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Authors = K. Manigandan

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19 pages, 4606 KiB  
Article
Thermomechanical Characterization of SiC/SiC Ceramic Matrix Composites in a Combustion Facility
by Ragav P. Panakarajupally, Michael J. Presby, K. Manigandan, Jianyu Zhou, George G. Chase and Gregory N. Morscher
Ceramics 2019, 2(2), 407-425; https://doi.org/10.3390/ceramics2020032 - 17 Jun 2019
Cited by 37 | Viewed by 5665
Abstract
A combustion facility which includes uniaxial mechanical loading was implemented that enables environmental conditions more akin to jet engine environments compared to conventional static environment tests. Two types of woven SiC/SiC ceramic matrix composites (CMCs), melt-infiltrated (MI) and chemical vapor infiltrated (CVI), were [...] Read more.
A combustion facility which includes uniaxial mechanical loading was implemented that enables environmental conditions more akin to jet engine environments compared to conventional static environment tests. Two types of woven SiC/SiC ceramic matrix composites (CMCs), melt-infiltrated (MI) and chemical vapor infiltrated (CVI), were subjected to fatigue loading in the combustion facility and under isothermal furnace conditions. Some CVI test coupons were coated with a multilayer environmental barrier coating (EBC) of mullite + ytterbium monosilicate using slurry infiltration process to demonstrate the performance with a coating. Combustion conditions were applied using a high velocity oxy fuel gun on the front side of the specimen and mechanical loading was applied using a horizontal hydraulic MTS machine. All the specimens considered were subjected to tension-tension fatigue loading at 100 MPa, stress ratio of 0.1 and specimen front-side surface temperature of 1200 ± 20 °C. Nondestructive evaluation (NDE) methods, such as electrical resistance (ER), was used as an in-situ health monitoring technique. Similar fatigue tests were performed in an isothermal furnace for comparison. A much lower fatigue life was observed for the uncoated specimens tested under combustion conditions in comparison to isothermal furnace condition. This difference in fatigue life was attributed to damage associated with added thermal stress due to the thermal gradient and higher rate of oxidative embrittlement due to the presence of high velocity combustion gases in the combustion environment. EBC coating increased the fatigue life in combustion environment. However, EBC coated specimens experienced spallation in the high-velocity flame due to the presence of micro cracks in the coating surface. Fracture surfaces of the failed specimens were investigated under the scanning electron microscope (SEM) to determine the extent of oxidation and damage. Full article
(This article belongs to the Special Issue Damage and Lifetime of Ceramic Matrix Composites)
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27 pages, 8203 KiB  
Article
Influence of Nickel Particle Reinforcement on Cyclic Fatigue and Final Fracture Behavior of a Magnesium Alloy Composite
by Tirumalai S. Srivatsan, K. Manigandan, Chinmay Godbole, Muralidharan Paramsothy and Manoj Gupta
Metals 2012, 2(2), 143-169; https://doi.org/10.3390/met2020143 - 7 Jun 2012
Cited by 10 | Viewed by 9680
Abstract
The microstructure, tensile properties, cyclic stress amplitude fatigue response and final fracture behavior of a magnesium alloy, denoted as AZ31, discontinuously reinforced with nano-particulates of aluminum oxide and micron size nickel particles is presented and discussed. The tensile properties, high cycle fatigue and [...] Read more.
The microstructure, tensile properties, cyclic stress amplitude fatigue response and final fracture behavior of a magnesium alloy, denoted as AZ31, discontinuously reinforced with nano-particulates of aluminum oxide and micron size nickel particles is presented and discussed. The tensile properties, high cycle fatigue and final fracture behavior of the discontinuously reinforced magnesium alloy are compared with the unreinforced counterpart (AZ31). The elastic modulus and yield strength of the dual particle reinforced magnesium alloy is marginally higher than of the unreinforced counterpart. However, the tensile strength of the composite is lower than the monolithic counterpart. The ductility quantified by elongation to failure over 0.5 inch (12.7 mm) gage length of the test specimen showed minimal difference while the reduction in specimen cross-section area of the composite is higher than that of the monolithic counterpart. At the microscopic level, cyclic fatigue fractures of both the composite and the monolithic alloy clearly revealed features indicative of the occurrence of locally ductile and brittle mechanisms. Over the range of maximum stress and at two different load ratios the cyclic fatigue resistance of the magnesium alloy composite is superior to the monolithic counterpart. The mechanisms responsible for improved cyclic fatigue life and resultant fracture behavior of the composite microstructure are highlighted. Full article
(This article belongs to the Special Issue Magnesium Technology)
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