3.1. Minimal Surfaces
Mathematically, a minimal surface is a surface that locally minimizes its area, and hence has zero mean curvature. Minimal surfaces are those considered to contain minimum potential energy and are the most stable [
21]. A physical model to see the formation of a minimal surface can be made by dipping a wire frame into a soap solution, forming a soap film, which is a helicoid minimal surface, the boundary of which is the wire frame, as can be seen in
Figure 4.
The gyroid is a triply periodic minimal surface (TPMS), which is one of the most studied surfaces, and is used to create structures showing a characteristic robust mechanical performance. This minimal surface was first described by a NASA scientist. This surface seems to be the only known example of an intersection-free infinite periodic minimal surface which contains neither straight lines nor plane lines of curvature. The geometry of the gyroid surface unit cell and lattice is shown in
Figure 5. Trigonometrically, the gyroid surface can be approximated by the equation: sin(x)cos(y) + sin(y)cos(z) + sin(z)cos(x) = 0. It was demonstrated that with sandwich panel structures with minimal surfaces, particularly gyroid, cores considerably lower material consumption while simultaneously maintaining mechanical properties [
22]. Gyroids make MEX parts stronger and lighter.
Due to the complexity of this structure, it was designed by computational means, but was not able to be manufactured until the arrival of additive manufacturing. This method allows for accurate replication of the most sophisticated bio-inspired surfaces and structures, allowing them to reach their best mechanical properties. Some studies were performed to understand the mechanical properties of gyroid structures under bending forces, varying some of their principal parameters to analyze how their mechanical behavior is modified. One of the most influential parameters is the gyroid thickness, which results in an obvious stiffness increase with a deformation decrease due to a decrease in the porosity of the structure [
23]. Further, the von Mises and shear stresses decrease when the gyroid thickness increases. Although a greater thickness usually implies better mechanical properties, the weight of the structure is increased. Therefore, when considering applications where light-weight structures are desired, a balance between mechanical behavior improvement and the weight should be found.
Furthermore, other studies were performed to analyze the behavior of gyroid cells under compressive loads, wherein the infill density was varied to study how this parameter affects the mechanical properties of the structure. Independently of the infill density, gyroid structures deform uniformly within the elastic region, but higher relative densities lead to a more uniform deformation. In addition, when the infill density is increased, the performance of structures under compressive forces is obviously improved. The advantages of using gyroid-like structures include their high stiffness and low maximum von Mises stress compared to other cell types, making them particularly suitable for use in lightweight components. Gyroid structures have two regions of localized deformation per unit cell, while other TPMS structures possess only one region per unit cell. In addition, unlike other TPMS lattices, gyroid-like structures possess axisymmetric stiffness, meaning that these structures will be able to withstand forces acting on the structure in many directions, and are therefore very suitable for applications where there are uncertainties about the magnitude and direction of the forces acting on the body.
3.2. Test Specimens Design and Manufacturing
To investigate the orthotropic properties of the extrusion-based AM, various mechanical tests, such as flexural and compressive tests, were conducted. Polylactic acid (PLA) was chosen to be used as the AM material; its characteristics are shown in
Table 2.
A gyroid lattice was generated using Matlab (The Math Works, R2020b) and imported separately into Ultimaker Cura 4.8.0, the program used to set up the test sample to be 3D printed, where Prusa i3 Mk3s (Prusa Research, Prague, Czech Republic) (
Figure 6) was selected as the 3D printer. The test samples were set to contain a gyroid infill, and the density (
λinfill) was varied to study how this affects the mechanical behavior of the structure. Hence
λinfill depends on the case study. As the cuboid and the plates were imported as two separate models, the cuboid infill density was set to the specific percentage being studied, whilst the plates always had an infill density of 100%. In addition, the shell setting was used to modify the model wall thickness, by treating both models separately. The cuboid model was set to have no wall count for both the bottom and top layers. On the other hand, the plate model was set to have a wall count of 1 with a wall thickness of 0.8 mm. The printing settings used with the Prusa i3 Mk3 are shown in
Table 3.
Another variable that was studied along with the infill density was the printing filament angle. To study this, the Blackbelt 3D printer (Blackbelt 3D B.V., Belfeld, The Netherlands) (
Figure 7) was used, as it allows for printing under various nozzle angles. This is a continuous turning belt base printer that is able to produce series by printing individual models continuously or by producing very long parts. As this printer has the characteristic of infinite Z print, BlackBelt Cura 3.6.2 was used to slice the samples for this printer. This software is a version of Cura specially programmed for the Blackbelt printer. The main difference in the setup process is the explicit specification of the printing angle.
A parametric study was performed by changing different parameters in the setup to analyze the mechanical behavior of the structure with a gyroid pattern infill. The parameters chosen to study were the infill density (
λinfill), the printing angle (
θp), and the specimen thickness (
th). Carbon-fiber-reinforced plastic (CFRP) inserts were considered in some cases. Carbon fiber is used in this study due to its excellent specific strength compared to that of the other continuous fibers. Mechanical characterization of the coupons was performed to obtain the mechanical properties required by the simulation [
7,
25]. The infill density and printing angle were modified by changing the printing settings for the two different 3D printers. The sample geometry had a length (
l) of 140 mm, a width (
b) of 30 mm, and a height (or thickness) (
th) of 15 mm. These dimensions were kept constant along the whole experiment to ensure fair tests. Tests were performed under ISO 178:2019 standards [
26] using an Instron 5967 (Illinois Tool Works Inc., Glenview, IL, USA) 30 kN load cell with a loading rate of 0.5 mm/s. The first test was performed by adjusting the printing settings in Ultimaker Cura with a gyroid infill pattern using an infill density of
λinfill = 9.5%. Depending on the orientation the specimens had on the build plate, the gyroid was printed in one direction or another; therefore this was studied by printing 3 specimens in each direction, called X and Y, as shown in
Figure 8. The second test involved the same principles as the first one, but this time with
λinfill = 13%. Additionally at this stage, CFRP rods with a diameter of 1.5 mm were inserted into the structure through four different points of the specimen to investigate how the reinforcement of the external elements would affect the results. The CFRP rods were connected to the gyroid structure with epoxy glue and inserted through the longitudinal wholes generated by the gyroid infill pattern. The resulting test samples for the second test can be seen in
Figure 9. Four specimens were printed in each direction, X and Y, and were tested with and without CFRP rods, with a total of sixteen specimens printed in this case.
To perform the third test, the procedure was exactly the same as that for the second test. However, in this case,
λinfill = 15%. Four specimens were printed in each direction, X and Y, and were tested with and without CFRP rods, with a total of 16 specimens therefore printed. The fourth test studied the variation in the printing angle,
θp. In this case, the software BlackBelt Cura was used to specify the printing settings. Throughout the test, the parameters of all the specimens were kept constant, except for the printing angle, which was studied for
θp = 15°, 25°, and 45°, as shown in
Figure 10. The infill density of these specimens was 15%. The addition of CFRP rods supposed an increase in mass of 10.8%, high enough to be considered as a design factor.
3.3. Flexural Test Analysis
A three-point bending flexural test was performed to simulate the main forces present during flight on an aircraft wing. The test method involved the use of a specified test fixture on a universal testing machine; the sample was placed on two supporting pins with a span distance (
L) of separation between them (ISO 178:2019) (
Figure 11). Then, a load descended that applied a desired force (
F), deforming the specimen until a deflection settled. A span distance between both supports of
L= 100 mm was set on the machine. To make it fair, all the tests were performed under the same conditions. In addition, 4 samples were examined for each configuration of test probe. These data will be used throughout this section to calculate the flexural stress and strain for each of the cases, allowing a comparison of these experimental results with those obtained by FE methods in the future.
The total deformation includes the bending component
δb and shear component
δs., the deformation,
δ, can be obtained as:
where:
p is the applied load,
l is the total length of the beam,
is the equivalent flexural rigidity,
is the equivalent shear rigidity, and
B1 and
B2 are constants of proportionality. The equivalent flexural and shear rigidity can be calculated as:
where
is the Young´s modulus of the core,
Ef is the Young´s modulus of the face sheets,
is the shear modulus of the core [
22].
The first test performed was for the samples with
λinfill = 9.5% and
θp = 0°. Average values were calculated from the results obtained for both directions of the gyroid infill, which are shown in
Figure 12.
Those specimens printed in the X direction reached their yield limit at a greater force, which means these specimens had a greater yield strength. Further, the deformation of the specimen at the elastic limit was approximately the same for both cases; it occurred at about 3.8 mm. From that point onwards, the specimens continued deforming without reaching the breaking point. This occurred due to the 0° printing direction, as the strength contribution from the filaments did not depend on the quality of the joint between the filaments. This printing angle represented the deposition of filaments along the principal stress lines which, as will be seen in this section, improved the anisotropic limitation of the conventional layer-based MEX.
In addition, flexural stress and strain were calculated, confirming their behavior. Further, the maximum flexural stress value (σ
f,max), which is the point where the specimen bears the maximum stress, and the maximum flexural strain value (ϵ
f,max), which is the maximum strain the specimen can bear before breaking, were calculated and are shown in
Table 4. Therefore, these results suggest that this printing method could be quite appropriate for aircraft wings developed from additive manufacturing.
In order to extrapolate the results obtained experimentally in the case of a real UAV wing manufactured by an additive manufacturing processes, the test samples had to be printed with an angle of
θp = 90°. Therefore, the second test was performed over four samples printed with an infill density of 13% and a printing direction of 90°, tested for the gyroid in the X and Y direction. The mean and standard deviation of the results were plotted in the graph shown in
Figure 13.
It can be seen that the mechanical behavior of the specimens with the gyroid pattern printed in both directions was quite similar to that of the specimens that exhibited elastic behavior, until they suddenly broke with no plastic deformation. The average maximum load was approximately the same for X and Y cases, 261.3 N and 295.2 N, respectively. The samples exhibited high brittleness behavior, which is not the behavior desired for an aircraft wing, as wings should be flexible and show some elastic behavior—enough to allow for some wing buckling. Therefore, four CRFP rods were inserted per sample, keeping all parameters the same, to test their effect on the structure. The evolution of the bend extension of the specimen reinforced with CFRP rods and printed with an angle of 90° and infill density of 13% with an applied load is presented in
Figure 14 and
Table 5.
The results show that there were differences on the maximum flexural stress, but these were not significant, and that the maximum flexural strain increased when the rods were introduced. This suggests that the addition of these rods slightly improved the mechanical behavior of the structure; however, this small improvement did not compensate for the addition of extra weight to the structure, so the use of rods inserted in this way should be discarded.
In addition, as four samples were tested for each case, the standard deviation of the maximum flexural stress was calculated, as shown in
Table 4. Except for the case of the Y gyroid direction without rods, these values show that the variability of the data set is relatively low, as the standard deviation is relatively low. This means that the results obtained are quite precise and do not vary much from the mean value, making this quite representative. For the case of the Y gyroid direction without rods, more tests could be performed to obtained more reliable results.
The same test as before was performed for an infill density of 15% instead of 13%, without implementing the CRFP rods. This test allowed for a comparison of the results obtained for different infill densities. The mean and standard deviation of the results obtained for the fourth test were plotted in the graph shown in
Figure 15. As seen in the results, the mechanical behavior of the specimens was very similar to that shown previously in the second test with an infill density of 13%, therefore reaching the same conclusions. Surprisingly, comparing both results, the average yield stress of the structure decreased as the infill density increased, but the average maximum strain increased. Nevertheless, again, this high brittleness behavior shown by the specimens printed in these conditions is not the desired behavior for an aircraft wing.
A parametric study was performed that varied the printing angles, leaving three cases for study, for angles of 15°, 25°, and 45°, and the average results for each printing angle were plotted, as shown in
Figure 16. For the specimens printed with an angle of 15°, the results show a high yield strength. Nevertheless, the specimen did not break as the gyroid structure in the inside, together with the angle adopted by the PLA filaments in the printed piece, absorbed the load applied by deforming themselves, which resulted in an increasing in the extension.
When the printing angle of the specimens was increased to 25°, the average yield strength increased. However, in this case, from this point, the specimen started to deform plastically until it reached the breaking point around an extension of 25 mm, showing a high ductility, as it was able to absorb a lot of energy in the plastic region.
The last bending test performed was with samples of specimens printed with an angle of 45°. From the results, it can be said that there was an increase in the yield strength with respect to the previous cases. This means that an increase in the printing angle led to an increase in the yield strength of the structure. The breaking point was rapidly reached, at an extension of approximately 10 mm.
From
Figure 16, it can be observed that initially the three cases showed very similar behavior; however, the greater the printing angle, the greater the load the structure was able to withstand before it started to deform and show plastic behavior; therefore, after this, it did not return to its original shape. This means that the maximum yield strength increased with increases in the printing angle. As an average, for the samples printed at an angle of 15°, the elastic limit was reached at approximately a force of 275 N and an extension of 3.7 mm, whilst for those printed at an angle of 25°, the elastic point appeared at 282 N and 3.9 mm, and for the samples printed at 45°, these values were 304 N and 3.8 mm.
Figure 16.
Evolution of the bend deformation of the specimen, printed at different degrees, with an applied load.
Figure 16.
Evolution of the bend deformation of the specimen, printed at different degrees, with an applied load.
On the other hand, analyzing
Figure 16, it can be seen how those samples printed at lower angles were able to withstand forces for a longer period before breaking by deforming themselves, or even without breaking, as was the case for the samples printed at 15°. In these cases, the structure was able to absorb greater quantities of energy in the elastic region. This suggests that for greater printing angles, the breaking point of the structure will be reached earlier, and therefore will deform less before breaking.
The results in
Table 5 show a clear trend:
σf,max increased when
θp increased, whilst
ϵf,max decreased when
θp increased. The differences in
ϵf,max with variations in
θp were much more significant than those for
σf,max. This shows that the optimal printing angle is the one which approximates 0°, because the deposition of filaments along the principal stress lines improves the anisotropic limitation of the conventional layer-based MEX, but this may require more forming material. Therefore, the smaller the angle, the greater the deformation of the structure before it collapsed, withstanding very similar maximum loads in each case.
Moreover, the calculation of the standard deviation for each case shown in
Table 6 suggests results are relatively precise and the actual mean could be used as a representative value.
After the analysis performed from the results obtained for the bending tests, some conclusions can be made regarding the optimization of the mechanical properties of a wing with a gyroid infill. Firstly, it is preferable to print the gyroid pattern in the Y direction when a conventional printer is used. When considering a Z-infinite printer applied to a wing structure, the best mechanical properties are obtained with smaller printing angles. Finally, the infill density should be as high as possible, and the weight of the structure should not be compromised, as with greater infill densities, the best mechanical properties, applicable to wings, are obtained.
3.4. Compression Test Analysis
Compression tests are used to determine the behavior of a material under applied crushing loads and are typically conducted by applying compressive pressure to a test specimen (usually of either a cuboid or cylindrical geometry) using plates or specialized fixtures on a universal testing machine. To proceed with the test, the sample is placed in between the two plates that distribute the applied load across the entire surface area of two opposite faces of the test sample, and then the plates are pushed together by a universal test machine, causing the sample to flatten.
The purpose of performing this test is to understand the mechanical behavior of the sample under compressive forces by measuring fundamental variables, such as strain, stress, and deformation. An analysis of the results obtained for these parameters, together with the values of a specific material, will allow for determining the suitability of the material test for specific applications. These materials tested often need to have a great load-bearing capacity under compressive forces, for which it is crucial their integrity and ability to maintain their shape without plastically deforming are sustained. There are different types of compression tests, including the top load test, which was performed in this case. In the following subsections, the experiment setup, as well as the results obtained, will be further explained. To evaluate the mechanical compressive behavior of the specimens, the tests were performed, as stated before, with a universal material electromechanical testing machine, at standard conditions (atmospheric pressure of 1 atm and temperature of 20 °C). The machine was set with the compression plates available in the laboratory, which were specific to the testing machine being used, and was mounted as shown in
Figure 17. All the tests were performed under the same conditions, with a maximum compression of 20 mm. In addition, to ensure a reliable test, four samples were tested for each configuration of the test probe.
In this case, the specimens designed for the experiment used the same principles as those used to design the specimens for the bending test. First, a cuboid was designed, and then two plates were placed on the top and bottom of the structure, and a gyroid infill was developed on the inside of the structure. However, in this case, the lengths of the specimens were different, leaving the following dimensions: l= 70 mm, b= 30 mm, and d= 15 mm. After performing the compression tests, the universal material electromechanical testing machine stored all the relevant data measured from the tests in raw Excel documents, which were used to plot the specific graphs for each case study. Then, these plotted graphs were used to analyze the results obtained.
Figure 17.
Compression test setup with specimen between plates.
Figure 17.
Compression test setup with specimen between plates.
The first test performed was for those samples where the variations in the infill density were studied under compressive forces for
λinfill = 9.5%,
λinfill = 13%, and
λinfill = 15%. It can be seen that the specimens underwent a deformation with a similar pattern for different infill densities, reaching a small peak at the start where the elastic region ended. Then, the specimens started to deform plastically, reaching a point where the infill gyroid structure was fully collapsed at about 9 mm of deformation, and the load applied tended to infinity with nearly no deformation. However, this last part was cut from the graph, as it is not valuable to the purpose of the research; the plot was kept between the range of values that could be reached during a real situation [
27].
Comparing the average results obtained for each infill density (
Figure 18), surprisingly, it can be seen that the specimens with the highest yield strength were those with
λinfill = 13%, whilst those specimens with
λinfill = 9.5% were the least strong. This graph shows that the specimens with
λinfill = 13% had the highest maximum compressive stress, but those specimens with
λinfill = 15% had the highest strain before the structure showed plastic deformation.
As was demonstrated, the infill density plays an important role in the mechanical behavior of the structure under compressive forces, as with an increase in the infill density, the structure becomes stronger and stiffer, but it will increase its weight considerably. Therefore, as this will be applied to the case of an aircraft wing where weight must be minimized, a commitment between the strength required under compressive forces and the weight of the structure should be obtained.
Next, how the thickness of the structure affects its compressive behavior was studied. For this, the test was carried out using a specimen of the following dimensions:
l = 15 mm,
b = 20 mm and
h = 25 mm. The specimens used in this case were manufactured with a Blackbelt 3D printer and were therefore printed with the filaments placed in a non-horizontal plane. This means that this test also enabled us to study how the printing angle affects the mechanical behavior of the structure. For each thickness, four samples were tested, and average values were calculated, as shown in
Figure 19. The deformation was 12 mm for each coupon.
The specimens underwent a deformation with a similar pattern for different thicknesses, reaching a small peak at the start where the elastic region ended. Then, the specimens started to deform plastically, reaching a point where the infill gyroid structure was fully collapsed and the load applied tended to infinity with nearly no deformation. For the case of h = 25 mm, after a deformation of nearly 15 mm, the structure did not reach this irreversible point, and it was observed during the test that the structure partially recovered its shape once the load was removed.
Analyzing
Figure 19, it can be observed where the elastic limit occurred in each case. For the specimens with
h = 15 mm, this point occurred at a deformation of about
e = 0.9 mm and with a force applied of
F = 890 N. For the case of
h = 20 mm, the elastic limit was reached around
e = 0.8 mm and F = 720 N. For the case of
h = 25 mm, the elastic limit was reached around
e = 0.75 mm and
F = 530 N. Interestingly, comparing in
Figure 19 the average results obtained for each thickness, it can be seen that the initial deformation slope was practically identical; however, the yield point peak was reached at a lower displacement and a lower force applied for the thicker specimens. This means that, when the thickness of the structure is increased, the structure will start to deform plastically at lower loads and with a smaller deformation. Even though from this point onwards the structure deforms plastically, it will still be able to return partially to its original shape and size.
Applying this to the case of an aircraft wing, these results suggest that the thickest parts of the wings will deform more easily, i.e., they will deform with a lower compressive force applied, but will be able to partially recover their shape once these forces are removed. Additionally, the thinner parts of the wing will be able to withstand greater compressive forces, deforming elastically in the process.
Figure 19.
Comparison of the evolution of the displacement of the specimen with a force applied for different thicknesses.
Figure 19.
Comparison of the evolution of the displacement of the specimen with a force applied for different thicknesses.
Furthermore, the last factor that was analyzed under compressive forces was the election of the additive manufacturing system. By comparing the results obtained for specimens with the same thickness (h = 15 mm) in
Figure 18 and
Figure 19 it can be clearly seen that specimens printed with a conventional printer have a greater deformation before the yield point, which is reached with the application of a greater load. Therefore, these structures seem to be stronger under compressive forces. In addition, structures printed with the conventional 3D printer collapse entirely after a greater deformation. This means that, generally, it is preferable to manufacture structures with a conventional 3D printer, rather than with an infinite Z printer, which places filaments on a certain angle, as those structures should be able to withstand great compressive forces, as was demonstrated.