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Keywords = calibration of spherical indenters

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11 pages, 9419 KB  
Article
Finite Element Analysis of the Mechanical Response for Cylindrical Lithium-Ion Batteries with the Double-Layer Windings
by Young Ju Ahn
Energies 2024, 17(14), 3357; https://doi.org/10.3390/en17143357 - 9 Jul 2024
Cited by 4 | Viewed by 1919
Abstract
The plastic properties for the jellyroll of lithium-ion batteries showed different behavior in tension and compression, showing the yield strength in compression being several times higher than in tension. The crushable foam models were widely used to predict the mechanical responses to compressive [...] Read more.
The plastic properties for the jellyroll of lithium-ion batteries showed different behavior in tension and compression, showing the yield strength in compression being several times higher than in tension. The crushable foam models were widely used to predict the mechanical responses to compressive loadings. However, since the compressive characteristic is dominant in this model, it is difficult to identify distributions of the yield strength in tension. In this study, a simplified jellyroll model consisting of double-layer windings was devised to reflect different plastic characteristics of a jellyroll, and the proposed model was applied to an 18650 cylindrical battery under compressive loading conditions. One winding adopted the crushable foam model for representing the compressive plastic behavior, and the other winding adopted the elastoplastic models for tracking the tensile plastic behavior. The material parameters in the crushable foam model were calibrated by comparing the simulated force–displacement curve with the experimental one for the case where the cell was crushed between two plates when the punch was displaced by 7 mm. A specific cut-off value (10 MPa) was assigned to a yield stress limit in the elastoplastic model. Further, the computational model was validated with two more loading cases, a cylindrical rod indentation and a spherical punch indentation, as the punch was displaced by 6.3 mm and 6.5 mm, respectively. For three loading cases, deformed configurations and plastic strain distributions were investigated by finite element analysis. It was found that the proposed model clearly provides the plastic behavior both in compression and tension. For the crush simulation, the maximum compressive stress approached 222 MPa in the middle of the jellyroll, and the maximum effective plastic strain approached 60% in the middle of the layered roll. For indentation with the cylindrical and the spherical punch, the maximum effective plastic strain approached 52% and 277% in the layered roll, respectively. The local crack or location of a short circuit could be predicted from the maximum effective plastic strain. Full article
(This article belongs to the Special Issue Electrochemical Conversion and Energy Storage System)
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17 pages, 3239 KB  
Article
A New Elementary Method for Determining the Tip Radius and Young’s Modulus in AFM Spherical Indentations
by Stylianos Vasileios Kontomaris, Andreas Stylianou, Georgios Chliveros and Anna Malamou
Micromachines 2023, 14(9), 1716; https://doi.org/10.3390/mi14091716 - 31 Aug 2023
Cited by 5 | Viewed by 2440
Abstract
Atomic force microscopy (AFM) is a powerful tool for characterizing biological materials at the nanoscale utilizing the AFM nanoindentation method. When testing biological materials, spherical indenters are typically employed to reduce the possibility of damaging the sample. The accuracy of determining Young’s modulus [...] Read more.
Atomic force microscopy (AFM) is a powerful tool for characterizing biological materials at the nanoscale utilizing the AFM nanoindentation method. When testing biological materials, spherical indenters are typically employed to reduce the possibility of damaging the sample. The accuracy of determining Young’s modulus depends, among other factors, on the calibration of the indenter, i.e., the determination of the tip radius. This paper demonstrates that the tip radius can be approximately calculated using a single force–indentation curve on an unknown, soft sample without performing any additional experimental calibration process. The proposed method is based on plotting a tangent line on the force indentation curve at the maximum indentation depth. Subsequently, using equations that relate the applied force, maximum indentation depth, and the tip radius, the calculation of the tip radius becomes trivial. It is significant to note that the method requires only a single force–indentation curve and does not necessitate knowledge of the sample’s Young’s modulus. Consequently, the determination of both the sample’s Young’s modulus and the tip radius can be performed simultaneously. Thus, the experimental effort is significantly reduced. The method was tested on 80 force–indentation curves obtained on an agarose gel, and the results were accurate. Full article
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7 pages, 971 KB  
Article
Lateral Deformation of Human Red Blood Cells by Optical Tweezers
by Pavel Yale, Michel A. Kouacou, Jean-Michel E. Konin, Eugène Megnassan and Jérémie T. Zoueu
Micromachines 2021, 12(9), 1024; https://doi.org/10.3390/mi12091024 - 27 Aug 2021
Cited by 6 | Viewed by 2908
Abstract
In this paper, we studied the lateral deformation of human red blood cells (RBCs) during lateral indentation by an optically trapped silica bead with a diameter of 4.5 µm (Bangs Laboratories, Inc. Fishers, IN, USA). The images were captured using a CCD camera [...] Read more.
In this paper, we studied the lateral deformation of human red blood cells (RBCs) during lateral indentation by an optically trapped silica bead with a diameter of 4.5 µm (Bangs Laboratories, Inc. Fishers, IN, USA). The images were captured using a CCD camera and the Boltzmann statistics method was used for force calibration. Using the Hertz model, we calculated and compared the elastic stiffness resulting from the lateral force, showing that the differences are important and that the force should be considered. Besides the lateral component, this setup also allowed us to examine the lateral cell–bead interaction. The mean values of the cell shear stiffness measured during indentation were 3.37 ± 0.40 µN/m for biconcave RBCs, 3.48 ± 0.23 µN/m for spherical RBCs, and 3.80 ± 0.22 µN/m for crenelated RBCs, respectively. These results show that this approach can be used as a routine method for RBC study, because it enabled us to manipulate the cell without contact with the wall. Full article
(This article belongs to the Special Issue Optical Trapping of Micro/Nanoparticles)
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24 pages, 6340 KB  
Article
Novel Monitoring Techniques for Characterizing Frictional Interfaces in the Laboratory
by Paul A. Selvadurai and Steven D. Glaser
Sensors 2015, 15(5), 9791-9814; https://doi.org/10.3390/s150509791 - 27 Apr 2015
Cited by 18 | Viewed by 6152
Abstract
A pressure-sensitive film was used to characterize the asperity contacts along a polymethyl methacrylate (PMMA) interface in the laboratory. The film has structural health monitoring (SHM) applications for flanges and other precision fittings and train rail condition monitoring. To calibrate the film, simple [...] Read more.
A pressure-sensitive film was used to characterize the asperity contacts along a polymethyl methacrylate (PMMA) interface in the laboratory. The film has structural health monitoring (SHM) applications for flanges and other precision fittings and train rail condition monitoring. To calibrate the film, simple spherical indentation tests were performed and validated against a finite element model (FEM) to compare normal stress profiles. Experimental measurements of the normal stress profiles were within −7.7% to 6.6% of the numerical calculations between 12 and 50 MPa asperity normal stress. The film also possessed the capability of quantifying surface roughness, an important parameter when examining wear and attrition in SHM applications. A high definition video camera supplied data for photometric analysis (i.e., the measure of visible light) of asperities along the PMMA-PMMA interface in a direct shear configuration, taking advantage of the transparent nature of the sample material. Normal stress over individual asperities, calculated with the pressure-sensitive film, was compared to the light intensity transmitted through the interface. We found that the luminous intensity transmitted through individual asperities linearly increased 0.05643 ± 0.0012 candelas for an increase of 1 MPa in normal stress between normal stresses ranging from 23 to 33 MPa. Full article
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