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Keywords = nano-structured punch

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18 pages, 5360 KB  
Article
Anti-Icing and Frost Property of Superhydrophobic Micro-Nano Structures with Embossed Micro-Array Channels
by Han Luo, Xiaoliang Wang, Qiwei Li, Honglei Liu, Lei Chen, Debin Shan, Bin Guo and Jie Xu
Materials 2025, 18(20), 4813; https://doi.org/10.3390/ma18204813 - 21 Oct 2025
Viewed by 260
Abstract
Icing on aircraft surfaces during operation poses a threat to flight safety. As a passive anti-icing technology, hydrophobic microstructure can achieve long-term anti-icing. In this work, a composite process combining hot-embossing of PVD-coated punches with a low surface energy fluoride-modification scheme is proposed [...] Read more.
Icing on aircraft surfaces during operation poses a threat to flight safety. As a passive anti-icing technology, hydrophobic microstructure can achieve long-term anti-icing. In this work, a composite process combining hot-embossing of PVD-coated punches with a low surface energy fluoride-modification scheme is proposed to generate nanoscale cluster structures on hundreds of microns array channels to construct a superhydrophobic micro-nano composite structure. The droplet freezing and frosting behavior of the hydrophobic microstructures was analyzed, and it was found that the anti-icing and anti-frost properties of the microstructure surface improved with an increase in the microstructure period size (T). Compared with the original surface, the freezing time of the microstructure at T = 500 μm was delayed by 214.3% (7 s → 22 s), and the frost layer coverage time was delayed by 75.7% (70 s → 123 s). The maximum water contact angle of the superhydrophobic micro-nano composite structure was 153.3°, and the droplet freezing time was delayed to 95 s, which is a 1166.67% difference, indicating that the multi-stage micro-nano composite structure can significantly improve surface anti-icing performance. The main reason for this result is that the bottom of the microstructure can store air pockets, preventing droplet wetting and heat exchange. Full article
(This article belongs to the Section Advanced Nanomaterials and Nanotechnology)
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13 pages, 6076 KB  
Article
Fine Piercing of Amorphous Electrical Steel Sheet Stack by Micro-/Nano-Textured Punch
by Yukiya Komori, Yohei Suzuki, Kohta Abe, Tatsuhiko Aizawa and Tomomi Shiratori
Materials 2022, 15(5), 1682; https://doi.org/10.3390/ma15051682 - 23 Feb 2022
Cited by 10 | Viewed by 2317
Abstract
The periodic nanotexture was superposed to the micro-textured grooves on the side surface of the punch. These grooves with nanotextures were shaped to have parallel and vertical orientations to the punch stroke direction, respectively. A stack of five amorphous electrical steel sheets was [...] Read more.
The periodic nanotexture was superposed to the micro-textured grooves on the side surface of the punch. These grooves with nanotextures were shaped to have parallel and vertical orientations to the punch stroke direction, respectively. A stack of five amorphous electrical steel sheets was punched out with these micro-/nano-textured punches. The process affected zone at the vicinity of the punched hole was analyzed by SEM (Scanning Electron Microscopy) and a three-dimensional profilometer. The punch surfaces were also observed by SEM to describe the debris particle adhesion on them. The dimensional change in each layer of the stack before and after perforation was measured to describe the punching behavior with the comparison to the punch diameter. Full article
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13 pages, 9565 KB  
Article
Micro-/Nano-Texturing onto Plasma-Nitrided Tool Surface by Laser Printing for CNC Imprinting and Piercing
by Tatsuhiko Aizawa, Tomoaki Yoshino, Yohei Suzuki and Tadahiko Inohara
Micromachines 2022, 13(2), 265; https://doi.org/10.3390/mi13020265 - 6 Feb 2022
Cited by 5 | Viewed by 2511
Abstract
A new data transformation method for micro-manufacturing using a topological model for a micro-/nano-texture was proposed for a surface-decorated product. Femtosecond laser printing was utilized to form the micro-/nano-textures into the hardened thick layer of dies by plasma nitriding. At first, the plasma-nitrided [...] Read more.
A new data transformation method for micro-manufacturing using a topological model for a micro-/nano-texture was proposed for a surface-decorated product. Femtosecond laser printing was utilized to form the micro-/nano-textures into the hardened thick layer of dies by plasma nitriding. At first, the plasma-nitrided AISI316L flat substrate was laser-printed as a punch to imprint the tailored nano-textures onto the AA1060 aluminum plate for its surface decoration with topological emblems. Second, the plasma-nitrided SKD11 cylindrical punch was laser-trimmed to form the nanostructures on its side surface. This nano-texture was imprinted onto the hole surface concurrently with piercing a circular hole into electrical steel sheet. The fully burnished surface had a shiny, metallic quality due to the nano-texturing. The plasma nitriding, the laser printing and the CNC (computer numerical control) imprinting provided a way of transforming the tailored textures on the metallic product. Full article
(This article belongs to the Special Issue Micro and Nano Manufacturing (WCMNM 2021))
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12 pages, 6053 KB  
Article
Epitaxial Grown Carbon Nanotubes Reinforced Pyrocarbon Matrix in C/C Composites with Improved Mechanical Properties
by Ningkun Liu, Lingjun Guo, Gang Kou, Yunyu Li and Xuemin Yin
Materials 2021, 14(21), 6607; https://doi.org/10.3390/ma14216607 - 2 Nov 2021
Cited by 6 | Viewed by 2041
Abstract
In order to achieve the highly efficient preparation of high-performance carbon/carbon (C/C) composites, epitaxial grown carbon nanotubes (CNTs) and a pyrocarbon matrix were simultaneously synthesized to fabricate CNT-reinforced C/C composites (CC/C composites). With precise control of the temperature gradient, CNTs and the pyrocarbon [...] Read more.
In order to achieve the highly efficient preparation of high-performance carbon/carbon (C/C) composites, epitaxial grown carbon nanotubes (CNTs) and a pyrocarbon matrix were simultaneously synthesized to fabricate CNT-reinforced C/C composites (CC/C composites). With precise control of the temperature gradient, CNTs and the pyrocarbon matrix could grow synchronously within a 2D needle-punched carbon fiber preform. Surprisingly, the CNTs remained intact within the pyrocarbon matrix at the nano-level, and the CNT-reinforced nano-pyrocarbon matrix was compact, with virtually no gaps and pores, which were tightly connected with the carbon fibers without cracks. Based on the results of Raman analysis, there is less residual stress in the CNT-reinforced pyrocarbon matrix and carbon fibers, and less of a mismatch between the coefficient and thermal expansion. Additionally, CC/C composites fabricated by this method could achieve a low density, open porosity with a large size, and improved mechanical properties. More importantly, our work provides a rational design strategy for the highly efficient preparation and structural design of high-performance CNT-einforced C/C composites. Full article
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14 pages, 4684 KB  
Article
Femtosecond Laser Trimming with Simultaneous Nanostructuring to Fine Piercing Punch to Electrical Amorphous Steel Sheets
by Tatsuhiko Aizawa, Tomomi Shiratori, Yoshihiro Kira, Tomoaki Yoshino and Yohei Suzuki
Micromachines 2021, 12(5), 568; https://doi.org/10.3390/mi12050568 - 17 May 2021
Cited by 5 | Viewed by 2746
Abstract
A CVD (Chemical Vapor Deposition) diamond coated tungsten carbide (WC) and cobalt (Co) sintered alloy punch was trimmed by the femtosecond laser machining to sharpen its edge with about 2 μm and to simultaneously make nanostructuring to its side surface. In addition to [...] Read more.
A CVD (Chemical Vapor Deposition) diamond coated tungsten carbide (WC) and cobalt (Co) sintered alloy punch was trimmed by the femtosecond laser machining to sharpen its edge with about 2 μm and to simultaneously make nanostructuring to its side surface. In addition to the sharpened edge, its edge profile was formed to be homogeneous enough to reduce the damage layer width by piercing the electrical amorphous steel sheet stack. Each brittle sheet in the stacked work was damaged to have three kinds of defects by piercing; e.g., the droop-like cracking in the thickness and at the vicinity of hole, the wrinkling in peak-to-valley with partial cracking on the peaks, and the circumferential cracking. When using the WC (Co) punch with the inhomogeneous edge profile in the sharpened edge width, these three damages were induced into each sheet and the maximum damage width exceeded 80 μm. When using the punch with the sharpened edge and homogeneous edge profile, the wrinkling mode was saved and the total affected layer width was significantly reduced to less than 20 μm. Through the precise embossing experiments, this effect of punch edge profile condition to the induced damages was discussed with a statement on the nanostructuring effect on the reduction of damaged width in electrical amorphous steel sheets. The developed tool with the sharpened edge and homogenous edge condition contributes to the realization of a low iron loss motor with a reduced affected layer width. Full article
(This article belongs to the Special Issue Micro/Nano-surfaces: Fabrication and Applications)
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12 pages, 16750 KB  
Article
Simultaneous Nano-Texturing onto a CVD-Diamond Coated Piercing Punch with Femtosecond Laser Trimming
by Tatsuhiko Aizawa, Tomomi Shiratori, Yoshihiro Kira and Tadahiko Inohara
Appl. Sci. 2020, 10(8), 2674; https://doi.org/10.3390/app10082674 - 13 Apr 2020
Cited by 17 | Viewed by 4047
Abstract
In this study, a CVD (Chemical Vapor Deposition)-diamond coated tungsten carbide cobalt (WC (Co)) punch was trimmed to adjust its surface roughness and to significantly reduce its edge curvature for fine piercing by femtosecond laser processing. Through this laser trimming, the surface quality [...] Read more.
In this study, a CVD (Chemical Vapor Deposition)-diamond coated tungsten carbide cobalt (WC (Co)) punch was trimmed to adjust its surface roughness and to significantly reduce its edge curvature for fine piercing by femtosecond laser processing. Through this laser trimming, the surface quality of the diamond coating and the punch edge profile were improved to less than 0.5 μm at the maximum roughness and 2 μm in the edge width, respectively. In parallel with this improvement of surface quality, the side surface of the diamond coating was modified to include nano-textures via the LIPSS (Laser Induced Periodic Surface Structuring) process. Through the fine piercing process, this nanotexture was transcribed onto the pierced hole surface together with fine shearing of the hole by piercing. WLI (White-Light Interferometry) and SEM (Scanning Electron Microscopy) were utilized to describe this transcription of nanotextures during the piercing process. These semiregular nanotextures with an LIPSS period of 300 nm on the pierced hole surface induced a blue colored surface plasmon. Full article
(This article belongs to the Special Issue Micro/Nano Manufacturing II)
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