtained behavior of moments is in good agreement with the two-dimensional random anisotropy model where coherent magnetization rotation is dominant. Full article
(This article belongs to the Special Issue Investigation of Nanostructures with X-ray Scattering Techniques)
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