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Leak detection and repair (LDAR) plays an important role in controlling the fugitive emission of volatile organic compound (VOC) from chemical enterprises. At present, many policies and standards issued in China have set clear requirements for implementing LDAR in the pharmaceutical industry. In this study, the LDAR work of nine typical pharmaceutical enterprises was selected for analysis to allow investigation of the characteristics of VOC emissions from leaking equipment components. Some suggestions for controlling VOC are proposed to provide a reference for managing the fugitive emissions of VOC from pharmaceutical enterprises. The results showed that the number of equipment components used by the pharmaceutical enterprises ranged from several thousand to more than 20,000, which is lower than that in oil refining and coal chemical enterprises. The predominant leaky component was the flange, which accounted for 56.31% of the total, followed by connectors (21.51%) and valves (18.53%). Light liquid medium components accounted for the largest proportion of equipment (52.83%) on average, followed by gas medium components (45.52%, on average). Heavy liquid medium components, which are rarely used in pharmaceuticals, accounted for only 1.65%. The average leak ratio of the components in the pharmaceutical industry was approximately 0.99%. The leak ratio of the open-ended line was much higher than that of other types of components, reaching an average of 5.00%, while that value was only 0.92% for the flange, despite the numbers and proportion of them that were in use. The total annual VOC leakage from the nine pharmaceutical enterprises studied in this work was 20.11 tons, with an average of 2.23 tons per enterprise and an average of 0.22 kg/a per equipment component. Flanges, connectors, and valves were the top three contributors to leakage, generating 39.17%, 38.72%, and 16.79% of the total, respectively, and a total proportion of 94.68%. Although the number of pumps accounted for only 0.15% of the components, it generated 1.94% of the leakage. In terms of different production processes, the greatest unit product leakage came from the bulk production of chemicals used for pharmaceuticals, reaching 0.085 t/a. The production from traditional Chinese medicine enterprises was the lowest (0.011 t/a), which was only 12.80% of the leakage from the bulk production of chemicals for drugs. The leakage of VOC from the equipment components in the nine enterprises was reduced, to varying degrees, using LDAR. The overall reduction ratio was between 23.55% and 67.72%, with an average of 44.02%. The reduction in leakage was relatively significant after the implementation of LDAR; however, there is still room for improvement. Pharmaceutical enterprises should improve their implementation of LDAR and reduce VOC leakage by reducing the number of inaccessible components used and increasing the repair ratio of leaky components. Controlling the source of component leakage, which should be emphasized, can be realized by cutting down the number of components used, adopting low-leakage equipment, and putting anti-leakage measures in place. Full article

Gas leaks in the oil and gas industry represent a safety risk as they, if ignited, may result in severe fires and/or explosions. Unignited, they have environmental impacts. This is particularly the case for methane leaks due to a significant Global Warming Potential (GWP). Since gas leak rates may span several orders of magnitude, that is, from leaks associated with potential major accidents to fugitive emissions on the order of 10⁻⁶ kg/s, it has been difficult to organize the leaks in an all-inclusive leak categorization model. The motivation for the present study was to develop a simple logarithmic table based on an existing consequence matrix for safety related incidents extended to include non-safety related fugitive emissions. An evaluation sheet was also developed as a guide for immediate risk evaluations when new leaks are identified. The leak rate table and evaluation guide were tested in the field at five land-based oil and gas facilities during Optical Gas Inspection (OGI) campaigns. It is demonstrated how the suggested concept can be used for presenting and analysing detected leaks to assist in Leak Detection and Repair (LDAR) programs. The novel categorization table was proven valuable in prioritizing repair of “super-emitter” components rather than the numerous minor fugitive emissions detected by OGI cameras, which contribute little to the accumulated emissions. The study was limited to five land based oil and gas facilities in Norway. However, as the results regarding leak rate distribution and “super-emitter” contributions mirror studies from other regions, the methodology should be generally applicable. To emphasize environmental impact, it is suggested to include leaking gas GWP in future research on the categorization model, that is, not base prioritization solely on leak rates. Research on OGI campaign frequency is recommended since frequent coarse campaigns may give an improved cost benefit ratio. Full article

Optical Gas Imaging (OGI) cameras represent an interesting tool for identifying leaking components in hydrocarbon processing and transport systems. They make it possible to see exactly where a leak originates, thereby enabling efficient leak detection and repair (LDAR) programs. The present paper reports on an OGI test campaign initiated by the Norwegian Environmental Agency (NEA), and how this campaign stimulated cross-disciplinary cooperation at an LNG plant for better control of both fugitive hydrocarbon emissions and safety-related leaks. A surprising potentially severe leak detected in the NEA campaign triggered the introduction of in-house OGI cameras at plants and refineries, and an inter-disciplinary cooperation between specialists in the environment, technical safety and operations. Some benefits of in-house OGI cameras, as well as some concerns regarding their use are presented and discussed. The general experience is that an Ex safe, i.e., rated for safe use in a combustible hydrocarbon gas atmosphere, OGI camera, represents a very valuable tool for detecting fugitive emissions as the start point for LDAR programs. An OGI camera did, however, also turn out to be a valuable tool for fire and explosion risk management, and has led to reduced downtime after leak incidents. The concerns relate to leaks seen through the OGI camera that may look overwhelming, even with concentrations well below the ignitable limits of the released gas. Based on the LNG plant experiences, it is generally recommended that specialists in the environment, technical safety, operations and teaching fields cooperate regarding the introduction and use of OGI cameras. Suggestions for training courses are also discussed. Full article